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Resolution of α-Phenylethylamine Data Sheet

This document is a data sheet for an experiment involving the resolution of (±)-α-phenylethylamine. It includes spaces to record raw data from the experiment, including the mass or volume of various reagents and products. The data includes the mass of (±)-α-phenylethylamine used, tartaric acid used, weights of filter paper before and after drying salt crystals, the mass of the (-)-α-phenylethylammonium hydrogen (+) -tartrate salt obtained, weights of an empty beaker and beaker with solvent-free amine product, the mass and optical rotation of the (-)-α-phenylethylamine product obtained, and any observations. The data sheet is to be

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Meraal Syed
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53 views1 page

Resolution of α-Phenylethylamine Data Sheet

This document is a data sheet for an experiment involving the resolution of (±)-α-phenylethylamine. It includes spaces to record raw data from the experiment, including the mass or volume of various reagents and products. The data includes the mass of (±)-α-phenylethylamine used, tartaric acid used, weights of filter paper before and after drying salt crystals, the mass of the (-)-α-phenylethylammonium hydrogen (+) -tartrate salt obtained, weights of an empty beaker and beaker with solvent-free amine product, the mass and optical rotation of the (-)-α-phenylethylamine product obtained, and any observations. The data sheet is to be

Uploaded by

Meraal Syed
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
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Download as PDF, TXT or read online on Scribd
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EXPERIMENT 

3: RESOLUTION OF (±)‐α‐PHENYLETHYLAMINE 
DATA SHEET  
(to fill out in ink, to be signed by your TA and to include with your lab report) 
 
Your name: ________________________________    Lab Session Date: ___________________ 
 
Your TA’s name: ____________________________                Lab section: _______ 
 
Your lab partner’s name: ________________________ 

1. Complete the table below with your raw data IN INK.  
Do not include calculated yields, specific rotation or optical purity here. Report those in your lab 3 report.  
 
Volume used of (±)‐α‐phenylethylamine (from step 1 of part A in the lab manual) 
mL 
Mass of (+)‐tartaric acid used (from step 2 of part A)  g 

Weight of empty paper for air‐drying (step 2 of part B in the lab manual)  g 

Weight of paper with air‐dried salt crystals (step 2)  g 

Mass of (‐)‐α‐phenylethylammonium hydrogen (+)‐tartrate salt obtained  g 

Weight of empty 50 mL beaker containing 1 or 2 boiling stones (step 11)  g 

Weight of 50 mL beaker, boiling stone(s) and solvent‐free amine (step 14)  g 

Mass of (‐)‐α‐phenylethylamine obtained  g 

Raw optical rotation α of (‐)‐α‐phenylethylamine obtained (include the +/‐ sign of your   
measurement) 
Observations (use this space for any observations relevant to the results – use the reverse side for 
additional space) 
 
 
 
 
 
 
 
 
 
 
2. Get your TA to review this sheet and your partner’s sheet, and to sign it below before you leave. 
3. When preparing your report, scan this page and save as a PDF file with a unique filename that 
identifies what it is. Include that PDF file with your report when you submit your lab report to 
Crowdmark and Turnitin using the appropriate links on eClass.  
4. Your deadline to submit your lab 3 report is 7 days from today’s date at the same time as your lab 
sessions normally end (1:00 pm, 5:30 pm or 10:00 pm). Late penalties of 10% per day or part thereof 
will apply. Do not procrastinate.  
 
TA’s signature of acknowledgment: ______________ 

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