RPV Spec Bhatta
RPV Spec Bhatta
0 SCOPE
This specification establishes minimum requirements for low alloy steel forgings for Reactor Pressure
Vessel used for ISMR 235. The forgings are required to be made from fine grained, killed and vacuum
degassed low alloy steel equivalent to DIN 20MnMoNi55 grade with modified chemical composition.
The manufacturing process adopted shall ensure cleanliness of the highest order, isotropy of the
mechanical, chemical and metallurgical properties, superior fracture toughness and weldability. This
specification is appended with following Annexures (if any).
2.0 CONTENTS
The requirements of this Specification are presented under the following headings
Scope 1.0
Contents 2.0
Applicable Codes & Standards 3.0
Process of Manufacture 4.0
Chemical Composition 5.0
Heat Treatment 6.0
Mechanical Properties 7.0
Tests & Examinations 8.0
Non-Destructive Examination 9.0
Repairs 10.0
Procedures, Plans, Reports & Documentation 11.0
Quality Surveillance 12.0
Simulated Heat Treatment Cycle Fig.1
UT Scanning Direction for Shells Fig.2
UT Scanning Direction for Forged Bars Fig.3
UT Scanning Direction for Dished Ends Fig.4
UT Scanning Direction for forged plate & PWTC Fig.4A
Test Specimen Orientation Fig.5
Test Specimen for Impact Test Fig.6
Test Coupons Location for plate Fig.7
Material Sampling & Testing Plan-Plate Fig.8
Product Analysis & Metallurgical Examination-Plate Fig.9
Test Coupon Location-Ring Forgings Fig.10
Material Sampling & Testing Plan for STC-A- Ring Forging Fig.11
Material Sampling & Testing Plan for STC-B,C,D,E & F Fig.12
Test Coupons Location Dished End Forgings Fig.13
Material Sampling & Test Plan-Dished End Forgings Fig.14
Test Coupon Location- Nozzle Forgings Fig.15
Material Sampling & Test Plan - Nozzles Fig.16
Metallurgical Test Plan - Nozzles Fig.17
Extent of Tests-Plate Table-1
Extent of Tests- Shell & Ring Forgings Table-2
Extent of Tests-Primary Head & Dished End Forgings Table-3
Extent of Tests - Nozzles of ID upto 250 mm Table-4
Extent of Tests-Nozzles of ID over 250 mm Table-5
3.0 APPLICABLE CODES AND STANDARDS
The following codes and standards of the issue in effect on the date of issuing the tender document
shall form part of this specification. In case of conflict between the codes/standards listed below and
this specification, generally the specification will govern. The supplier must obtain necessary
clarification from the purchaser in such a case.
4.1 Melting:
The steel shall be made by basic electric process and shall be vacuum degassed to remove
objectionable gases particularly Hydrogen. Vacuum system should be of sufficient capacity to effect
a blank-off pressure which is sufficiently low for sufficiently long duration.
4.2 Discard:
Sufficient discard shall be made from each ingot to secure freedom from piping and excessive
segregation.
Grain size shall be measured as per ASTM-E-112 and shall be 6 or finer. The grain size and
microstructure shall be determined on a notched bar impact test specimen, obtained from simulated
Heat Treated Test Coupons. The examination shall be on the Longitudinal - Normal Section. In case
of determination on an untested side (e.g. Plate, Nozzles), these examinations shall be carried out
on the forging directly. The micrographs for assessing the microstructure shall be made at a
magnification allowing unambiguous assessment (as a rule: X 200).
The components shall be hot forged as close as practicable to their final finished shape and size by a
press or hammer of sufficient capacity to work the metal throughout its section. The forging ratios
shall not be less than 3. Tube sheet and primary head forgings, where overlay cladding is done, shall
be processed in such a way that the minimum segregation portion shall be identified and kept for
cladding zone. Material flow shall be such as to favourably resist the stresses encountered in service
(Main Working Direction).
