Abstract
The development of procedures for the quantification of dietary fiber (DF) has been evolving steadily since the “dietary fiber” term was coined. At the same time, the DF concept has been enriched and thus, the methodologies required to evaluate all the new components included in the improved concept need to be modified. In this context, it is necessary to recognize the evolution of the term to understand the modifications of the analysis methods, as well as to know the methodologies to comprehend the group of compounds that are quantified when the analyses are conducted. In the following chapter the most common current methods to determine soluble, insoluble and total dietary fiber as well as its components are described.
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References
ALINORM 09/32/26 (2008) Report of the 30th session of the Codex committee on nutrition and foods for special dietary uses 3–7 November 2008
Asp NG, Johansson CG, Hallmer H, Siljeström M (1983) Rapid enzymatic assay of insoluble and soluble dietary fiber. J Agric Food Chem 31:476–482
BeMiller JM (2010) Carbohydrates analysis. In: Nielsen SS (ed) Food analysis. Springer, New York
Brunt K (2011) Dietary fibre levels in bread according to AOAC 985.29 and AOAC 2009.01 method. First results. In: 9th International Food data Conference 14–17 Sept. 2011. http://www.eurofir.org/2014/10/30/oral-presentations-from-the-9th-ifdc/
Brunt K, Sanders P (2013) Improvement of the AOAC 2009.01 total dietary fibre method for bread and other high starch containing matrices. Food Chem 140:574–580
Căpriţă R, Căpriţă A (2011) Chemical methods for the determination of soluble and insoluble non-starch polysaccharides – review. Anim Sci Biotechnol 44:73–80
Causey JL, Fertag JM, Gallaher DD, Tungland BC, Slavin JL (2000) Effects of dietary inulin on serum lipids, blood glucose and the gastrointestinal environment in hypercholesterolemic men. Nutr Res 20:191–201
Champ M, Langkilde A-M, Brouns F, Kettlitz B, Collet YLB (2003) Advances in dietary fibre characterisation. 1. Definition of dietary fibre, physiological relevance, health benefits and analytical aspects. Nutr Res Rev 16:71–82
DeVries JW (2004) Dietary fiber: the influence of definition on analysis and regulation. J AOAC Int 87:682–706
DeVries JW, Camire ME, Cho S, Craig S, Gordon D, Jones JM, Li B, Lineback D, Prosky L, Tungland BC (2001) The definition of dietary fiber. Cereal Foods World 46:112–129
Dhingra D, Michael M, Rajput H, Patil RT (2012) Dietary fibre in foods: a review. J Food Sci Technol 49:255–266
Englyst H, Wiggins HS, Cummings JH (1982) Determination of the non-starch polysaccharides in plant foods by gas-liquid chromatography of constituent sugars as alditol acetates. Analyst 107:307–318
European Food Safety Authority (2010) Scientific opinion on dietary reference values for carbohydrates and dietary fibre. EFSA J 8:1–77
FDA (2014) Food labeling: revision of the nutrition and supplement facts labels
Garcia-Amezquita LE, Tejada-Ortigoza V, Heredia-Olea E, Serna-Saldívar SO, Welti-Chanes J (2018) Differences in the dietary fiber content of fruits and their by-products quantified by conventional and integrated AOAC official methodologies. J Food Compos Anal 67:77–85
Hipsley EH (1953) Dietary “fibre” and pregnancy toxaemia. Med J Aust 2:341–342
Hollmann J, Themeier H, Neese U, Lindhauer MG (2013) Dietary fibre fractions in cereal foods measured by a new integrated AOAC method. Food Chem 140:586–589
Jenkins DJA, Kendall CWC, Vuksan V (1999) Inulin, oligofructose and intestinal function. J Nutr 129:1431s–1433s
Kaczmarczyk MM, Miller MJ, Freund GG (2012) The health benefits of dietary fiber: beyond the usual suspects of type 2 diabetes mellitus, cardiovascular disease and colon cancer. Metab Clin Exp 61:1058–1066
Lee SC, Prosky L, DeVries JW (1992) Determination of total, soluble and insoluble fiber foods. J Assoc Off Anal Chem 75:395–416
McCleary BV (2007) An integrated procedure for the measurement of total dietary fibre (including resistant starch), non-digestible oligosaccharides and available carbohydrates. Anal Bioanal Chem 389:291–308
McCleary BV (2014) Modification to AOAC official methods 2009.01 and 2011.25 to allow for minor overestimation of low molecular weight soluble dietary fiber in samples containing starch. J AOAC Int 97:896–901
McCleary BV, DeVries JW, Rader JI, Cohen G, Prosky L, Mugford DC, Champ M, Okuma K (2011) Collaborative study report: determination of insoluble, soluble, and total dietary fiber (Codex definition) by an enzymatic-gravimetric method and liquid chromatography. Cereal Foods World 56:238–247
McCleary BV, Sloane N, Draga A, Lazewska I (2013) Measurement of total dietary fiber using AOAC method 2009. 01 (AACC International approved method 32-45. 01): evaluation and updates. Cereal Chem 90:396–914
Norma Oficial Mexicana (2010) NOM-051-SCFI/SSA1–2010, Especificaciones generales de etiquetado para alimentos y bebidas no alcohólicas preenvasados-Información comercial y sanitaria
Prosky L, Asp NG, Furda I, DeVries JW, Schweizer TF, Harland B (1984) Determination of total dietary fiber in foods and food products: collaborative study. J Assoc Off Anal Chem 68:677–679
Sluiter A, Hames B, Ruiz R, Scarlata C, Sluiter J, Templeton D, Crocker D (2008) Determination of structural carbohydrates and lignin in biomass. National Renewable Energy Laboratory. Technical Report NREL/TP-510-42618
Southgate DAT (1969a) Determination of carbohydrates in foods II. – unavailable carbohydrates. J Sci Food Agric 20:331–335
Southgate DAT (1969b) Determination of carbohydrates in foods I. J Sci Food Agric 20:326–330
Tejada-Ortigoza V, Garcia-Amezquita LE, Serna-Saldívar SO, Welti-Chanes J (2016) Advances in the functional characterization and extraction processes of dietary fiber. Food Eng Rev 8:251–271
Templeton D, Ehrman T (1995) Determination of acid-insoluble lignin in biomass. National Renewable Energy Laboratory
Theander O, Aman P (1979) Studies on dietary fibres. Analysis and chemical characterization of water-soluble and water-insoluble dietary fibers. Swed J Agric Res 9:97–106
Theander O, Aman P, Westerlund E, Andersson R, Pettersson D (1995) Total dietary fiber determined as neutral sugar residues, uronic acid residues, and Klason lignin. J AOAC Int 78:1030–1044
Tobaruela E d C, Santos A d O, de Almeida-Muradian LB, Araujo E d S, Lajolo FM, Menezes EW (2018) Application of dietary fiber method AOAC 2011.25 in fruit and comparison with AOAC 991.43 method. Food Chem 238:87–93
Trowell H (1976) Dietary fibre redefined. Lancet 307:1129
Zielinski G, Rozema B (2013) Review of fiber methods and applicability to fortified foods and supplements: choosing the correct method and interpreting results. Anal Bioanal Chem 405:4359–4372
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Garcia-Amezquita, L.E., Viacava, F., Jacobo-Velázquez, D.A. (2020). Analysis of Fiber and Its Components. In: Welti-Chanes, J., Serna-Saldívar, S., Campanella, O., Tejada-Ortigoza, V. (eds) Science and Technology of Fibers in Food Systems. Food Engineering Series. Springer, Cham. https://doi.org/10.1007/978-3-030-38654-2_4
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