|. Identify one which does not come under the Chemical methods of qualitative analysis? a) Gravimetric b) Titrimetric c) Volumetric d@Magnetic Susceptibility 2. Select the inappropriate statement regarding quantitative analysis a) It helps in determining the outcome of the product b) It helps in determining the impurities in the sample @ [1 fails to indicate the presence of lead in some compound d) It could identify the amounts of dosage present in the drug 3, identify the test which is not a part of qualitative analysis? a@Litmus test b) Castle-Meyer test ( c) Iodine test d) Flame test 4. Analyses in which substances are identified or classified on the basis of their chemical or physical properties called as i ® Qualitative analysis b) Quantitative analysis c) Both a and b 4), None of these ’ 4 5 Testing used for finding out which functional group present in the compound. called as. a Qualitative analysis b) Quantitative analysis c) Both aandb d) None of these 6. The constituents those present in amounts between 100 ppm (0.01%) and 1 ppb are called a) major constituentsb) mi Y Minor g . Trae, - The consti s 1 are calne aunts those present in the Tange of 1 to 100% by mass of sample ® major Constituents b) minor Constituents ©) Trace constituents 4) Ultra trace constituents 8. The process by which a representative fraction is acquired from a material ot interest is termed as... a) Titration b) Calibration ® Sampling d) None of these 9, for laboratory analysis, the gross sample is usually reduced in size and homogenized to create the... a) Sampling unit b) Gross sample @) Laboratory sample dj All of these 10. Systematic errors can be eliminated by a) Exercizing care b) By calibration ¢) By the proper use of standards, @) All of these blanks, and reference materials . goses vem 11. Well-mixed solutions of liquids and gases rede a) More sample b) Fewer samples ¢) Small sample @) Both band c 12. In a titration, the analyte reacts with @ Standardized reagent called a8 sat b) Standardized reagents called calil c) Reactants. d) Products. ion 5 «in calibration '3. To avoid systematic enor wyepated f ©) Standards must be accurately PPP jemtica st be b) Chemical state of standards ™0¢) Both a and b d) None of these - a 14.How will you separate a solution (miscible) of benzene and CHC? a) Sublimation @ Distillation c) Filtration d) Crystallisation vcs sac tunine de 15. Which one of the following methods can be used to separate a mixture of ortho and para - nitrophenols? a) Crystallisation b) Solubility ¢) Sublimation @) Steam distillation 16. Which one of the following can be purified by sublimation? a) Fa b) Ch c) hy @ Br 17. Which is purified by steam distillation? ) Aniline b) Petroleum ¢) Benzoic acid d) Napthalene 18. Sublimation is a process in which a solid: @ Changes into vapor form b) Changes into another allotropic from. c) Changes into liquid form d) None of above 19. A mixture of camphor and benzoic acid can be separated by: a) Sublimation b) Extraction with a solvent @) Chemical method d) Fractional distillation 20. The best method for the separation of naphthalene and benzoic acid from their mixture is: a) Crystallisation @) Solvent extraction ¢) Chromatography 4d) Distillation 21. Vor the purification, isolation and separation of organic compounds, thelatest technique Followed is: @ Chromatography b) Steam distillation ©) Fractional crystallization. d) Sublimation 22. Which of the following reagents will be fruitful for separation of a mixture of nitrobenzene and aniline? a) H20 b) Aqueous NaOH c) Aqueous NaHCO3 gp raucous HT ing point can be purified by: 23. A liquid which decomposes at its b a) Distillation at atmospheric pressure @ Distillation under reduced pressure ¢) Fractional di tillation d) Steam distillation 24, Turpentine oil can be purified by: Steam distillation b) Vacuum distillation c) Fractional distillation d) Sublimation d out on-the-basis of theinextentol 25, Two substances when separate on is called: adsorption by one material, the phenomem @) Chromatography b) Crystallisation <) Sublimation ¢) Steam distillation 26. Vacuum distillation is used to purify liquids wnich: a) Are highly volatile 5) Are explosive in nature water @Pccomposes below their B.P's “) Solvent e: 4) Sublimation ‘Ntraction 2A Venice Y Powders, mon adsort y “red Sdzorbent Used jy eqtowmn chromaasrsPn® " charcoalc) Alumina d) Sodium carbonate 29. The latest technique for the purification of organic compounds is: a) Fractional distillation @ Vacuum distillation c) Chromatography d) Crystallization 30, Fixed melting point of an organic compound informs: @) Purity of an organic compound b) Conductivity of compound ¢) Chemical nature of compound d) Whether the compound is liquid or gas. 1. A mixture of camphor and KCI can be separated by Sublimation b) Decantation c) Evaporation d) Filtration 32. In steam distillation, the sum of the vapor pressure of the volatile compound and that of water is: a) Equal to atmospheric pressure ®) Less than atmospheric pressure c) More than atmospheric pressure d) Exactly half of the atmospheric pressure 33. Which of the following is an error that may occur in the measurement ofa physical quantity .. a) Systematic error b) Random error 7 c) Absolute error @! of the above 34, Which of the following is type of systematic error... a) Instrumental error b) Gross error ¢) Error due to dps! of the above imperfections t, it is found that the experimental value is very close to The‘experimental value ean be called 35. In an experiment! actual value, hence t @ Accurate b) Precisec) Suitable d) Mean 36. What is the reason for the occurrence of systematic errors in an ing, a) No use for a long time tte @ High use c) Manufacturing fault d) Delivery fault 37, How are systematic errors removed usually for an instrument? a) By replacing it @ By re-calibrating it c) By using a repairing service : d) By not using it for some time 38. in 5 experiments with the same objective, the values obtained are very near to each other. These values can be called @ precise b) Accurate c) Average d) Invalid 39.Mesurement that is close to the true value called as {40 Which of the following is type of determ! inate error. a) Instrumental error b) Operative error ¢) Error of method of the above 41.Ja the set 10,2,10.4,10.8,1 1,0,11.2 the median 1s...- a) 104 10.8 e110 d) 2 42, The F test is used ....- a) For rejection of data @ For testing of sign’ fiance c) For obtaining best itting line d) For completion of data43.Method of averages is used....... a) For rejection of data p) For testing of significance For obtaining best fitting line 4 d) For completion of data 44.For rejection of result, the test used is....- a) F-test b) Testing of significance 45, Standard deviation for the following set of results 10,28. 10,24.10.25,10,25.10.30 @) 0.0187 b) 10.26 ¢) 10.25 dy 0.223 46.For rejection of result which of the following rule is used a) 25d rule - ee by) 40d rule @, Bon aands d) None of these