[Summary]

File Name TYOCT.DAT

Date of measurement 11/10/2021
Time of measurement 9:20:19
COMMENT1 TYOCT
COMMENT2 dehdashti
COMMENT3 180C 30MIN
COMMENT4 Taban Lab
Serial number 888
Version

Sample weight 0.0834 [g] Saturated vapor pressure 85.255 [kPa]

Standard volume 9.779 [cm3] Adsorption cross section area 0.162 [nm2]
Dead volume 14.715 [cm3] File name of walladsorption
Equilibrium time 0 [sec] all adsorption correction value 1
Adsorptive N2 all adsorption correction value 2
Apparatus temperature 0 [C] Number of adsorption data 29
Adsorption temperature 77.000 [K] Number of desorption data 21

BET plot
Vm 47.252 [cm3(STP) g-1]
as,BET 205.66 [m2 g-1]
C 124.66
Total pore volume(p/p0=0.990) 0.4749 [cm3 g-1]
Mean pore diameter 9.2364 [nm]
Langmuir plot
Vm 39.152 [cm3(STP) g-1]
as,Lang 170.41 [m2 g-1]
B 7.0001
t plot
Plot data Adsorption branch
a1 199.21 [m2 g-1]
V1 0 [cm3 g-1]
BJH plot
Plot data Adsorption branch
Vp 0.4811 [cm3 g-1]
rp,peak(Area) 3.09 [nm]
ap 249.5 [m2 g-1]
[Adsorption / desorption isotherm]
File Name TYOCT.DAT
Date of measurement 11/10/2021
Time of measurement 9:20:19
COMMENT1 TYOCT
COMMENT2 dehdashti
COMMENT3 180C 30MIN
COMMENT4 Taban Lab
Serial number 888
Version

Sample weight 0.0834 [g] Saturated vapor pressure 85.255 [kPa]

Standard volume 9.779 [cm3] Adsorption cross section area 0.162 [nm2]
Dead volume 14.715 [cm3] File name of walladsorption
Equilibrium time 0 [sec] all adsorption correction value 1
Adsorptive N2 all adsorption correction value 2
Apparatus temperature 0 [C] Number of adsorption data 29
Adsorption temperature 77.000 [K] Number of desorption data 21

Al 25%Ni
No pi/kPa pe/kPa pe2/kPa p0/kPa p/p0 Va/cm3(STP) g-1 p/p0
ADS
1 0 0.2005 0 85.016 0.0023587 22.864 302.864 0.0090803
2 0 1.8633 0 85.032 0.021913 36.364 316.364 0.020371
3 0 4.8634 0 85.048 0.057184 43.155 323.155 0.055732
4 0 5.9134 0 85.083 0.069502 44.777 324.777 0.073812
5 0 7.1868 0 85.148 0.084404 46.539 326.539 0.089223
6 0 8.8617 0 85.371 0.1038 48.614 328.614 0.1091
7 0 9.236 0 85.392 0.1082 49.064 329.064 0.1339
8 0 11.071 0 85.405 0.1296 51.151 331.151 0.1494
9 0 12.481 0 85.407 0.1461 52.692 332.692 0.1645
10 0 13.806 0 85.412 0.1616 54.082 334.082 0.1843
11 0 15.473 0 85.401 0.1812 55.832 335.832 0.2236
12 0 18.711 0 85.403 0.2191 59.193 339.193 0.254
13 0 21.38 0 85.419 0.2503 62.028 342.028 0.3036
14 0 25.549 0 85.392 0.2992 66.567 346.567 0.3522
15 0 29.639 0 85.389 0.3471 71.398 351.398 0.4516
16 0 37.255 0 85.358 0.4365 81.724 361.724 0.5488
17 0 38.437 0 85.328 0.4505 83.554 363.554 0.6431
18 0 45.869 0 85.307 0.5377 96.827 376.827 0.6516
19 0 46.764 0 85.318 0.5481 98.91 378.91 0.7351
20 0 52.19 0 85.262 0.6121 112.84 392.84 0.7456
21 0 55.051 0 85.205 0.6461 122.17 402.17 0.8294
22 0 64.228 0 85.199 0.7539 171.69 451.69 0.8384
23 0 66.132 0 85.195 0.7762 188.77 468.77 0.8463
24 0 74.359 0 85.152 0.8733 248.71 528.71 0.933
25 0 77.744 0 85.146 0.9131 267.5 547.5 0.9469
26 0 81.249 0 85.187 0.9538 283.57 563.57 0.969
27 0 82.384 0 85.174 0.9672 291.2 571.2 0.988
28 0 83.981 0 85.221 0.9854 302.06 582.06 0.9911
29 0 84.35 0 85.187 0.9902 307.21 587.21
DES 280 0.9684
1 0 83.078 0 85.19 0.9852 304.61 584.61 0.9477
2 0 82.772 0 85.182 0.9717 302.86 582.86 0.8563
3 0 81.242 0 85.168 0.9539 297.42 577.42 0.8474
4 0 76.818 0 85.164 0.902 284.13 564.13 0.804
5 0 73.775 0 85.156 0.8664 273.63 553.63 0.7594
6 0 72.135 0 85.187 0.8468 267.38 547.38 0.7509
7 0 69.027 0 85.185 0.8103 255.53 535.53 0.6789
8 0 68.521 0 85.187 0.8044 253.25 533.25 0.6611
9 0 65.753 0 85.195 0.7718 241.25 521.25 0.6524
10 0 64.252 0 85.184 0.7543 233.35 513.35 0.5721
11 0 61.544 0 85.223 0.7222 216.99 496.99 0.5511
12 0 59.319 0 85.189 0.6963 198.57 478.57 0.4419
13 0 53.865 0 85.223 0.632 137.3 417.3 0.3506
14 0 50.418 0 85.268 0.5913 120.17 400.17 0.2971
15 0 47.498 0 85.353 0.5565 109.39 389.39
16 0 47.038 0 85.35 0.5511 107.64 387.64
17 0 41.505 0 85.373 0.4862 93.86 373.86
18 0 38.496 0 85.355 0.451 87.738 367.738
19 0 31.573 0 85.363 0.3699 76.313 356.313
20 0 29.861 0 85.358 0.3498 70.866 350.866
21 0 25.42 0 85.344 0.2979 66.116 346.116