4.5 Machining
Prior to the heat treatment, forgings shall be contour machined as close to the finish dimensions as
possible.
0.17- 1.2-1.5 0.15- 0.44- 0.5-0.8 0.20 0.08 0.02 0.03 0.01-
0.23 0.3 0.55 0.03
Note (1) - If these figures are exceeded and check analysis levels of up to P :S 0.015%, S :S 0.015%,
Mo :S 0.63%, Cu :S 0.18%, Sn :S 0.016% and N (tot) :S 0.015% are accepted, the inspection agency
shall determine until further notice whether heat affected zone simulation tests and, where
applicable, tangential section examination are required. If intermediate annealing at 550° C is
planned in the course of further processing the permissibility of this annealing temperature shall be
demonstrated in the course of the aforementioned tests/examinations. Extent and implementation
of testing shall be agreed upon with the Inspection Agency.
6.1 Sufficient vacuum degassing and Argon Lancing in LRF prior to ingot casting stage shall be given
to bring the Dissolved H2 ≤ 1 ppm. Dissolved H2 shall be analysed in pony ladle sample also.
Hydrogen sample analysis
shall be done on the
solidified Ingot casted on
top and bottom discard.
The Homogenisation
treatment of the ingot as
outlined below , however ,
with prior experience with
the supplier this can be
modified based on the
Laddle (LRF) sample
analysis, shall be imparted.
The Hydrogen content shall
be less than 1 ppm.
The hot forging operation shall be done above 1250℃ and forming operation shall not be done
below 1050℃ . Minimum forging ratio of 3 to be maintained. The forgings shall be supplied in
quenched and tempered condition. The forgings, after contour machining near to finish dimensions,
shall be heated to a temperature which produces an austenitic structure and then quenched in a
suitable liquid medium ensuring uniform cooling. The tempering temperature shall be between 650
to 680°C. The measured highest temperature during stress relief heat treatment shall not be higher
than the measured lowest temperature during tempering. The uniformity of temperature during
any of the heat treatment shall be proved by continuous temperature recording instruments with
the help of thermocouples attached to the component.
(sample QT graph)
[ quenching in higher rate means it shall be cooled as fast as possible while quenching in water and
the water temperature shall be maintained using cooling mechanism]
The simulated heat treatment (SHT) is intended to simulate the heating cycles which the actual
component may experience during the course of fabrication. Such heat treatment is given to some
of the test coupons called Simulated Heat Treated Coupons (STC). Heating and cooling rates shall be
as indicated in the figure below:
The simulated heat treatment (SHT) is intended to simulate the heating cycles which the actual
component may experience during the course of fabrication. Such heat treatment is given to some
of the test coupons called Simulated Heat treated Coupons (STC). Heating and cooling rates shall be
as indicated in the figure below:
7.0 MECHANICAL PROPERTIES:
7.1 The mechanical tests shall be conducted as per ASTM A-20 and ASTM A-370 (DIN 50115, DIN
50125 and DIN EN 10002-1). Following minimum requirements shall be met with both in Quenched
and Tempered and simulated heat treated condition for all products except manhole cover /
handhole cover wherein minimum requirement shall be met in Quenched & Tempered condition.
Rm=Tensile strength
R p 0.2=Yield Strength (0.2 % offset
A5 =% Elongation on 5d (in 50 mm minimum gauge length)
Z=% Reduction in area
L=Longitudinal; Tr= Transverse; N=Normal; SV=single value; AV=average value
7.1.1 General
Sl. At RT At 3500C
Tensile Requirements
No.
1. Tensile strength, MPa 550-725 550 min.
2. Yield strength, minimum [0.2% offset], MPa 345 285
3. Elongation in 2” or 50 mm, minimum, % 18 16
4. Reduction of area, minimum, % 38 To be
reported
RT: Room Temperature;
Notes:
(i) The above minimum values are applicable to all test
specimen orientations viz. Longitudinal/ Transverse/
Normal or Radial/ Tangential/ Axial.
