Thanks to visit codestin.com
Credit goes to link.springer.com

Skip to main content

Analysis of Fiber and Its Components

  • Chapter
  • First Online:
Science and Technology of Fibers in Food Systems

Part of the book series: Food Engineering Series ((FSES))

  • 1165 Accesses

  • 3 Citations

Abstract

The development of procedures for the quantification of dietary fiber (DF) has been evolving steadily since the “dietary fiber” term was coined. At the same time, the DF concept has been enriched and thus, the methodologies required to evaluate all the new components included in the improved concept need to be modified. In this context, it is necessary to recognize the evolution of the term to understand the modifications of the analysis methods, as well as to know the methodologies to comprehend the group of compounds that are quantified when the analyses are conducted. In the following chapter the most common current methods to determine soluble, insoluble and total dietary fiber as well as its components are described.

This is a preview of subscription content, log in via an institution to check access.

Access this chapter

Subscribe and save

Springer+
from £29.99 /Month
  • Starting from 10 chapters or articles per month
  • Access and download chapters and articles from more than 300k books and 2,500 journals
  • Cancel anytime
View plans

Buy Now

Chapter
GBP 19.95
Price includes VAT (United Kingdom)
  • Available as PDF
  • Read on any device
  • Instant download
  • Own it forever
eBook
GBP 71.50
Price includes VAT (United Kingdom)
  • Available as EPUB and PDF
  • Read on any device
  • Instant download
  • Own it forever
Softcover Book
GBP 129.99
Price includes VAT (United Kingdom)
  • Compact, lightweight edition
  • Dispatched in 3 to 5 business days
  • Free shipping worldwide - see info
Hardcover Book
GBP 89.99
Price includes VAT (United Kingdom)
  • Durable hardcover edition
  • Dispatched in 3 to 5 business days
  • Free shipping worldwide - see info

Tax calculation will be finalised at checkout

Purchases are for personal use only

Institutional subscriptions

Similar content being viewed by others

References

  • ALINORM 09/32/26 (2008) Report of the 30th session of the Codex committee on nutrition and foods for special dietary uses 3–7 November 2008

    Google Scholar 

  • Asp NG, Johansson CG, Hallmer H, Siljeström M (1983) Rapid enzymatic assay of insoluble and soluble dietary fiber. J Agric Food Chem 31:476–482

    Article  CAS  Google Scholar 

  • BeMiller JM (2010) Carbohydrates analysis. In: Nielsen SS (ed) Food analysis. Springer, New York

    Google Scholar 

  • Brunt K (2011) Dietary fibre levels in bread according to AOAC 985.29 and AOAC 2009.01 method. First results. In: 9th International Food data Conference 14–17 Sept. 2011. http://www.eurofir.org/2014/10/30/oral-presentations-from-the-9th-ifdc/

  • Brunt K, Sanders P (2013) Improvement of the AOAC 2009.01 total dietary fibre method for bread and other high starch containing matrices. Food Chem 140:574–580

    Article  CAS  Google Scholar 

  • Căpriţă R, Căpriţă A (2011) Chemical methods for the determination of soluble and insoluble non-starch polysaccharides – review. Anim Sci Biotechnol 44:73–80

    Google Scholar 

  • Causey JL, Fertag JM, Gallaher DD, Tungland BC, Slavin JL (2000) Effects of dietary inulin on serum lipids, blood glucose and the gastrointestinal environment in hypercholesterolemic men. Nutr Res 20:191–201

    Article  CAS  Google Scholar 

  • Champ M, Langkilde A-M, Brouns F, Kettlitz B, Collet YLB (2003) Advances in dietary fibre characterisation. 1. Definition of dietary fibre, physiological relevance, health benefits and analytical aspects. Nutr Res Rev 16:71–82

    Article  CAS  Google Scholar 

  • DeVries JW (2004) Dietary fiber: the influence of definition on analysis and regulation. J AOAC Int 87:682–706

    Article  CAS  Google Scholar 

  • DeVries JW, Camire ME, Cho S, Craig S, Gordon D, Jones JM, Li B, Lineback D, Prosky L, Tungland BC (2001) The definition of dietary fiber. Cereal Foods World 46:112–129

    CAS  Google Scholar 

  • Dhingra D, Michael M, Rajput H, Patil RT (2012) Dietary fibre in foods: a review. J Food Sci Technol 49:255–266

    Article  CAS  Google Scholar 

  • Englyst H, Wiggins HS, Cummings JH (1982) Determination of the non-starch polysaccharides in plant foods by gas-liquid chromatography of constituent sugars as alditol acetates. Analyst 107:307–318

    Article  CAS  Google Scholar 

  • European Food Safety Authority (2010) Scientific opinion on dietary reference values for carbohydrates and dietary fibre. EFSA J 8:1–77

    Google Scholar 

  • FDA (2014) Food labeling: revision of the nutrition and supplement facts labels

    Google Scholar 

  • Garcia-Amezquita LE, Tejada-Ortigoza V, Heredia-Olea E, Serna-Saldívar SO, Welti-Chanes J (2018) Differences in the dietary fiber content of fruits and their by-products quantified by conventional and integrated AOAC official methodologies. J Food Compos Anal 67:77–85

    Article  CAS  Google Scholar 

  • Hipsley EH (1953) Dietary “fibre” and pregnancy toxaemia. Med J Aust 2:341–342

    Article  Google Scholar 

  • Hollmann J, Themeier H, Neese U, Lindhauer MG (2013) Dietary fibre fractions in cereal foods measured by a new integrated AOAC method. Food Chem 140:586–589

