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Filter Medium (Characteristics of filter medium)
In case of cake filtration, the choice of a filter medium is often the most important
consideration in assuring satisfactory operation of a filter. The filter medium in any
filter must meet the following requirements
1. Itshould retain the solids to be filtered, giving a reasonably clear filtrate
Unit Operations-1 5.0 Filtration and Sedimentation
2. It should not plug or blind (low rate of entrapment of solids within its interstices).
3. Itshould be mechanically strong to withstand the process conditions.
4. It should be resistant to the corrosive action of fluid.
5, It should offer as little resistance as possible to the flow of filtrate.
6. Itshould possess ability to discharge cake easily and cleanly =
7. Itshould have acceptable resistance to mechanical wear.
8. Itshould be cheap.
9, Ishould have long life.
In cake filtration, the filter medium is frequently a textile fabric.
Canvas cloth, woolen cloth, metal cloth of monel or stainless steel, glass cloth and
synthetic fibre cloth - nylon, polypropylene, etc., are commonly used as filter media
in industrial filtration practice depending upon the process conditions.
For an alkaline slurry, nylon cloths are used while for an acidic slurry, polypropylene
cloths are used as a filter medium,
Filter Aids
Filtration of slurties containing very finely divided solids or slimy, deformable floes
is very difficult due to formation of a dense, impermeable cake that quickly plug the
filter media. In such cases the porosity of the cake must be increased to allow passage
of the filtrate at a reasonable rate. This is achieved by adding a filter aid to the slurry
before filtration
A filter aid is a granular or fibrous material which packs to form a bed of very high
voidage. Because of this, they are capable of increasing the porosity of the filter cake.
A filter aid should be of fow bulk density, should be porous, should be capable of
forming a porous cake, and must be chemically inert to the filtrate.
The commercial filter aids are diatomaceous earth - almost pure silica prepared from
deposits of diatom (marine organisms) skeletons, expanded pearlite, and asbestos
fibres. The filter aids are used for sludges that are difficult to filter and the use of
filter aids is normally restricted to filtration technique in which the filtrate is valuable
and the cake is the waste product.
‘Methods of using filter aids
(i)_ adding a filter aid to the slurry before filtration, and
(i) precoating, i.c., by depositing a layer of a filter aid on the filter medium before
filtration.
Scanned with CamScannerUnit Operations-1 51 Filtration and Sedimentation
© Precoats prevent gelatinous solids from plugging the filter medium and give a clear
filtrate. The precoat is a part of the medium rather than that of the cake. When the
filter aid is directly added to the slurry before filtration, the presence of it increas
the porosity of the sludge, decreases its compressibility and reduces the resistance of
cake during the filtration operation,
FACTORS AFFECTING RATE OF FILTRATION
The rate at which the filtrate is obtained in a filtration operation, i.e., the rate of filtration
depends upon the following factors
1. Pressure drop across the feed inlet and far side of the filter medium.
Area of the filtering surface.
Viscosity of the filtrate,
Resistance of the filter medium and initial layers of cake.
Resistance of the filter cake.
The rate of filtr directly proportional to the pressure difference across a filter
medium. Therefore, higher the pressure difference across a filter medium, higher will
be the rate of filtration.
© The rate of filtration is directly proportional to the square of the area of a filtering
surface. Therefore, higher the area of a filtering surface, higher will be the rate of
filtration,
© The rate of filtration is inversely proportional to the viscosity of the filtrate.
Therefore, higher the viscosity of the filtrate, lower will be the rate of filtration.
© The rate of filtration is inversely proportional to the resistance of a cake or filter
medium. Therefore, higher the resistance of a cake or filter medium, lower will be
the rate of filtration.
TYPES OF FILTRATION EQUIPMENTS
(a) Filters are generally divided into two major groups based on the function or goal of
filtration (.e., based on whether to produce a cake or sparkling liquid).
(i) Cake filters.
