* Conicat Flach 5 Round bottom flak “Flot baton: ask 5 Peaeuring Tor © Gas Jaw ¥ Desiceater a Nu Ob Bn nfo 3. types Gloss ogparatus Preise opgneats Date 19.08 22 Pyge No, 01 Expert Ob 2 Misallancas ogpaatu, — lass Soparatus Beaker = 2 Cniaal Psk = ‘fat batn Faa= Yo Shady the commen. uted spgaratus in the artery The tuner used ofgamtac in the labaasiry have been cased TE is used te cates quis Tb watt te timle tee sans is used fp carry out restos, ‘uFlot bute fiosk~ Th ul fe cast data water Measuring Tv — eis ued fo measure the velums of pots Tks sed to collet the gases 1k ia waad te neep the abeartn of mgstre Lor i dry cnt Janets to sidF Waten goss 9 Test tuoe “Te Fane aes oa vy Guass tute 2 Feeeinn tae Pugeno at No OL seater ass = Th is used =| Goer the tater ithe substances Test ie Th used carry out chemad tests sen This and fo fie re sito ‘eivanser the clsienlqa acs rok = 1 used 40 br fh sett, lous tube = DLs used to ad selston. drop uit Rovesiain apparatas sLChina dh — Tie used to eimporte caluent daring crystainten Ror e= Bie used to provde. waite background 10 coger cake change dusting rahen, Msc pparian s.Aloetee sheet = This cae to hap ot agparabs 2 Syatsia Tie used tans a he sabstarces fram the ‘te 2 fur of tangs Wi uses to a hea agra,1 taaates Sheet 1 Gene ‘far af tenas “A Test sake pots ry No Ob a Teot tube alder — Tet habe star ~ «fied stand ne gauze Hi used oid tel tube ring eating reas We uced te hosp the feat tubes. a ene place. 6 utd fe support te ogparane during ating procs Ihe wens To beget unerm haog prod apparatus from tleExperiment - 02 Rim — Th bunsen burner liquefied petroleum gas (Lea) is used os. a fuel. Tt is primarily o mixture of propane and outone. — Parts of Burner — \.Base ~ It is a “heavy metal block having 0 Sitle tube Through the side. _ — tube gas enters in the base. Then gas escapes Hage the _ nozzle ond enters the burner tube. | 4 2.Burner tube — It is a “eyjindatcal metal ube Th consists of ‘isa air a holes ot tne bottom. __ 3. Pir “vegulatnr— = This a metal vying... On shcning air: aegulnter around “ “the burner _ —tulbs, cir tholts con lor opened or closed. This regulates tne t _ Supply of air togas . The side tutor of burner is connected 4o _ _ The gastop by means of a rubhir tubs. The oir holes are _ closed ond ges top is opened. The tourer is lighted with o an burning moich stick ond the Following obseruations are — mode. —« —lninen the burner is lighted by completely closing the oir holes) & lumincus flame is cbtainer ond ushen the ol holes are open, non luminous flame is obtained, i-Luminous Flame — Tt is bright yellow coluwred light having soot. This flame —gjves_ligit lout less heat. Hence i \s_net_used for eacherT > ae : f | k Ly te ns 2 rar FS oe repute eae ae a 1, » SS uw Se Fg Qunsen Burner \ Bais, Be | a oe - Speirs \ Shae yy do tie he et mwaragel | wpe) MV Dav cone ena a fame bu fi tito iare of Grduent at a “comin rom bra fig, Zones oF Flame of Bunsen Burney jy + m2! gem ome or Passo oF heateg parse, - Nen-harinous fame = Nen-tumnnous. ham cans of thru eténet poe, PAPE nner sone itis pot conses of unbart ghs ana i eae eat Eire, 08 prdues tess hea TR tumness onsets sone this grt 8h tinmaten of - spetths eae dees er ras [Notas ate sme= ns arte sae neo Seat Garin Hint. yess Tatum ted ant -teharquut gate nape he, Be ‘8 ied Sor htohing purge Note — — - ‘The 608 Gam may oe cared by 209 anh raiore ice io sand oe ‘ean ps og, frie SueDate fi aye N 03 Page No 06 U — Experiment —05 Aim - Construction ef Leash bolle. for Construction of usash beltle tht folowing fas usork Is +o be