(ii) Testing scope for Manhole covers in quenched & tempered
condition shall be same as that of, STC-B‟ of shell forgings.
Testing scope for Production Weld Test Coupon (PWTC) plates
in both quenched & tempered and simulated heat treated condition
shall be same as that of ,STC-B‟ of shell forgings. Notes:
(iii) The above minimum values are applicable to all test specimen
orientations viz. Longitudinal/ Transverse/ Normal or Radial/
Tangential/ Axial.
(iv) Testing scope for Manhole covers in quenched & tempered
condition shall be same as that of „STC-B‟ of shell forgings.
Testing scope for Production Weld Test Coupon (PWTC) plates in
both quenched & tempered and simulated heat treated condition
shall be same as that of STC-B‟ of shell forgings
.
7.1.3 Fracture Toughness Requirement
RTNDT shall be less than or equal to (–)15°C. Three Charpy V-notch (Cv)
transverse specimens shall be tested at +18°C (ie. RTNDT + 33) for certification of
RTNDT. The minimum absorbed energy and lateral expansion shall not be less
than 68 J and 0.89 mm respectively, for any of the specimens. The
percentage shear fracture shall be reported.
Charpy V-notch impact strength versus temperature curve shall be established. Tests shall be
conducted at least at six different temperatures including
(-)15°C and +18°C, to fully define upper and lower energy shelves. The upper energy shelf shall
have 100% shear fracture and lower energy shelf a maximum of 10% shear fracture. The test reports
shall include absorbed energy, percent shear fracture and lateral expansion, plotted against
temperature. The upper shelf energy shall be more than 100 J. The absorbed energy and lateral
expansion values at +18°C and (-)15°C shall meet the requirements of 7.1.3.2 and 7.1.3.3.
7.1.4 Hardness Requirement
Inclusion rating (Heavy and Thin Series) shall be determined as per ASTM-E 45
(Method A or D) and shall be better than –
A B C D
2.0 2.0 1.0 1.5
7.1.6.2 Through suitable metallurgical tests for which details shall be proposed in the offer
and finalized prior to award of the Contract the following shall be ensured by the
manufacturer:
The Contractor/Manufacturers shall arrange to submit complete details for various tests and
investigations which can be carried out by the manufacturers of the forged product. Quotations
should accompany the details regarding facilities available with the suppliers giving the test plans
and complete methodologies.
Compliance of the material with the specification requirements is checked on various categories of
test coupons described as under:
i) Raw Material Test Coupons (RTC) Test coupons obtained from the quenched and tempered
forgings or forging extensions. RTC samples shall be tested first.
ii) Simulated Heat Treated Test Coupons (STC) Test coupons obtained from the quenched and
tempered forgings and subjected to simulated heat treatment described in paragraph 5.3.7.3.
iii) Base Metal Test Coupons (BMTC) These are in the same condition as RTC. RTC and STC shall
be tested at the forging supplier‟s works whereas BMTC shall be dispatched with the ordered items
for production tests at equipment manufacturer‟s works.
iv) Production Weld Test Coupons (PWTC) PWTC wherever required shall be from the same heat.
The PWTC (generally flat plates of approximately 2500mm x 210mm x „t‟ thickness) shall
undergo same amount of deformation and shall be supplied in same heat treatment (Q&T) condition
as that of respective forgings
The test coupons shall be taken in such a way that the test specimens shall have their longitudinal axis at
least 1/4 t from any surface and with the mid length of the specimens at least 1/2 t (80 mm for shell, plate
and nozzle forging) from any second surface, where 't' is the maximum heat treated thickness of the forging
Top and bottom of the forgings shall be same as respective ends of the ingot. Sufficient material in
the form of integrally forged ring or disc prolongations shall be provided for the purpose of testing.