(ii) Clari
*© Filters that retain appreciable quantities of filtered solids on the surface of the filter
medium are referred to as cake filters.
eae
ing filters,
© Filters that remove small amounts of solids to produce sparkling clear liquids are
referred to as clarifying filters or deep bed filters. These filters are commonly
employed in water treatment.
Filters may be classified according to the method of operation or operating cycle as
(i) Batch filters
(ii) Continuous filters
(c) Filters may be classified based on the driving force used for separa
pressure, vacuum or centrifugal.
(b)
ion, &.g., gravity,
Scanned with CamScannerUnit Operations-1 5.12 Filtration and Sedimentation
In filtration operation, the filtrate is forced to flow through a filter medium by virtue
of a pressure difference across the medium. The pressure difference may be created
by gravity, superatmospheric pressure on the upstream of the filter medium, sub-
atmospheric pressure on the downstream of the filter medium or centrifugal force
across the medium. Therefore, filters may be classified as
(i) gravity filters, Gi) pressure filters,
(iii) vacuum filters, (iv) centrifugal filters.
Industrial cake filters are usually classified as follows
1.
Batch (discontinuous) pressure filters
e.g. filter press - plate and frame press, pressure leaf filters.
Continuous pressure filters
e.g., pressure filter-thickener, continuous rotary pressure filters.
Batch vacuum filters
e.g. vacuum nutsches, vacuum leaf filters.
Continuous vacuum filters
e.g., rotary drum filters, vacuum precoat filters.
Centrifugal filters (batch and continuous)
e.g., suspended basket centrifuge - top driven or bottom driven, continuous filtering
centrifugals.
The most important cake filters which will be referred to are : plate and frame filter
press, rotary drum filter, and basket centrifuge
In many cases, in the chemical industry, it is the solids that are wanted.
‘The factors to be considered while selecting equipment for filtration and operating
conditions are :
1. Properties of the fluid such as vi
reactivity,
ity, density and corrosiveness/chemical
2. Nature of the solid which includes particle size, size distribution, particle shape
and packing characteristics of solid particles.
3. Concentration of solids in slurry, ie., feed slurry concentration.
4. Quantity of slurry to be handled and its value.
5. Valuable product of operation.
6. Necessity of washing the solids.
7. Initial investment.
8. Necessity of pretreatment of the slurry for ease in filtration.
9. Cost of labour and power.
Primary Filter - Sand Filters
Sand filters (clarifying filters) are used for water treatment and water purification.
The medium of this filter is sand of varying grades. When we have to remove taste
and odour, the sand filter may include a layer of activated carbon. There are several
kinds of sand filters : rapid (gravity) sand filters, slow sand filters, pressure sand
filters and upflow sand filters.
Scanned with CamScanneree jt zhe betes tone
Plate and Frame Filter Press
Construction :
© It consists of plates and frames arranged alternately and supported on a pair of rails.
The plate is a solid piece having a ribbed surface. The frame is hollow and provides
the space for the filter cake, The altemate arrangement of plates and frames results in
the formation of chambers. The plates and frames are square or rectangular in shape
and can be made of cast iron, stainless steel, nickel, aluminium, monel, hard rubber
or plastics (polypropylene). Coated materials are also used (rubber or lead or epoxy
resin covered).
Feed Channel
t Filter cloth
Lower part of plate
|
Open channel for
Fig. 5.4 : Plate and frame filter press (sectional view)
Scanned with CamScannerFeed inlet
Hollow
Frame Plate
Fig. 5.5 : Plate and frame
¢ Filtercloths are placed over each plate to cover the plate surface on both sides so that
hollow frame is separated from the plate by the filter cloth. The plates and frames
have circular holes on the comers for feed and discharge as shown in Fig. 5.5. The
filter cloths are also having holes that match the holes on the plates and frames. The
filter cloths themselves act as gaskets.
* When the press is closed by means of a hand screw or hydraulically, a continuous
channel is formed along the whole length of the press out of the corner holes in the
plates, cloths, and frames. The frames have openings in the interior from the comer
holes so that the slurry channel opens into the interior of frame (i.e., in the chamber
formed between each pair of successive plates). At the bottom of the plates, holes are
cored which connect the faces of the plates to the outlet cocks.