dane. \ Cutting @ glass tube A deep Scotch is made on o glasstubs vith triangulon file of the vequired place. The tube is _ held _usith both the bonds by Keeping thumbs on either side of the suatch but in thi oppasite direction. Thin the force is applied to it, 10. break — Tne gloss tubs. po 2. Bending of gjass +ube— The port. of 0 giass tube which Is to be_bent is Meattd ino nen-luminous flame by holding _ the tobe in both the hands ond votating swt, _ so That all sides ore Weoted unifoymiy. When the glass tube becomes soft, if is vemoved 9nd glouily bent iv the desired shape. Then it_is cooled boy keeping it on asbestos sheet. aMaking a jet tube te ogiass tube— Heat inthe middle of the glass tube dust Uke above Hil It becomes soft. Then the two ends of glass tube aye pulled out quicaty and carefully The glass Ault is cooltd anc cur in Ane Wridale 19 get two tubes Hoving © nozzle Teacher's SignahreKo caest Ns — sa a ey ff ty “ous “Cork boring — 9 cork horse ofa reqared aise & pact an — the Gece task of a Bart core anc presen {by vetating, io ancuusse direction. Tht cork. berer pierce thrauys Ma dock curing svat Lore het. 7 fe cara ue moet | [Construction of wasn battle — She ue for canst wasn ba Sm At an fn te ton. $i Hts ata ca err teehee tnt elk 0 Shar ere bend neh oe ca nee a tera et ate sing oer ore eras thon a veer + eg en te Cae Wan sash batt is 40 te ub aie % inen Mca, “the serall_ott tube soater Comes cat tncaugh ne it sy |S usta br vonsting opparatic,.th Cxperiment 04 aH ins Aim — Different methods of filtaration and heating of Fitreration — * Principe Seperation of saids fron Uquids ly passing thrmudy porous moakerial Filteration by ordinary method — * Apparatus ~ funnel )oeoker , glass rod , fitter paper + Procedure — fad Me filter paper twice and divide the foudings by Keeping % folds on one sie and one foid on other side Place tru filter paper indie funnel dnd wel if vaith fader. Keep the funnel on dandy pour the solution 10 be Ailteved into the furnst along ‘Wt ginss vod, «Example — Cocos in woler, Filtration using suction — “Appovotus — Buckner funng , Suction pump, beakin ,qliss rod , filter poper | * Procedure — filtevation is Carried out kay, Under reduced pressure using suction mM 1G created oyOfDate Page No. 10 _ Experiment - 05.0. Aim — Purification of benzoic acid and copper eaiphate (Cu50u) Princip Crystouaniion is one of the echnques foctru purifica -bion of inapuns compounds. In thir meted impute Compounds ore dissolved in suitobbi. solvents. On 4 Evaporation of the, _soluint pure crystals Segara a Chewwicals = Ousoy , Bursid Oud» Alcona, voosen - “Provedure- ee + Grystouization of custy— > = ~Tmpurs Sample 9 0.804 is tokas_ and solved in minimum quantity of water to obtain soturctad Solution, — ~The about solution ib Filtered and transferred into china dish. The Aleved solution i heated to concentvate solution. ~The Solution is cnoled tui the fine ond purr crystil of Cally Separated out ont drud __ _ Crystallization | of Bemac oud — a — Dp Sompi_of Benge ocd ia tokun_in ear tube, “panna quantity of Oltehst U odad, 7 Teacher's Signature :Date WV Page No | faspt. No. “The Oboe dest tube is Kept in wwotkn wath th disse the i Somp\e. = — —Hot_solution & filtered on G_wotdt gloss ond coolud th loenzoie acid . Tar purity tbfain purse and fine aystal of [oF sampls uu thecked by duterfmining Tha rmatting point. I — - } = = + —= = Teacher » SignatureDate 05 6 Page No, 1% Experiment — 05. b Rim — Determination of metting paint of sovd a Theory - Melting point of & Substance u tha tenperotuar oF wWidh th