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Fatigue Performance of an Improved Creep Strength 10%Cr Steel

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Abstract

The deployment of 9-12% Cr steels for elevated temperature applications up to 650 °C presents a cost-effective alternative to more expensive nickel-based alloys in steam turbine power generation. To enhance creep resistance at this temperature range, a novel ferritic-martensitic steel, designated CPJ7, was developed and fabricated at the National Energy Technology Laboratory. The alloy design aimed to mitigate the transformation of strengthening carbides into deleterious phases that degrade creep performance. Results have demonstrated that CPJ7 exhibits favorable creep and oxidation resistance at 650 °C. However, its fatigue performance remains unexplored. This study builds upon prior research by evaluating the low cycle fatigue behavior of CPJ7 and verifying that modifications beneficial to creep performance were not detrimental to the fatigue performance. The alloy was tested at both 650 °C and ambient temperature under fully reversed bending conditions (R = − 1) and a load ratio of 0.05. The alloy exhibits cyclic softening, a behavior consistent with other 9-10 wt.% Cr steels. Analysis of the microstructure and hysteresis loops further corroborate cyclic softening mechanisms typical of ferritic-martensitic steels. Overall, the fatigue performance of CPJ7 meets or exceeds that of P91 steel, demonstrating its potential for high-temperature structural applications.

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Abbreviations

LCF:

Low cycle fatigue

N f :

Failure cycle

K :

Stress intensity factor

Δε :

Strain range

σ f :

Is the frictional stress

σ max :

Is the maximum stress from the half hysteresis loop

σ y :

Is the yield stress

σ b :

Is the back stress

PAG:

Prior austenite grain

References

  1. R. Viswanathan, J.A. Hawk, R.C. Schwant, D. Saha, T. Totemeier, S.Goodstine, A. M. Mcnally, D.B. Allen, Steam Turbine Materials for Ultrasupercritical Coal Power Plants, Independence, OH, 2009, pp. 1-535.

  2. J.R. DiStefano, V.K. Sikka, J.J. Blass, C.R. Brinkman, J.M. Corum, J.A. Horak, R.L. Huddleston, J.F. King, R.W. McClung, W.K. Sartory, Summary of Modified 9Cr-1Mo Steel Development Program, 1975-1985, United States, 1986.

  3. C. Pandey, M.M. Mahapatra, P. Kumar and N. Saini, Some Studies on P91 Steel and their Weldments, J. Alloys Compd., 2018, 743, p 332–364.

    Article  CAS  Google Scholar 

  4. T. Fujita, Current Progress in Advanced High Cr Ferritic Steels for High-Temperature Applications, ISIJ Int., 1992, 32(2), p 175–181.

    Article  Google Scholar 

  5. J.A. Hawk and P.D. Jablonksi, Heat Resistant Advanced 9% Cr Steel for Fossil Energy Power Generation, TechConnect, Briefs, 2017, 2, p 152–155.

    Google Scholar 

  6. M. Detrois, P.D. Jablonski and J.A. Hawk, Evolution of Tantalum Content during Vacuum Induction Melting and Electroslag Remelting of a Novel Martensitic Steel, Metall. Mater. Trans. B, 2019, 50(4), p 1686–1695.

    Article  CAS  Google Scholar 

  7. M. Detrois, P.D. Jablonski, J.A. Hawk, Martensitic Steel CPJ7 for Improved High-Temperature Creep Capabilites in Power Plants, in: J.S.M. Takeyama (Ed.) Joint EPRI—123HiMat International Confrence on Advances in High Temperature Materials, ASM International, Nagasaki, Japan, 2019.

  8. M. Detrois, J.A. Hawk and P.D. Jablonski, Creep-Resistant Ferritic-Martensitic Steels for Power Plant Applications, J. Mater. Eng. Perform., 2024, 33(1), p 1–42.

    Article  CAS  Google Scholar 

  9. J.A. Hawk, P.D. Jablonski, C.J. Cowen, Creep Resistant High Temperature Martensitic Steel, in: U. States (Ed.) US Department of Energy, USA, 2013.

  10. J.A. Hawk, P.D. Jablonski, C.J. Cowen, Creep Resistant High Temperature Martensitic Steel, in: U. States (Ed.) US Department of Energy, USA, 2015.

  11. E. Kiss and S. Ranganath, On-Line Monitoring to Assure Structural Integrity of Nuclear Reactor Components, Int. J. Press. Vessels Piping, 1988, 34(1–5), p 3–15.

    Article  Google Scholar 

  12. J. Heliot and R. Fritz, Framatome Operating Transients Monitoring-System used for Equipment Mechanical Surveillance, Int. J. Pressure Vessels Piping, 1989, 40(3), p 247–258.

    Article  Google Scholar 

  13. M. Banaszkiewicz, On-Line Monitoring and Control of Thermal Stresses in Steam Turbine Rotors, Appl. Therm. Eng., 2016, 94, p 763–776.