Working :
© Slurry to be filtered is pumped through the feed channel. It runs into the chambers
formed and fills the chamber completely (i.e., frames). As the feed pump continues to
supply the slurry to be filtered, the pressure goes on increasing. Because of this, the
filtrate passes through the cloth, runs down the faces of plates and finally leaves the
filter through discharge cocks. (Fig. 5.4). The solids are deposited on the filter cloth.
The two cakes are formed simultaneously in each chamber and these join when the
frame is full and no more slurry can enter into it. The press is then said to be jammed.
Wash liquid may be introduced in the press to remove soluble impurities from the
solids and the cake is then blown with air to remove the residual liquid from it. The
press is then dismantled, and the cake of solids scrapped off from each plate.
© In simple washing, the wash liquor is introduced through the feed channel and leaves
the filter through the outlet cocks (i.e., it follows the same path as the slurry and
filtrate). It is suited when the cake is uniform and permeable.
* In open discharge type, the filtrate is discharged through cocks into an open launder,
so that the filtrate from each plate can be inspected and any plate can be isolated
Scanned with CamScannerfrom the service by shutting off the cock if it is not giving a clear filtrate. Hence, it is
used when absolutely clear filtrate is required. In closed discharge, the filtrate
channel runs the entire length of press into a discharge pipe at one end. The closed
technique is used when toxic or volatile materials are to be filtered.
In many presses, arrangement is done for steam heating. Due to this, the viscosity of
the filtrate is reduced and a higher rate of filtration is achieved.
These units are made in plate sizes ranging from 100 x 100 mm to 1500 x 1750 mm.
Operating pressures upto 700 kPa are common. The press may be operated at
pressure upto 7 MPa by using a suitable material of construction.
Washing Press
Washing of the precipitate is more easy in the plate and frame press than in the
chamber press. Two methods of washing are simple washing and thorough washing.
The simple washing is ineffective when the frame is completely full. In thorough
washing, which is a more effective technique, the wash liquor is admitted through a
separate channel behind the filter cloth on alternate plates. These plates are called
washing plates. The wash liquor thus passes through the entire thickness of the cake
and is discharged through the drain cocks.
Wash inlet Three buttons ‘Two buttons
ez
Feed inlet
Washing plate
Non-washing plate
Fig. 5.6 : Plates and frames of washing press
Scanned with CamScanner&. § & & & &§ §, §
3@ 52 S2 Se 32 Se 32 32
BG Bg 2a Ba Bg Ba BE Ba
ak af af 28 af oa af 28
| |
Wash water inlet passage/wash channel
a
:
0
,
Filter cloth Filter cloth [ :
=| =z
cod
Cake Cake Cake Cake 4, Cake
my.
LILI
Ge
Closed ohn Closed Open
Fig. 5.7 : Section through Washing Press (Washing cycle)
L
feos
[
The plates and frames of the washing press are shown in Fig. 5.6. For ease in
identification and quick proper assembling the press, it is common practice to cast
buttons on the sides of plates and frames. The non-washing plate is having one
button, the frame is having two buttons, and the washing plate is having three
buttons. The press is assembled in such a way as to give the order of plate and frame
in the form 1-2-3 -2~1...... etc. (See Fig. 5.7).
The various channels lead to connections on the fixed head. During the filtration run,
a wash channel is closed by a valve on the head of the press. Filtration is carried out
as in the non-washing plate and frame press described earlier. When the frames are
filled (by solids retained on filter cloths), the feed channel is closed, the outlet cocks
on all three button plates are closed, and wash liquor is introduced into a wash
channel.
As the wash channel has cored openings connecting with both faces of three botton
plates, wash liquid enters between the plate and the cloth on all these plates. The
wash liquid passes through the cake, down the faces of one botton plates, and out
through the cocks on the one button plates as cocks on one bottom plates are open
and that on three botton plates are closed.