Solid stake of substance oegins te Change into liquid state, Material — Tele's ‘se armani Copyidoy tube, Seep frocedure — _ ~ Stok one end of thu_capitlaxy tube. b by heating _ ~ Crush and fiu the Sample ints copitiory tube wp to Lom ~Tog the Copilory tube to the thumenster such thot the | lower 2nd of capillary be ond the truamomctn bulb ort of 4ht some level. = — | ~ Dip the thermometer tn tin Niquid paraffin such ‘that the Wowser end of copilary is compulsory /completeny inside the paraffin. _ Heat the side arm of the Thiee's tube Lott o loo flame and hott down the tempevotur Where the solid stants mutting. — Teacher's SignatureDB somo * Bat ES. neg os Bes ‘Experiment ~ 95 e 4m — Detinionte Wey Fee ie agane Cingirt arya pet ota uu fimetise oF wien st change ts peas “I Biting poids bt antncy tenga ot eth Wy 8 gs ry a Pomp hia precios Pres Date Dem Sea ey \ qua ligt Frocedure — Sch Tat lower tad hs ‘ibe and hunmemeer bata of tu sams ag aflary tube by heating nd dived on tha Ud taken fo tak pen ube Meat tra stl arm of Tes tube sit aw Slama and ade (een te temperatia, fees Babe sas mg try ‘rem i apilony ube 1 faa ts open Biting pnt of cepted wi Sroerimene = 06 Shen test me gen sa ana erm gng ma canctbur? sical 51 dng bets (nur enous fppeonan = Crypt. Sey Semen wsonee ten oF Hor = Criptaton. ecuaes Lith eeutinn of uation, 4 - ear fame \Diteicaten oF aud, toasts Expense ——Woservaton Tiernan 4 Thin oF AL wejadh No Change Wh Seite BEING of Suigal & aim st anh contaate *taj tomes 18,0 Redan erown gas \s trate Un sane pet all pe of saat evn seb eater its on tain counenaToRy, Test “Cres ing 1, Sait Brow og erred gH Nita lon U Conf ‘sun aad te anton oF Ant 4 Ht. ene prepared 0, « oad AM wit ne aged tent fat[ apt. No. Pase No 95 Tadentification of basic radicots — ~ Inference Experiment Observation “Add ILHG the Formation gf white Group T radical Is present att soution precipitate (ead) CONFIRMATORY “TEST Add potassiuen iodide Formosion oF yw 4o the Sakt Solution. pvecipitade. lead ian is confirmed Report + The tests confirmid thu presence of (03) Nitrate onion and (Pb™) lead cation in ‘the given Salt ‘Resutt : The guin salt is led Nitrate “PoLNO,)v Date Pape No, '@ Experiment ~ 0b. 1 Aim— To fest given eait and identify the constituent adi coy/ions. Pretmuriovy tests ——— — aaa _ Colour — (olouriess______ ~ ~ Appearance — Crystowuar — _ Solubility — Soluble in_water_ Action of heat — Sour Sullimes sith evolunnon, of, gas wlth. dense write furnes_wohen o guass rod dipped _in_Gone. HQ. is placed. ___—_—— — “pungent smeuing, Toentification of Acid radicals — _ oe __Byeviment —__|___Oloser ating _____—— _Inferere _~ Action of BL-HCL, added. isin BSc _Apsence_ef sulphide and ___to the Smt Sm. __ __— ~ Carloonctt—_ _= Chron chloride dst, Red - orange. “Nogturs car Chioride ions odL present. gery 05 i oddud to, Cvolwed, a __ so sol ind headed — _ voit cone: 4,0, — — ——____—_ - = = “coNAIeuATORY test __| - “Str. nitrate dest; add A cuvdy_tshite precipitate. Chloride ions ore olifute NOW 49 Soltis formed __ lonfirnae.cl Sol. Gnd ft add a Ag(NO3), —t eo —_—_— Teacher's SignahreDate Expt. No Page No, 4 — Tatatification of Basie raatieats — —— : - - Lxpeviment Observation Trference Ada NaOH E] a Reddish brown préciptote LArannoniun ion 1S - duo dvops of 0 confirmed. _ 7 Nesslev's veagent +P Salt: Sot. Roport + The tests confirmed ths presence of (02) Cipiids ion & — bats Amorim Coton in “5 soit. :Experiment ~ 6.02 La il aes oe Aim— To test the given salt and identify the pensntves vadicols fions __ — Pretimanary tests —__ _ - giving _denst. vatatt_funuis with a goss red dipped Colour — Coldurless Approwana.