Prolongations at both ends shall be provided for cylindrical/conical shells and nozzle forgings from
which more than one nozzle is to be made. Dished ends, tube sheets and single
nozzle forgings shall have prolongation on the bottom end. From each coupon, a number of test
specimens are to be made as per the testing requirements mentioned elsewhere in this specification.
Hence the coupons should be of sufficient size to meet all testing requirements including
contingency requirements. Exact requirement for each forging product shall be worked out by the
Manufacturer and submitted for Purchaser‟s review and approval.
RTC, STC and BMTC shall be taken from the adjacent areas at any location of the cross section in
the following manner(Refer Figure – 12):
i) Full circumferential test rings shall be parted off from the forging prolongations after the final heat
treatment. In general, the cross section shall be divided into three sectors (say A, B & C at bottom
and D, E & F at top, as applicable) approximately spaced at 1200, so as to accommodate
test specimens required as per the extent of testing specified elsewhere in this specification.
ii) Each sector shall be suitably marked to accommodate RTC, STC and BMTC, adjacent to each
other. Identification of the coupons shall be ensured by suitable methods prior to their separation
from the test ring and all through the various stages of testing.
iii) The location of test coupons in the top and bottom test ring shall be diametrically opposite to
each other.
iv) Any balance material from the test rings, if in excess of the test requirement shall be marked as
reserve (RES) and preserved for any contingency which may arise during the course of testing/
manufacture of equipment.
v) Test coupons for forged plate for Manhole/ Handhole covers and PWTC shall be taken from one
end of the forged plate. Locations of test coupons for various forging products and material sampling
& testing plan are indicated in Figures 5 to 10. BMTCs, PWTC plates and reserve coupons (RES) if
any shall be dispatched along with the ordered items for final and pre-production tests at equipment
manufacturer‟s works. Any unused/ balance RTC and STC shall also be properly identified, marked,
packed and dispatched along with the product forgings.
The mechanical properties are to be established along the following three mutually perpendicular directions:
Chemical analysis shall be carried out in accordance with ASTM-E 30 & ASTM-E 350. If the ingot is made from
one heat, only one ladle analysis is required. However, in case of an ingot made from more than one heat,
weighted average shall be reported.
For product analysis, samples from each STC shall be analyzed. Samples for chemical analysis shall be taken
from a depth of 1/4t from any tempered wall surface and at least at a distance of 1 /2t from the heat treated
edge of the coupon. Broken mechanical test specimens may be used.
Apart from STC samples, the chemical composition shall also be determined as required by individual
product specifications.
The extent of tests required for each product has been included in tabular form under the product
specifications.
For tension test, one specimen shall be tested from a sampling point at room temperature and at 350°C.
For impact test, one set of 3 Charpy-V notch specimens shall be tested at a given temperature.
NDT temperature shall be determined using STC Pellini specimens from one location. The NDT temperature
so determined shall also be confirmed by tests on two transverse specimens taken from STC & RTC coupons
from other locations (See Tables I, 2 & 3). However, in case of Nozzle forgings (Table 4 & 5) NDT temperature
shall be confirmed by testing two transverse Pellini specimens from STC coupons as shown therein.
All forging after the final heat treatment and machining shall be ultrasonically examined in
accordance with SA-388, recommended practice for Ultrasonic Exanimation of Heavy Steel
Forgings and as per Annexure-A. Where ultrasonic examination is not feasible or only partially
feasible due to the final component geometry after machining, examination shall be carried out for
acceptance in the semi-machined condition. The forgings shall be examined for the total volume
using both straight beam and angle beam search units, observing the scanning directions
as indicated in Figure – Figure 2, 3, 4 and 4A. The reference level for the straight beam examination
shall be 6mm diameter flat bottom hole for t>100mm and 3mm for t≤100mm. For angle beam
examination, the reference level shall be a 3mm wide x 12mm long x 0.03 t deep notch (3mm
maximum depth), where t is final thickness of the material.