    Article  CAS  Google Scholar 

  • Jenkins DJA, Kendall CWC, Vuksan V (1999) Inulin, oligofructose and intestinal function. J Nutr 129:1431s–1433s

    Article  CAS  Google Scholar 

  • Kaczmarczyk MM, Miller MJ, Freund GG (2012) The health benefits of dietary fiber: beyond the usual suspects of type 2 diabetes mellitus, cardiovascular disease and colon cancer. Metab Clin Exp 61:1058–1066

    Article  CAS  Google Scholar 

  • Lee SC, Prosky L, DeVries JW (1992) Determination of total, soluble and insoluble fiber foods. J Assoc Off Anal Chem 75:395–416

    CAS  Google Scholar 

  • McCleary BV (2007) An integrated procedure for the measurement of total dietary fibre (including resistant starch), non-digestible oligosaccharides and available carbohydrates. Anal Bioanal Chem 389:291–308

    Article  CAS  Google Scholar 

  • McCleary BV (2014) Modification to AOAC official methods 2009.01 and 2011.25 to allow for minor overestimation of low molecular weight soluble dietary fiber in samples containing starch. J AOAC Int 97:896–901

    Article  CAS  Google Scholar 

  • McCleary BV, DeVries JW, Rader JI, Cohen G, Prosky L, Mugford DC, Champ M, Okuma K (2011) Collaborative study report: determination of insoluble, soluble, and total dietary fiber (Codex definition) by an enzymatic-gravimetric method and liquid chromatography. Cereal Foods World 56:238–247

    CAS  Google Scholar 

  • McCleary BV, Sloane N, Draga A, Lazewska I (2013) Measurement of total dietary fiber using AOAC method 2009. 01 (AACC International approved method 32-45. 01): evaluation and updates. Cereal Chem 90:396–914

    Article  CAS  Google Scholar 

  • Norma Oficial Mexicana (2010) NOM-051-SCFI/SSA1–2010, Especificaciones generales de etiquetado para alimentos y bebidas no alcohólicas preenvasados-Información comercial y sanitaria

    Google Scholar 

  • Prosky L, Asp NG, Furda I, DeVries JW, Schweizer TF, Harland B (1984) Determination of total dietary fiber in foods and food products: collaborative study. J Assoc Off Anal Chem 68:677–679

    Google Scholar 

  • Sluiter A, Hames B, Ruiz R, Scarlata C, Sluiter J, Templeton D, Crocker D (2008) Determination of structural carbohydrates and lignin in biomass. National Renewable Energy Laboratory. Technical Report NREL/TP-510-42618

    Google Scholar 

  • Southgate DAT (1969a) Determination of carbohydrates in foods II. – unavailable carbohydrates. J Sci Food Agric 20:331–335

    Article  CAS  Google Scholar 

  • Southgate DAT (1969b) Determination of carbohydrates in foods I. J Sci Food Agric 20:326–330

    Article  CAS  Google Scholar 

  • Tejada-Ortigoza V, Garcia-Amezquita LE, Serna-Saldívar SO, Welti-Chanes J (2016) Advances in the functional characterization and extraction processes of dietary fiber. Food Eng Rev 8:251–271

    Article  CAS  Google Scholar 

  • Templeton D, Ehrman T (1995) Determination of acid-insoluble lignin in biomass. National Renewable Energy Laboratory

    Google Scholar 

  • Theander O, Aman P (1979) Studies on dietary fibres. Analysis and chemical characterization of water-soluble and water-insoluble dietary fibers. Swed J Agric Res 9:97–106

    CAS  Google Scholar 

  • Theander O, Aman P, Westerlund E, Andersson R, Pettersson D (1995) Total dietary fiber determined as neutral sugar residues, uronic acid residues, and Klason lignin. J AOAC Int 78:1030–1044

    Article  CAS  Google Scholar 

  • Tobaruela E d C, Santos A d O, de Almeida-Muradian LB, Araujo E d S, Lajolo FM, Menezes EW (2018) Application of dietary fiber method AOAC 2011.25 in fruit and comparison with AOAC 991.43 method. Food Chem 238:87–93

    Article  CAS  Google Scholar 

  • Trowell H (1976) Dietary fibre redefined. Lancet 307:1129

    Article  Google Scholar 

  • Zielinski G, Rozema B (2013) Review of fiber methods and applicability to fortified foods and supplements: choosing the correct method and interpreting results. Anal Bioanal Chem 405:4359–4372

    Article  CAS  Google Scholar 

Download references

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to Luis Eduardo Garcia-Amezquita .

Editor information

Editors and Affiliations

Rights and permissions

Reprints and permissions

Copyright information

© 2020 Springer Nature Switzerland AG

About this chapter

Check for updates. Verify currency and authenticity via CrossMark

Cite this chapter

Garcia-Amezquita, L.E., Viacava, F., Jacobo-Velázquez, D.A. (2020). Analysis of Fiber and Its Components. In: Welti-Chanes, J., Serna-Saldívar, S., Campanella, O., Tejada-Ortigoza, V. (eds) Science and Technology of Fibers in Food Systems. Food Engineering Series. Springer, Cham. https://doi.org/10.1007/978-3-030-38654-2_4

Download citation

Publish with us

Policies and ethics