= Crystauing _ Solubility - Setwele in usater Action of heat= Salt gubotinass —vsitl - avauuhon ot pungent smelting gas r amsifcotion of Add vasitals = — - OD Expevinaant Ob serwodken Tifexnce _> Action_oF di “Herd Brick efFernesenncs ef colour Corbonate lon iS _confirmad ___ HU U addi 4 solr less. en Solution — _Totwitification of tonsic vodienls— Experiment Odoserwotion Thtexence Add NogH ond fovmadion of “feddish-brown Ammonium jor Lb Neseier's reagunt 4 | —_ conticmed Sout fal- — — Teacher's Signature»Date xpt. No. Page No. 19 Report.» The tests confitm the Presence of (t0,") carnenou anton ang (NHS) famenium codion WHat given Gout Resuit + The given Salt is ammonium Corbenate (n1,), CosDate Experiment ~ 06-3 Pim — Te fest the gwen salt and identify The constituent vodscals) ions a - Preliminary tests— Colour = Colourless. _ —_—_— = Appeavanet - Deliquescent quid ans Soluble In wotty — Obstruation _Thference sulphidt 2 “experiment _ | > bution of 4). HU add No Change is observed. posers, of gil HU to sous Sst - ot, “tx bttom ot Byowwids ion maybe present __ coneeuatogy TEST "silver 1 vitvate test, Pode yulnews precipita. iL Bromide ion is ‘confirmed add Ag Ald, to Subt sok. forma. __|___— __Taentification of basic radicals — | _ | Experiment _______Ohsevvatinn: | Thferenae hdd AlaoH ¢40 formativn of ‘o redaph Ammenium ton fees dvops oF Messin brovn predpitate confirmud. Fengud 16 salt. Sot a ee Teacher's Signatur7 Date oN Page No. 2U yn. No. _— —— ~ . al epost Tests. confirm tnx presente oF (ar) reniat ortion. € (nn) Aumuoniun cotion, and Resutt : “The given catt is Am radian bromide (rye)ow t Experiment — 06-4 fim—"h test the quuun saut ond identify the constant vodsicass/ Aor. oe - Preuwwinary Tests — _ Colour — Colours - —— — — A Appearance - Crystoine __ Solubility — Sobubia. Log ter — __ Action of heat — Ne changed Le observed. — _ Tdentification of acid radicals — ___ Experiments_ Observations, Tnference Acton of ail-HU, _ Nb_change _olseyweo — Absence of Sulphide © add OL HU tothe sat > = _Creonote. solution. —— — — _ hdd_ail- HO. ots sail Truce voit, precipitate. | outphom ion UW confirmed ‘olution and then Bach 16 Formed ___| — ou — |. Tdentificanon of basic vadicals— =| Expevime nts _____Dbservations Tneerene *hdd NaOH +0 Solt sa No thangs is observed. — Absence 4 Aamonitee ion, Y than nessua's —_ - Foqgent , — Teocher's Signature »_Date Page No. 73 Aluminium ton UW conFrmad Aad NHysH and — frelatinous vont _ Nyt fo the salt precipita U formed _ Solution _ Report: The tests confirm thu presente of (50,7) sulphate anion and (ACT) Auaminium catenin the given Salt Dees: Ta fier sot «Aluminium Sulphate (ni, ts, . .Dat ap \v 0 5 Page No. 24 Experiment — 06-5 Aims "Ta test tt given salt and. ifentify. the constituent radicals fictmumary tests - — sana Colpurkigs - — Appeavance - Crystodine — “sowbiaty - Tnsolrbu in woter - Fionn test Gwassy gaeun on “prongs easing. - Taentitication of add vosicels —_ - | €xpyiment — Observation — - Tnferences “thon of dilute HU, Alo one w_sbserued. Absence 6f Sulphias a add ollt-HU te tht Covioonate __Sodt Souution. hdd dil: HU te tH “saat dni. 1 previ, Sulphots ion Sutin ond then is. formed — COMA _ Bau, 4p } ‘Luentification of basic vadicols— | Expeviment Observation Tnterences Add dil: Hu_tp tha No change observa fostnee of gioup t (Pe) _ SoSH Seyution Adah Ny ond Ai No caangp wustrusd Rosen of group lt (M7) 4D Salk Solution. Toodhor's SignaturDate Exp No Page No. 25. 4 “AMG HAS to The bee No change obserusd Absen. 