Scanned with CamScannerAfter washing, the excess liquid from the cake is removed by compressed air for easy
discharge of the cake,
In this pr
the filtrate (during filtration) p:
added resistance of the cake ca
faces of three botton plates
s, the wash liquid passes through the whole thickness of the cake whereas
s through only half the thickness of cake. The
the liquid to distribute itself uniformly over the
and thus, to pass through the cake uniformly.
Recessed Plate or Chamber Press :
Itis similar to the plate and frame filter press except that the use of frames is avoided
by recessing the ribbed surface of the plates. The filter chambers are formed in
recesses between the successive plates. The fed is generally located in the centre of
the plate. Filter cloth on the recessed surface of each side of the plate is sealed around
the feed opening by two cloths sewn together at the hole or by clip nuts. The slurry
containing relatively large solid particles can be easily handled in this press as there
are no chances of blocking the feed channels. When the slurry is pumped in the press,
it will fill all the opening between the cloths and afterwards as pumping continu
the filtrate passes through the cloths, runs down the ribbed surface of the plates and
finally leaves through the outlets provided on each plate. This press
washing of the cake.
is not adopted for
Recessed
plate
Slurry
Fig, 5.8 : Recessed plate and chamber press
The plate and frame press is widely used, particularly when the cake is valuable
and relatively small in quantity. It can handle slimy material.
Scanned with CamScannerAdvantages of Plate and Frame press :
8.
TAYE
Simple in construction.
Low first cost.
Maintenance cost is low.
It provides a large filtering area per unit area of floor space occupied.
High operating pressures are easily developed.
It is possible to alter the capacity.
The majority of joints are external, so leakage is easily detected.
Flexibility.
Disadvantages of Plate and Frame press :
1.
2.
3.
4.
5
Labour requirement is very high.
Discontinuous in operation. Periodic manual dismantling results in high wear on the
cloths. So the filter cloth life is relatively short.
Not suitable for high throughputs.
Presses frequently drip and leak, making housekeeping in the area a problem.
Washing of cake is likely to be imperfect.
Scanned with CamScannerRotary Drum Filter
* A rotary drum filter is the most common type of continuous vacuum filter. In this
filter filtration, washing, partial drying and discharge of cake all take place
automatically.
Construction :
* A rotary drum filter is shown in Fig. 5.9 (B). It consists essentially of a cylindrical
sheet metal drum mounted horizontally. It may be from 50 to 400 cm in diameter
and 50 to 800 cm long.
¢ — The outer surface of the drum is formed of perforated plate. A filter medium such as
canvas covers the outer surface of the drum which turns at 0.1 to 2 r/min in an
agitated slurry trough, Inside the outer drum, there is a smaller drum with a solid
surface.
¢ The annular space between the two drums is divided into number of
compartments/sectors by radial partitions and separate connection is made between
the compartments and a special type of rotary valve. As the drum rotates, vacuum
and air are alternately applied to each compartment.
¢ Apart from cast iron, the other materials of construction of this filter include
stainless steel, titanium, plastics such as PVC, etc. These materials give much
improved corrosion res for many slurries.
Wash spray ——+2%@
Cloth covered
outer drum
Slurry trough
Fig. 5.9 (B) : Rotary drum filter
Scanned with CamScannerWorking :
Wash water —>4
The drum is immersed to the desired depth in the slurry which is mildly agitated to
prevent the settling of the solids. Vacuum is then applied to the portion of drum
which is submerged in the slurry through the rotary valve. Because of this, the liquid
(filtrate) is sucked into the compartment and solids get deposited on the cloth to form
a cake of the desired thickness which can be regulated by adjusting the speed of the
drum. With higher speeds, thinner cake will be formed and consequently, high rate of
filtration will be achieved. The filtrate from the compartment then goes to a filtrate
collecting tank through the internal pipe and rotary valve.