Chart Title

300

250
V a/cm3 (STP) g-1

200

150

100

50

0
0 0.1 0.2 0.3 0.4 0.5 0.6 0.7 0.8 0.9 1
p/p0
[BET plot]
File Name TYOCT.DAT
Date of measurement 11/10/2021
Time of measurement 9:20:19
COMMENT1 TYOCT
COMMENT2 dehdashti
COMMENT3 180C 30MIN
COMMENT4 Taban Lab
Serial number 888
Version

Sample weight 0.0834 [g] Saturated vapor pressure 85.255 [kPa]

Standard volume 9.779 [cm3] Adsorption cross section area 0.162 [nm2]
Dead volume 14.715 [cm3] File name of walladsorption
Equilibrium time 0 [sec] all adsorption correction value 1
Adsorptive N2 all adsorption correction value 2
Apparatus temperature 0 [C] Number of adsorption data 29
Adsorption temperature 77.000 [K] Number of desorption data 21

Starting point 1
End point 13
Slope(Linear) 0.020994
Intercept(Linear) 0.00016977
Correlation coefficient 0.9996
Vm 47.252 [cm3(STP) g-1]
as,BET 205.66 [m2 g-1]
C 124.66
Total pore volume(p/p0=0.990) 0.4749 [cm3 g-1]
Mean pore diameter 9.2364 [nm]

No p/p0 p/Va(p0-p)
0 0 0
1 0.0023587 0.00010341
2 0.021913 0.0006161
3 0.057184 0.0014055
4 0.069502 0.0016681
5 0.084404 0.0019808
6 0.1038 0.0023825
7 0.1082 0.0024718
8 0.1296 0.0029117
9 0.1461 0.003248
10 0.1616 0.0035651
11 0.1812 0.0039631
12 0.2191 0.0047397
13 0.2503 0.0053824
14 0.2992 0.0064136
15 0.3471 0.0074462
16 0.4365 0.0094768
17 0.4505 0.0098105

Chart Title
0.012

0.008
p/V a(p 0-p)
 0.008
p/V a(p 0-p)

0.004

0
0 0.25
p/p0 0.5
[Langmuir plot]
File Name TYOCT.DAT
Date of measurement 11/10/2021
Time of measurement 9:20:19
COMMENT1 TYOCT
COMMENT2 dehdashti
COMMENT3 180C 30MIN
COMMENT4 Taban Lab
Serial number 888
Version