6 ‘goup 1 (} itd, NIHyoe, sans _, Souation Ado Hy CL NHL OH, formation of volite Presence of your a OO; OC to gout Soe precipitate = CONFIRMATORY TEST Forassium chromate tat, Formation ef yolews Barium in is _cenfirmed 04d Ky Grd, 10 the precipitate | b0T Sou Report The test confivm ‘he presence of (S04) Suiphate anions and (Ba") Barium Cation in the gen gut - a, - Ihe given. sol is Sulphate Battun [Ba60.] a Teacher's SignatureDate a. Paye No 26 Experiment - 06.6 Aim- To test “tac. we salt and iaenrtinn the constituent wha- Prexinanony_ tals = oo _- __Colouw - Colousbtesg __fippenronee — Cysteine _ 7 _Govubility — Soluble in water —_ - _Taentifcation ri aad voctica— - _Expudmnent ___ Obsservatiens Thromu Action of d-Hu, add No change i Obseuned Absence a} sutpracs ait HU $0 Salt Sel and Conon ate, got aut HU 40 the Tinsouuble rt aap i Suipnatk_ ion UW loot ond Bat to’. formed. confirma } — - Taian f ac raat eo eqetimant — (tosvations ——Tatesence ha aH se salt No change ib observed. _— Absente of group elution. (pe) - 7d MiiyCt and NOH No Changs ts caste Apsent 4 goup T. hts out Sot A) Ada NHAC, NHJoH 4 formation ef vans Presence 94 fac) ions TS 4p ths Soll sol precipitate. —_ Teacher's Signatwe |Date Expt. No Page No. 24 CONFIRMATORY TESTS AO NacH fete — Thscuable vote precipita (Zn™*) Zine ona confine —saut- formed ced — [Report + The teats confirm, Hager of (S04) Suiphose anion. fp and Cn") Zine cation in the quen sais —Resuit: The given satt is zine supnate (2nso.) := Page No. ab [xy : Experiment ~ © & t i ducalt finn B Aut the gen solt anc identifying cia constituant 7% Poununay tat —- — Coour- Cloutas a forowronce Daliquaent fod — Seiutruhy - Sotample on_rookat —— - Al tut - Pate Fink 7 eo [Taentfcation ef Acid _vodicals— _ Thterence 4 Observosion —_— L Expeiementt — —— =— hction, ¢ dil: HU,add fo Change iu_ observed. Absence of sulpric. a ail HU tothe St _cOxbonate. = — Solution - eS _ A Carer Carts ait, Red Orang weopouns— Presence ¥ (atoridg. — ery in nd tp — 044 eM, — te Salt Solution _ haa ted tuith Cone: H$0y > Sil, nitrote tat, add A cud vor precipitate dil HAO, Ae Sout sof is formed Yy than odd AgNCy — —____— CONFIRMATORY Tests —— _ Chioride tong Us confirmed.Date — Lacitircation of Basic vacti cats Crpdonot Observations | Toferene = Anon ef il MeL atl No change is observed Absence of qioup (74) a HEL 49 Sand Sol: Hs UicH ond (Ao change 1 osenad Absence of cup (AU) WAU ty tes Sout | oo + - 1 Soustion. - Pad 5 fe th 166 No Change ia observed fan § goup Con’) m2 oo ihe ta), Cte |Alo change is obiuved been poop! the fof in a je i (eat! Ca Ad Any HOy te the hit pei om Presence “t a " _bovin Qe I ia) Report “Tha tate. tengiem ts. presence of (A) thbrias. avon and (Ma) Magnadium cation ints given Sat [Rew Th. gan salt Sant 8 maga outs Ca)Vou eta 7 Bret om a 20.5 m3 Date LN. oF j i ~ Gpsiownt or stonatea 84% nasto, tain ang + ateninction of strungih_of by titsting uth stanaaay Stlulin oF taco, Lana {Poporatus — Burttie Pipes, conias ‘haan Uh ete. cateuuntons 4 Nad + CO) + Ho 7 eevee Hose shann ne o> os - - - Naat, + ie Creicats— My.o, Ht, seta trong HO M2 procedure OO Ne —* Hye ot Mer 1s, F2EP9 Sf annyércus Ha\coy ib tonen nai woth gaa ana atone ¢ hae " lhaniftsrad 4 reaku contain soon ny oF distuss sister oom Welumatic flaak added te the lok Uptetan mi tuk Ah Soustion 1s transfeusd tp. i {Dishived wot 4 woth wat and ti filed with sedating " a sone ee Nan Meek = = te eae wna Taped ‘nto o eon conical fioak mg f os ss ite cas mets Pia von’ art repeated 1 concancent ausdingt ak canes -faua5 5 CSUR stung st Hui 4.0015