Thanks to visit codestin.com
Credit goes to link.springer.com

Skip to main content
Log in

Review of fiber methods and applicability to fortified foods and supplements: choosing the correct method and interpreting results

  • Review
  • Published:
Analytical and Bioanalytical Chemistry Aims and scope Submit manuscript

Abstract

Fiber is known to be an important part of our nutrition and has many positive health benefits, including weight management and maintaining heart health. In recent years, a number of new ingredients have been manufactured or isolated that are being used to increase the health benefits of a product. Some are used as prebiotics that stimulate the growth of the beneficial bacteria in the gut, or are used as replacements for sugars, starch, or fat in manufactured foods. Fiber supplements have also been produced that can be taken to provide additional fiber to the diet. The term “fiber” does not relate to a single analyte or entity, but instead relates to a multitude of components. This adds to the complexity of analytical testing as there are a number of AOAC International and AACC International official methods which have been validated and can be used. Although methods have been developed for specific fiber ingredients, a number of methods have also been developed to capture just “fiber”. These “fiber” methods will capture differing degrees of the different fiber ingredients, so knowledge of the fiber sources is critical. The net result is that a variety of testing approaches may be used, but caution must be exercised in order to ensure that the total fiber result is accurately determined. A critical review of available fiber methodology and possible testing approaches is presented, along with how to accurately interpret and understand results.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Subscribe and save

Springer+
from £29.99 /Month
  • Starting from 10 chapters or articles per month
  • Access and download chapters and articles from more than 300k books and 2,500 journals
  • Cancel anytime
View plans

Buy Now

Price includes VAT (United Kingdom)

Instant access to the full article PDF.

Fig. 1
Fig. 2
Fig. 3
Fig. 4
Fig. 5

Similar content being viewed by others

Abbreviations

DP:

Degree of polymerization

DP2:

Degree of polymerization of 2

DP3:

Degree of polymerization of 3

EU:

European Union

FOS:

Fructooligosaccharide

GOS:

Galactooligosaccharide

HPAEC:

High-performance anion-exchange chromatography

HPLC:

High-performance liquid chromatography

IDF:

Insoluble dietary fiber

SDF:

Soluble dietary fiber

SDFP:

Precipitated soluble dietary fiber

WASDF:

Water/alcohol-soluble dietary fiber

References

  1. Institute of Medicine of the National Academies (2005) Dietary reference intakes for energy, carbohydrate, fiber, fat, fatty acids, cholesterol, protein, and amino acids. National Academy Press, Washington

    Google Scholar 

  2. US Department of Agriculture and US Department of Health and Human Services (2010) Dietary guidelines for Americans, 7th edn. United States Government Printing Office, Washington

    Google Scholar 

  3. Code of Federal Regulations (2012) Title 21, part 101.76. United States Government Printing Office, Washington

    Google Scholar 

  4. Code of Federal Regulations (2012) Title 21, part 101.77. United States Government Printing Office, Washington

    Google Scholar 

  5. Code of Federal Regulations (2012) Title 21, part 101.81. United States Government Printing Office, Washington

    Google Scholar 

  6. Code of Federal Regulations (2012) Title 21, part 101.54. United States Government Printing Office, Washington

    Google Scholar 

  7. Hipsley EH (1953) Br Med J 2:420–422

    Article  CAS  Google Scholar 

  8. DeVries JW (2004) J AOAC Int 87(3):683–706

    Google Scholar 

  9. DeVries JW, Rader JI (2005) J AOAC Int 88(5):1349–1366

    CAS  Google Scholar 

  10. Institute of Medicine (2001) Dietary reference intakes: proposed definition of dietary fiber. National Academy Press, Washington

    Google Scholar 

  11. AACC International (2001) Cereal Foods World 46(3):112–126

    Google Scholar 

  12. Codex Alimentarius Commission (2011) Guidelines on nutrition labeling. CAC/GL 2-1985. Codex Alimentarius Commission, Rome

    Google Scholar 

  13. Code of Federal Regulations (2012) Title 21, part 101.9 (c) (6) (i). United States Government Printing Office, Washington

  14. Code of Federal Regulations (2012) Title 21, part 101.9 (g) (2). United States Government Printing Office, Washington