Sample weight 0.0834 [g] Saturated vapor pressure 85.255 [kPa]

Standard volume 9.779 [cm3] Adsorption cross section area 0.162 [nm2]
Dead volume 14.715 [cm3] File name of walladsorption
Equilibrium time 0 [sec] all adsorption correction value 1
Adsorptive N2 all adsorption correction value 2
Apparatus temperature 0 [C] Number of adsorption data 29
Adsorption temperature 77.000 [K] Number of desorption data 21

Starting point 1
End point 2
Slope(Linear) 0.025542
Intercept(Linear 0.0036487
Correlation coeff 1
Vm 39.152 [cm3(STP) g-1]
as,Lang 170.41 [m2 g-1]
B 7.0001

No p/kPa p/Va
1 0.2005 0.0087706
2 1.8633 0.05124
3 4.8634 0.1127
4 5.9134 0.1321
5 7.1868 0.1544
6 8.8617 0.1823
7 9.236 0.1882
8 11.071 0.2164
9 12.481 0.2369
10 13.806 0.2553
11 15.473 0.2771
12 18.711 0.3161
13 21.38 0.3447
14 25.549 0.3838
15 29.639 0.4151
16 37.255 0.4559
17 38.437 0.46
18 45.869 0.4737
19 46.764 0.4728
20 52.19 0.4625
21 55.051 0.4506
22 64.228 0.3741
23 66.132 0.3503
24 74.359 0.299
25 77.744 0.2906
26 81.249 0.2865
27 82.384 0.2829
28 83.981 0.278
29 84.35 0.2746

Chart Title
0.6

0.4
 Chart Title
0.6

0.4
p/V a

0.2

0
0 45 90
p/kPa
[t plot]
File Name TYOCT.DAT
Date of measurement 11/10/2021
Time of measurement 9:20:19
COMMENT1 TYOCT
COMMENT2 dehdashti
COMMENT3 180C 30MIN
COMMENT4 Taban Lab
Serial number 888
Version

Sample weight 0.0834 [g] Saturated vapor pressure 85.255 [kPa]

Standard volume 9.779 [cm3] Adsorption cross section area 0.162 [nm2]
Dead volume 14.715 [cm3] File name of walladsorption
Equilibrium time 0 [sec] all adsorption correction value 1
Adsorptive N2 all adsorption correction value 2
Apparatus temperature 0 [C] Number of adsorption data 29
Adsorption temperature 77.000 [K] Number of desorption data 21

Plot data Adsorption branch

Starting point 0
End point 1
Slope(Linear) 129.27
Intercept(Linear) 0
a1 199.21 [m2 g-1]
V1 0 [cm3 g-1]
Starting point 33
End point 33

No p/p0 t/nm Va/cm3(STP) g-1

0 0 0 0
1 0.019797 0.27 34.903
2 0.023702 0.28 36.708
3 0.034754 0.3 38.836
4 0.048412 0.32 41.466
5 0.065713 0.34 44.278
6 0.086862 0.36 46.802
7 0.1119 0.38 49.425
8 0.1408 0.4 52.191
9 0.173 0.42 55.101
10 0.2079 0.44 58.197
11 0.244 0.46 61.455
12 0.2807 0.48 64.853
13 0.3171 0.5 68.373
14 0.3528 0.52 72.059
15 0.3876 0.54 76.077
16 0.4212 0.56 79.956
17 0.4535 0.58 84.012
18 0.4844 0.6 88.712
19 0.5135 0.62 93.153
20 0.5412 0.64 97.528
21 0.567 0.66 103.03
22 0.591 0.68 108.25
23 0.6135 0.7 113.21
24 0.6625 0.75 129.71
25 0.7032 0.8 148.42
26 0.7375 0.85 164.17
27 0.7668 0.9 181.57
28 0.8134 1 211.72
29 0.8492 1.1 233.86
30 0.8766 1.2 250.29
31 0.8965 1.3 259.69
32 0.9114 1.4 266.74
 33 0.9232 1.5 271.5