As the portion of the drum on which the cake is formed comes out of the slurry, the
is washed by spraying wash liquid. The wash liquid leaves the filter through the
rotary valve and is collected separately in a separate tank. After washing, the cake
enters into a drying zone as the drum rotates where the cake is partially dried by
sucking air through the cake of solids, Afier the cake of solids has been sucked as dry
as possible, vacuum is cut off and the cake is removed by scrapping it off using a
adjustable doctor's knife. A little air is blown in under the cloth to aid the removal of
the cake. Once the cake is removed from the drum sector, it re-enters the slurry and
the cycle is repeated.
Wash sprays
Air connection
Continuous rotary fitter
‘Cake
Moisture trap.
Dry vacuum
pump
Vacuum
receivers.
Barometric seal
Fig. 5.10 : Flow sheet for continuous vacuum filtration
Scanned with CamScannerUsually, one-third of the cycle is used for filtration, one-half for washing and air
drying and one-sixth for cake removal
Advantages of Rotary drum filter :
1.
2.
It is entirely automatic in action and thus the man-power requirement is very low.
With cake consisting of coarse solids, it is possible to remove most of the liquid
from the cake before discharging
It has a large capacity for its size. Therefore, it is widely used for the filtration of
large quantities of free filtering material.
By changing the speed, it is possible to built up cakes of varying thickness. With
fine solids, the thickness of cake is small and is large with coarse solids.
Disadvantages of Rotary drum filter :
1.
2.
4.
The maximum available pressure difference is limited to less than one atmosphere.
As it being a vacuum filter, a difficulty is encountered in the filtration of hot liquids
due to their tendency to boil.
It cannot be employed for materials forming relatively impermeable cakes or cakes
that cannot be easily removed from cloth
Initial cost of the filter and vacuum equipment is high.
|CENTRIFUGAL FILTRATION
In case of slurries containing coarse granular or crystalline solids forming a porous
cake, the filtration operation can be carried by using centrifugal force rather than the
pressure force,
Centrifugal filters can be operated batchwise or in a continuous fashion. In these
filters, the slurry is fed centrally to a rotating basket. The perforations in the walls of
the basket are covered by a filter medium. The slurry is forced against the basket
sides by pressure resulting from the centrifugal action, ie., by centrifugal force. The
liquor passes through the filter medium and the solids are retained by the medium.
After building the cake to a predecided thickness, the feed is stopped and the cake of
solids is spun for a short period to remove residual liquid from the cake.
The principles of centrifugal separation and filtration are illustrated in Fig. 5.11.
In Fig. 5.11 (a), a stationary cylindrical bowl contains a slurry (liquid + particulate
solids of greater density than liquid), Since the bowl is not rotating, solids will settle
at the bottom with a horizontal liquid surface above the solids.
Scanned with CamScannerFig. 5.11 (b) shows that the bowl is rotating about its verti se, the
liquid and solids are acted upon by two forces — the gravity force acting downward
and the centrifugal force acting horizontally. Normally, the centrifugal force is very
large as compared to the gravity force and hence, the same may be neglected in
comparison with the centrifugal force. Under the action of the centrifugal force, the
solid particles are tightly pressed against the vertical bowl wall and the liquid layer
assume the equilibrium position with an almost vertical inner surface as shown in
Fig. 5.11 (b).
If the wall of the bowl is perforated and perforations are covered with a filter
medium such as a fine wire screen as shown in Fig. 5.11 (c), the liquid is free to
flow outward but the solids are not. Almost all the liquid quickly flows out of the
bowl, leaving behind the cake of filtered solids.
| Solids | Solids
fa) (b) (c)
Fig, 5.11 : Principles of centrifugal separation and filtration
(a) Bowl stationary, (b) Sedimentation in rotating imperforated bowl,
(c) Filtration in rotating perforated basket
Centrifugal Filters
A centrifuge or centrifugal is any rotating machine that utilises a centrifugal force
for the separation of liquid from solids as well as for the separation of immiscible
liquids of different densities. The essential components of a centrifuge machine
are:
1. a rotor or bowl! in which centrifugal force is applied to the contents of bowl,
a drive shaft,
»
a drive mechanism e.g. electric motor,
a frame for support, and align these and
= >»
acasing
Scanned with CamScannerCentrifugal Filters
Solids that form a porous cake can be separated from liquids in a filtering
centrifuge. Slurry is fed to a rotating basket having a slotted or perforated wall
covered with a filter medium such as canvas or metal cloth. Pressure resulting
from the centrifugal action forces the liquor through the filter medium, leaving
the solids behind. If the feed to the basket is then shut off and the cake of solids
spun fora short time, much of the residual liquid in the cake drains off the particles,
leaving the solids much “drier” than those from a filter press or vacuum filter.