  15. Health Canada (2012) Policy for labelling and advertising of dietary fibre-containing food products. Bureau of Nutritional Sciences, Food Directorate, Health Products and Food Branch, Health Canada, Ottawa

    Google Scholar 

  16. The Council of the European Communities (2008) Council Directive of 24 September 1990 on nutrition labeling for foodstuffs (90/496/EEC). Publications Office of the European Union, Luxembourg

    Google Scholar 

  17. Foreign Agriculture Service (2010) Mexican Official Norm NOM-051-SCFI/SSA 1-2010, general labeling specifications for pre-packaged food and non-alcoholic beverages—commercial and food safety information. http://www.mexico-usda.com.mx/home/media/NEW_NOM-051-SCFI-SSA1-ENGLISH.pdf. Accessed 4 Sep 2012

  18. Cho SS, Dreher ML (2001) Handbook of dietary fiber. Dekker, New York

    Google Scholar 

  19. Cho SS, Samual P (2009) Fiber ingredients: food applications and health benefits. CRC, Boca Raton

    Book  Google Scholar 

  20. L’Homme C, Arbelot M, Puigserver A, Biagini A (2003) J Agric Food Chem 51:224–228

    Article  Google Scholar 

  21. Lefranc-Millot C, Wils D, Keremaux L, Pochat M (2009) Nutriose®, more than just a soluble fiber. Poster presented at the 4th international dietary fiber conference, Vienna

  22. Tate & Lyle (2011) Promitor™ soluble corn fiber 85, Promitor dietary fiber. http://www.promitorfiber.com/promitor_dietary_fibers/pages/promitorsolublecornfiber85.aspx. Accessed 6 Sep 2012

  23. Tate & Lyle (2011) Promitor™ soluble corn fiber 70, Promitor dietary fiber. http://www.promitorfiber.com/promitor_dietary_fibers/pages/promitorsolublecornfiber70.aspx. Accessed 6 Sep 2012

  24. Kendall C et al (2008) J Am Coll Nutr 27(6):711–718

    CAS  Google Scholar 

  25. Torres D et al (2010) Compr Rev Food Sci Food Saf 9:438–454

    Article  CAS  Google Scholar 

  26. AOAC International (2005) Official methods of analysis of AOAC International, 18th edn. AOAC International, Gaithersburg

    Google Scholar 

  27. Cho S, DeVries J, Prosky L (1997) Dietary fiber analysis and applications. AOAC International, Gaithersburg

    Google Scholar 

  28. Lee S et al (1992) J AOAC Int 75(3):395–416

    CAS  Google Scholar 

  29. Prosky L et al (1985) J AOAC Int 68(4):677–679

    CAS  Google Scholar 

  30. Lee S, Prosky L, DeVries JW (1992) J AOAC Int 75(3):395–416

    CAS  Google Scholar 

  31. Gordon DT, Okuma K (2002) J AOAC Int 85(2):435–444

    CAS  Google Scholar 

  32. McCleary BV et al (2010) J AOAC Int 93(1):221–233

    CAS  Google Scholar 

  33. Hoebregs H (1997) J AOAC Int 80(5):1029–1037

    CAS  Google Scholar 

  34. McCleary BV, Murphy A, Mugford DC (2000) J AOAC Int 83(2):356–364

    CAS  Google Scholar 

  35. Craig SA, Holden JF, Khaled MY (2001) J AOAC Int 84(2):472–478

    CAS  Google Scholar 

  36. De Slegte J (2002) J AOAC Int 85(2):417–423

    Google Scholar 

Download references

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to Garrett Zielinski.

Additional information

Published in the topical collection Functional Foods and Dietary Supplements with guest editors Melissa M. Phillips and Catherine A. Rimmer.

Rights and permissions

Reprints and permissions

About this article

Cite this article

Zielinski, G., Rozema, B. Review of fiber methods and applicability to fortified foods and supplements: choosing the correct method and interpreting results. Anal Bioanal Chem 405, 4359–4372 (2013). https://doi.org/10.1007/s00216-013-6711-x

Download citation

  • Received:

  • Revised:

  • Accepted:

  • Published:

  • Issue date:

  • DOI: https://doi.org/10.1007/s00216-013-6711-x

Keywords