    Article  Google Scholar 

  14. Z. Chen, G. Li, H. Zhang and C. Chen, Fatigue Life Prediction of Regulating Valves on the Intermediate-Pressure Section of a 400 MW Steam Turbine, Eng. Fail. Anal., 2009, 16(5), p 1483–1492.

    Article  Google Scholar 

  15. Q. Xiong, H. Guan, H. Ma, Z.Y. Wu, J. Zeng, W.W. Wang and H.J. Wang, Crack Propagation and Induced Vibration Characteristics of Cracked Cantilever Plates under Resonance State: Experiment and Simulation, Mech. Syst. Signal Process., 2023, 201, p 110674.

    Article  Google Scholar 

  16. P.D. Jablonski and J.A. Hawk, Nitrogen Control in VIM Melts, Springer International Publishing, Cham, 2016, p 315–319

    Google Scholar 

  17. P.D. Jablonski and J.A. Hawk, Homogenizing Advanced Alloys: Thermodynamic and Kinetic Simulations Followed by Experimental Results, J. Mater. Eng. Perform., 2016, 26(1), p 4–13.

    Article  Google Scholar 

  18. ASTM, ASTM E466-21 Standard Practice for Conducting Force Controlled Constant Amplitude Axial Fatigue Tests of Metallic Materials, 2021.

  19. ASTM, ASTM E606-04 Standard Practice for Strain-Controlled Fatigue Testing, 2017.

  20. C. Zhao, J. Zhang, J. Fu, Y. Lian, Z. Zhang, C. Zhang and J. Huang, Low-Cycle Fatigue Behavior of the Novel Steel and 30SiMn2MoV Steel at 700 °C, Materials, 2020 https://doi.org/10.3390/ma13245753

    Article  PubMed  PubMed Central  Google Scholar 

  21. T.T. Nguyen, K.B. Yoon, J. Park and U.B. Baek, Characterization of Strain-Controlled Low-Cycle Fatigue and Fracture Behavior of P91 Steel at Elevated Temperatures, Eng. Fail. Anal., 2022, 133, p 105887.

    Article  CAS  Google Scholar 

  22. K. Guguloth, S. Sivaprasad, D. Chakrabarti and S. Tarafder, Low-Cyclic Fatigue Behavior of Modified 9Cr-1Mo Steel at Elevated Temperature, Mater. Sci. Eng. –Struct. Mater. Prop. Microstruct. Process., 2014, 604, p 196–206.

    Article  CAS  Google Scholar 

  23. R. Mishnev, N. Dudova and R. Kaibyshev, Effect of Microstructural Evolution on the Cyclic Softening of a 10% Cr Martensitic Steel under Low Cycle Fatigue at 600 °C, Int. J. Fatigue, 2020, 134, p 105522.

    Article  CAS  Google Scholar 

  24. L.F. Coffin, Fatigue at High Temperature-Prediction and Interpretation, Proc. Inst. Mech. Eng., 1974, 188(1), p 109–127.

    Article  Google Scholar 

  25. O.H. Basquin, The Exponential Law of Endurance Tests, Proc. ASTM., 1910, 10(2), p 625–630.

    Google Scholar 

  26. S.S. Manson and M.H. Hirschberg, The Role of Ductility, Tensile Strength and Fracture Toughness in Fatigue, J. Franklin Inst., 1970, 290(6), p 539–548.

    Article  Google Scholar 

  27. A.H. Cottrell, Dislocations and Plastic Flow in Crystals, Oxford University Press, London, England, 1953.

    Google Scholar 

  28. D. Kuhlmann-Wilsdorf and C. Laird, Dislocation Behavior in Fatigue, Mater. Sci. Eng., 1977, 27(2), p 137–156.

    Article  CAS  Google Scholar 

  29. D. Kuhlmann-Wilsdorf and C. Laird, Dislocation Behavior in Fatigue Part II. Friction Stress and Back Stress as Inferred from an Analysis of Hysteresis Loops, Mater. Sci. Eng., 1979, 37(2), p 111–120.

    Article  CAS  Google Scholar 

  30. D. Kuhlmann-Wilsdorf, Dislocation Behavior in Fatigue part III. Properties of Loop Patches—Do they Participate in Fatigue Cycling?, Mater. Sci. Eng., 1979, 39(1), p 127–139.

    Article  Google Scholar 

  31. D. Kuhlmann-Wilsdorf, Dislocation Behavior in Fatigue IV. Quantitative Interpretation of Friction Stress and Back Stress Derived from Hysteresis Loops, Mater. Sci. Eng., 1979, 39(2), p 231–245.

    Article  CAS  Google Scholar 

  32. D. Kuhlmann-Wilsdorf and C. Laird, Dislocation Behavior in Fatigue V: Breakdown of Loop Patches and Formation of Persistent Slip Bands and of Dislocation Cells, Mater. Sci. Eng., 1980, 46(2), p 209–219.

    Article  CAS  Google Scholar 

  33. C. Laird, J.M. Finney and D. Kuhlmann-Wilsdorf, Dislocation Behavior in Fatigue VI: Variation in the Localization of Strain in Persistent Slip Bands, Mater. Sci. Eng., 1981, 50(1), p 127–136.