All Recordable indications (above 20% of reference level), apparently within acceptable limits shall
be investigated to confirm that they are parallel to the forging faces and not in the transverse
direction, i.e. not in the thickness direction. Defect indications under following conditions are not
acceptable.
When a cluster of small indications are obtained on the screen whose amplitudes cannot be resolved,
then the gain shall be adjusted defect free region. At this gain setting, the cluster of indication
causing loss of back echo shall be a cause of rejection of the forging. Loss of back echo is assumed
when the back reflection falls below 5% of full calibration screen height. Additionally, at such
locations the sound attenuation shall be measured. The sound attenuation at 2MHz shall not be more
than 4DB/Meter of single sound path. Examination of forged bars must be performed from both
thickness faces and from the cylindrical surface with normal beam probes. Additional scanning in
the circumferential direction with 450 and 350 angle beam probes shall be carried out for bars larger
than 120mm in diameter. The acceptance standard shall be as follows
D<60mm C.R.R.-2mm
D>60mm C.R.R.-3mm
D>120mm C.R.R.-4mm
(C.R.R. – Circular Reference Reflector, D – diameter of the bar)
The Manufacturer shall prepare detail Ultrasonic Testing / Examination procedure and submit for
approval
Each forging after final machining shall be examined by magnetic particle method (MT) in accordance with
ASME Section III, Para NB-2545. The acceptance standards shall be as per para NB-2545.3. The extent of
examination shall be 100%. Demagnetization is required after test.
Each forging shall be checked for dimensional compliance with the approved drawings. The actual
dimensions shall be recorded in a sketch/drawing and submitted for final acceptance.
10.0 REPAIRS
Repair of forgings are not permitted. Slight surface defects may be smoothly ground and blended without
impairing the minimum wall thickness. No other repair shall be carried out without prior approval of the
purchaser or his authorized inspection agency. Plans for all repairs requiring heat treatment shall be
submitted to the purchaser or his authorized inspection agency for review and approval, prior to taking up
the job. Repairs involving welding are prohibited.
All non-conformities shall be recorded and reported to the Purchaser to determine their disposal.
The manufacturer shall prepare Quality assurance plan (QAP), manufacturing, testing, examination
procedures, Fabrication drawings etc. and obtain Purchaser's approval prior to the commencement of
manufacture. The manufacturer shall be responsible for preparation and issue of all certificates, reports and
documents which shall be certified by the Purchaser or his authorized agency. Such certified fmal documents
shall be supplied in bound volumes with proper identification. Final documentation containing all the above
shall also be submitted in soft form (pdf format) with proper indexing.
The forgings shall be subjected to quality surveillance by the Purchaser or his authorized agency during
manufacture. The forgings shall not be shipped until the shipping release is given by the Purchaser/his
authorized agency.
Each forging shall be marked with Product Serial Number, Heat number, Material Specification and main
working direction. In case of forgings accompanied with forged test plates, corresponding test plate
identification shall also be marked on the main forging indicating correspondence with top/bottom of
original ingot.
The forgings shall be protected against corrosion and damage in transit and shall be properly preserved and
packed for sea-worthiness. The supplier shall submit the preservation and packing plan for Purchaser's
approval. Before shipment, suitable rust preventive coating shall be applied on the forgings to ensure sea-
worthiness and tropical storage for two years.
Notes:
1. If testing of the first specimen at RT yields Z <65%, then two more test specimens from the same sampling
location shall be tested.
2. Chemical composition shall be determined from one sampling location each from top and bottom. At
other location C, Mn, P&S shall be verified.
3. Hardness along a maximum square grid of 1000 mm x 1000 mm on the cylindrical outside surface
and end faces. In case Sulphur print is required to be carried out as specified in clause 8.7 of this
Specification, than it shall be carried out on top and bottom faces at 120° apart and 200 mm long.
Annexure-A