When the filtered material must subsequently be dried by thermal means, consider-
able savings may result from the use of a centrifuge.
The main types of filtering centrifuges are suspended batch machines, which
are discontinuous in their operation; automatic short-cycle batch machines; and
continuous conveyor centrifuges. In suspended centrufuges the filter media are
canvas or other fabric or woven metal cloth. In automatic machines fine metal
screens are used; in conveyor centrifuges the filter medium is usually the slotted
wall of the basket itself.
SUSPENDED BATCH CENTRIFUGES. A common type of batch centrifuge in
industrial processing is the top-suspended centrifuge shown in Fig. 30.11. The
perforated baskets range from 750 to 1200 mm (30 to 48 in.) in diameter and from
18 to 30 in deep and turn at speeds between 600 and 1800 r/min. The basket is
held at the lower end of a free-swinging vertical shaft driven from above. A filter
medium lines the perforated wall of the basket. Feed slurry enters the rotating
basket through an inlet pipe or chute, Liquor drains through the filter medium
into the casing and out a discharge pipe: the solids form a cake 50 to 150mm
(2 to 6 in) thick inside the basket. Wash liquid may be sprayed through the solids
to remove soluble material. The cake is then spun as dry as possible, sometimes
a higher speed than during the loading and washing steps. The motor is shut
fe and the basket nearly stopped by means of a brake. With the basket slowly
Scanned with CamScannerMotor
Feed
inlet
Wash
valet
cesing +
“Solids
coke
Perforoted
hoor? “bathe!
FIGURE 30.11
Top-suspended basket centrifuge.
turning, at perhaps 30 to 50 r/min, the solids are discharged by cutting them out
with an unloader knife, which peels the cake off the filter medium and drops it
through an opening in the basket floor. The filter medium is rinsed clean, the
motor turned on, and the cycle repeated.
Top-suspended centrifuges are used extensively in sugar refining, where they
operate on short cycles of 2 to 3min per load and produce up to 5 ton/h of
crystals per machine. Automatic controls are often provided for some or all of the
steps in the cycle. In most processes where large tonnages of crystals are separated,
however, other automatic or continuous conveyor centrifuges are used.
Another type of batch centrifuge is driven from the bottom, with the drive
motor, basket, and casing all suspended from vertical legs mounted on a base
Scanned with CamScannerMECHANICAL SEPARATIONS 1013
plate. Solids are unloaded by hand through the top of the casing or plowed out
through openings in the floor of the basket as in top-suspended machines. Except
in sugar refining, suspended centrifuges usually operate on cycles of 10 to 30 min
per load, discharging solids at a rate of 300 to 1800 kg/h (700 to 4000 Ib/h).
AUTOMATIC BATCH CENTRIFUGES. A short-cycle automatic batch centrifuge is
Scanned with CamScanner‘SOLVED EXAMPLES)
cample 5.1 : For a sludge filtered in a washing plate and frame the filtration equation
V = Kr holds good, where Vis the volume of the filtrate obtained in time 1. When the
pressure is constant, 30 mt of filtrate is obtained in 10 h.
(i) Calculate the washing time if 3 m’ of wash water is forced to the cake at the end of
filtration.
(ii) the fitering arealsurface is doubled keeping all other things constant, how long
would it take to obtain 30 m’ of filtrate ?
Given : The rate of washing is one-fourth the final rate of filtration.