    Article  CAS  Google Scholar 

  34. J.Z. Xie, Low Cycle Fatigue and Fatigue Crack Growth Behaviros of Alloy IN718, in: E.A. Loria (Ed.) Superalloys 718 625 and Various Derivaties, 1991, pp. 491-500.

  35. F. Benjamin, S. Maxime, R. Alexandra, B. Françoise and P. André, Microstructural Evolutions and Cyclic Softening of 9%Cr Martensitic Steels, J. Nucl. Mater., 2009, 386–388, p 71–74.

    Article  Google Scholar 

  36. W. Electric, Statistical Quality Control Handbook, 1958.

  37. NIMS, Creep of P91 Steel. https://smds.nims.go.jp/creep/index_en.html.

  38. J.H. Xu, Z.W. Huang and L. Jiang, Effect of Heat Treatment on Low Cycle Fatigue of IN718 Superalloy at the Elevated Temperatures, Mater. Sci. Eng. A, 2017, 690, p 137–214.

    Article  CAS  Google Scholar 

  39. H. Oh, S. Kim, J.G. Kim, F. Taleghani and S. Kim, Low Cycle Fatigue Behavior of Inconel 706 at 650 °C, J. Mater. Res. Technol., 2022, 17, p 2624–2635.

    Article  CAS  Google Scholar 

  40. L. Xiao, D.L. Chen and M.C. Chaturvedi, Cyclic Deformation Mechanisms of Precipitation-Hardened Inconel 718 Superalloy, Mater. Sci. Eng. Struct. Mater. Propert. Microstruct. Process., 2008, 483–84, p 369–372.

    Article  Google Scholar 

  41. L. Pike, Low-Cycle Fatigue Behavior of HAYNES® 282® Alloy and Other Wrought Gamma-Prime Strengthened Alloys, Turbo Expo: Power for Land, Sea, and Air, 2007, pp. 161-169.

  42. B. Wang, X.H. An, P. Xue, F.C. Liu, D.R. Ni, B.L. Xiao, Y.D. Liu and Z.Y. Ma, Grain Size Effects on High Cycle Fatigue Behaviors of Pure Aluminum, Int. J. Fatigue, 2023, 170, p 107556.

    Article  CAS  Google Scholar 

  43. L.L. Liu, D.Y. Hu, D. Li, R.G. Hu, Y.X. Gu, R.Q. Wang, Effect of Grain Size on Low Cycle Fatigue Life in Compressor Disc Superalloy GH4169 at 600 C, 3rd InXternational Symposium on Fatigue Design and Material Defects (Fdmd 2017) 7 (2017) 174-181.

  44. A. Järvenpää, L.P. Karjalainen and M. Jaskari, Effect of Grain Size on Fatigue Behavior of Type 301LN Stainless Steel, Int. J. Fatigue, 2014, 65, p 93–98.

    Article  Google Scholar 

  45. N. Dudova, R. Mishnev and R. Kaibyshev, On the Mmicrostructural Evolution in a 10% Cr Martensitic Steel during Interrupted Low Cycle Fatigue Testing at 650 °C, Int. J. Fatigue, 2023, 175, p 107806.

    Article  CAS  Google Scholar 

  46. Z. Zhang, Z.F. Hu, S. Schmauder, B.S. Zhang and Z.Z. Wang, Low cycle Fatigue Properties and Microstructure of P92 Ferritic-Martensitic Steel at Room Temperature and 873 K, Mater Charact, 2019, 157, p 109923.

    Article  CAS  Google Scholar 

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Acknowledgment

This work was performed in support of the U.S. Department of Energy’s Fossil Energy and Carbon Management’s Advanced Energy Materials Research Program and executed through the National Energy Technology Laboratory (NETL) Research & Innovation Center’s Advanced Alloy Development FWP. The authors would like to thank Mr. Argetsinger and Mr. Mendenhall for assistance in melting and Mr. Powell for mechanical testing.

Funding

This project was funded by the U.S. Department of Energy, National Energy Technology Laboratory, in part, through a site support contract. Neither the United States Government nor any agency thereof, nor any of their employees, nor the support contractor, nor any of their employees, makes any warranty, express or implied, or assumes any legal liability or responsibility for the accuracy, completeness, or usefulness of any information, apparatus, product, or process disclosed, or represents that its use would not infringe privately owned rights. Reference herein to any specific commercial product, process, or service by trade name, trademark, manufacturer, or otherwise does not necessarily constitute or imply its endorsement, recommendation, or favoring by the United States Government or any agency thereof. The views and opinions of authors expressed herein do not necessarily state or reflect those of the United States Government or any agency thereof.

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Rozman, K., Hawk, J., Detrois, M. et al. Fatigue Performance of an Improved Creep Strength 10%Cr Steel. J. of Materi Eng and Perform (2025). https://doi.org/10.1007/s11665-025-12180-8

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  • DOI: https://doi.org/10.1007/s11665-025-12180-8

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