Chart Title
360

240
V a/cm3 (STP) g-1

120

0
0 1 2
t/nm
[BJH plot]
File Name TYOCT.DAT
Date of measurement 11/10/2021
Time of measurement 9:20:19
COMMENT1 TYOCT
COMMENT2 dehdashti
COMMENT3 180C 30MIN
COMMENT4 Taban Lab
Serial number 888
Version

Sample weight 0.0834 [g] Saturated vapor pressure 85.255 [kPa]

Standard volume 9.779 [cm3] Adsorption cross section area 0.162 [nm2]
Dead volume 14.715 [cm3] File name of walladsorption
Equilibrium time 0 [sec] all adsorption correction value 1
Adsorptive N2 all adsorption correction value 2
Apparatus temperature 0 [C] Number of adsorption data 29
Adsorption temperature 77.000 [K] Number of desorption data 21

Plot data Adsorption branch

Vp 0.4811 [cm3 g-1]
rp,peak(Area) 3.09 [nm]
ap 249.5 [m2 g-1]
25%Ni
No p/p0 rp/nm dVp/drp SVp/cm3 g-1 Sap/m2 g-1 rp/nm dVp/drp
1 0.99 95.277 0.00020641 0.0018483 0.038798 95.277 0.0003178
2 0.989 83.888 0.00026444 0.0055221 0.1264 83.888 0.00027375
3 0.987 71.898 0.00028662 0.0088142 0.218 71.898 0.00025201
4 0.985 61.313 0.0003194 0.011783 0.3148 61.313 0.00027265
5 0.982 53.044 0.00037588 0.013775 0.3899 53.044 0.00033081
6 0.98 46.13 0.00050316 0.017753 0.5624 46.13 0.00042035
7 0.976 39.006 0.00071101 0.02176 0.7679 39.006 0.00055542
8 0.972 33.814 0.00093641 0.025815 1.0077 33.814 0.00074108
9 0.968 29.501 0.0012385 0.030733 1.3411 29.501 0.0011152
10 0.963 25.548 0.0015409 0.036682 1.8068 25.548 0.0018203
11 0.957 22.072 0.0018266 0.042518 2.3356 22.072 0.0027972
12 0.95 18.936 0.0022495 0.048763 2.9952 18.936 0.0038101
13 0.941 16.287 0.0029386 0.05509 3.7721 16.287 0.0046154
14 0.932 14.125 0.0040847 0.062917 4.8803 14.125 0.005278
15 0.921 12.244 0.0059886 0.072199 6.3966 12.244 0.006596
16 0.909 10.651 0.0084926 0.084624 8.7297 10.651 0.010045
17 0.895 9.2279 0.01325 0.099988 12.06 9.2279 0.016922
18 0.878 7.985 0.019967 0.1219 17.539 7.985 0.02676
19 0.859 6.9462 0.028428 0.1481 25.104 6.9462 0.036525
20 0.838 6.0589 0.038216 0.1786 35.167 6.0589 0.044161
21 0.814 5.2867 0.054539 0.2135 48.345 5.2867 0.049375
22 0.787 4.6128 0.063019 0.2612 69.041 4.6128 0.052878
23 0.756 4.0284 0.073258 0.2954 86.028 4.0284 0.055678
24 0.722 3.5256 0.082387 0.333 107.35 3.5256 0.056882
25 0.684 3.0877 0.081918 0.374 133.9 3.0877 0.057168
26 0.642 2.7075 0.077951 0.3972 151.08 2.7075 0.056386
27 0.596 2.3795 0.063958 0.4183 168.8 2.3795 0.05616
28 0.547 2.0972 0.063379 0.4333 183.05 2.0972 0.055802
29 0.495 1.8527 0.056626 0.4477 198.68 1.8527 0.055178
30 0.441 1.6395 0.052749 0.4576 210.75 1.6395 0.053163
31 0.385 1.2126 0.03592 0.4811 249.5 1.2126 0.047154

0 .1
Chart Title

Bio-Al (b)
(23.17%)Ni@Bio-Al
0. 8
(23.17%)Ni-(3. 7%)Ce@Bio-Al

0. 6
r p
0 .1
Chart Title

Bio-Al (b)
(23.17%)Ni@Bio-Al
0. 8
(23.17%)Ni-(3. 7%)Ce@Bio-Al

0. 6

p
d V /d r
p
0. 4

0. 2

0.
1 10 10
rp/nm
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