Solution : The filtration equation provided/given for a constant pressure filtration is
V= Kt
where V is the volume ofthe filtrate obtained in time t
Differentiating the above equation, we get
wav = Kat
wlk
anv
533 Filtration and Sedimentation
Given
‘The final rate of filtration is given by
(avy _ K __ 90. ,
(Ge) = av =zaa5n 1S
Given: Rate of washing = 3 (Final rate of filtration)
fx (15) = 0375 mh
0m
Volume of wash water
(Volume of wash water user
Rate of washing = “Washing ime
Volume of wash water 3, :
Washing time Rate of washing "03757 84 ‘Ans. (i)
(i). Filtering surface is doubled,
We know ; Rate of filtration 2 A*
Rate = A\
Rate = cA”
(Rate, (Rate ithe rate with surface Ay
(Rate), = © A2 co with fice Ap
Given:
me of filtrate
Time
(Rate),
Rate);
Rate);
(Rate)
A 5
XGayre 12 mh
We have to find the time required to obtain 30 m' filtrate when the surface is doubled
eo Ans. (i)
Scanned with CamScanner
Volume of fitae
Time required = Yume or TtvateExample 5.2 : A filter press is used to filter a sludge forming a nonuniform compressible
cake. Ata constant pressure difference, 6000 | of filtrate is obtained in 1 h. Washing is done
with 1200 | of water, it proceeds exacily as filtration. The filtrate has the same properties as
the wash water. Neglecting the resistance of filter cloth, calculate the washing time requit
Given : Rate of washing = I/4 (final rate of filtration) for a filter press.
Solution : For a constant rate filtration, neglecting the cloth resistance, we have
dt
av = KV
which on integration gives
v
t= Ky
2 K. = 2vV?
Given :t=1h=60min ... V=6000/
2x40 60
Ke = (6Q00)2 = 3:33 x 10 min/?
IV
Wehave: wl,
The final rate of filtration is
(4) Ry, there V;= 6000 1
dt), = KVjr Where Vi=
1
= 333 x 10x 6000 = 50 min
1
Given: Rate of washing = q (final rate of filtration)
1
50 = 12.5 /min
Volume of wash water used = 1200/
Volume of wash water used
Washing time required
Volume of wash water 1200 .
Rate of washing = 50 = 24min + Ans.
Example 5.3 : A plate and frame filter press when filtering a sludge gave 8 m of filtrate
in 1800 s and 11 m’ of filtrate in 3600 s when filtration was stopped. Calculate the wahsing
time if 3 m’ of wash water is used to wash the cake. Neglect the resistance of a filter cloth
and assume a constant pressure filtration.
Given : Rate of washing = 1/4 (final rate of filtration)
Solution : For a constant pressure filtration, neglecting the filter cloth resistance, the
filtration equation is
Rate of washing =
Washing time =
dt
av = KV
wt
dt ~ KV
Scanned with CamScannertime if 3 m’ of wash water is used to wash the cake, Neglect the resistance of a filter cloth
and assume a constant pressure filtration.
Given : Rate of washing = 1/4 (final rate of filtration)
Solution : For a constant pressure filtration, neglecting the filter cloth resistance, the
filtration equation is
ae
av = KV
dv lt
dt ~ KV
Unit Operations-| 5.35 Filtration and Sedimentation
Integrating, we get
as
K.
2t
Ko =
Let us find K,.
2x 1800
Given: V = 8m’ and t= 1800s, K.= Ey = 56.25 s/im®
The filtration was complete at t = 3600 s during which 11 m' of the filtrate was
collected/obtained. Thus, the final rate of filtration is given by
dv) __1_ 3
(©) gh. vettm
1
~—! _ _ py ns
= 5625xi1 = 162% 10 m/s
L
Given: Rate of washing = 3 [final rate of filtration]
1 7
= gX 1.62 x 10% = 4.04 x 10% m/s
Volume of wash water
Rate of washing = yp
Washing time
Washing ti Volume of wash water 3m
giime — Volumeof wash water _ __dm
ashing time Rate of washing 4.04 x10 m/s
= 7428s vac Ans,
Scanned with CamScanner