Shimadzu GCsolution Chromatography Data System Operation Manual Version 2.0 Read the instruction manual thoroughly before you use the product. Keep this, instruction manual for future reference. @) sHimapzu shimadeu Corporation Anata Instruments Dison Kyoto, JapanCopyright Shimadzu Corporation 2060-2001, All rights are reserved, including those to reproduc this publication or paris ‘here of in ay Tar, without the express writen permission of Shimadzu Compoction, Tnformation in this publication is subject co change without notes and does ot represent commit onthe pat of the vendor, ‘Any eos or omissions Which may have occured inthis publication wil be comexted as soon as possible, but not neces ily immoditely upon detection, ‘Shimadcu Corporation makes no claims or warrany concering dhe influence ofthe application ofthis publication on the ‘operation ofthe machine, ‘Note that Shimadzu doesnot have any obligation conoeming the effects esuling fm the aplication ofthe contents of his manual Shimadz Corporation will cotiaue to supply orignal Shimadzu maintenance pars associated witha given product fora eto upto 10 years from the cessation of production ofthat produc. Please te informed that after this period of time, Shimadzu Corporation cannot gurantee supply of such orginal maint ance pats, However, following discontiauation of a produc, the period of avalabiliy of maintenance pats which have ben produced ona subcontract basis is upto the discretion of the concerned sub-contacting company (Gcsoluion sa trademark of Shimadzu Corporation. DBWAX isa product name of S&W Corporation. Adobe, Acrobat and Acrobat logo are trademark of Adoke Systems Inco: porated Micros isa regsered rademark of Micros Corporation, Meroso Windows™ isa product of Microsoft Corporation.Introduction “Thank you very mach for purchasing the GCsoutionsofivare for Shimadzu ets chromatograph workstations thera called *GCsoluton”, Gcsolution lows you to contol the gas chromatograph (herafier called "GC") from your personal computer, acquire chro rmatograms and other diferent kinds of data, and analyze the scquied data under diferent parameters on Your personal com pute ‘This manual hs been put together inorder to familiarize you withthe basic knowledge required to operate GCsolution, Be sure to read it through before using tis software. Afr reading the manual, kep it in a safe place so that it an be aceessed ‘whenever necessa: The "Functions Volume” ofthe Insist Mansa for GCsoaton for Shimadzu gas chromatograph workstations is atached ‘asan online manval, This manual covers the on-line help information in PDF format tions 07 GCsolution, eer wo de onde manual detailed information on the Re This manual assumes that the reader is knowledgeable of basic operations of WindowsNT(), dows TG), eer to he instucton manual that comes with tht product. the operation of WinItems included in the GCsolution package ‘The GCsohtion product package contains the fllowing items hom name ay | Paras, Remark ‘GCton CD-ROM 1 | 2zxosnss.o2 [Conan tb Gotaion progr andthe smiton mara or ‘GCsoluion (POF sersens of the operons an uncon Yo ‘Opentions Volume of wsmcion | 1 | 225-0066 | Dasenber how tase an analyze dt using GCsaton| aml or GCsiion : sonal compte, ying tht rode etUsing the instruction manual Hi Kinds of instruction manuals Te GCsolaton package contains the folowing information tat describes the ope tional proseires an eters. Name Media Description insricton ane for ‘Expl teoperaoal procedures for dam aequision and analy ing, Gesotton ‘ntne help ‘GCsclion program rwides deed information on paamstes and sting gos. Tis 6 ccs fom the Help men in GCsruton (Fr wing the ine help, inerveton vane for tha an be ewe on Your pesonal cone is acesibe om te Using the Ontine Maral 2 his tsution anal.) “ GCsolution PDF version) Ut te oli lp can be rtd ato rfernced appropiate the pv em the pers volun ef the istucton mal (PDF ver ‘oe manuals (PDF versions) aos you fuse ech nsacton mama ‘a th hyperink (For wing etch instruction mana is the peri, fete ston 112 iin the Ooine Ml p12 hs ton ‘ramal) PHBE Legends for instruction manual This manual uses the fllowing legends For ample [Fi at command mens tat yu shuld eck en the Fue = Nessa @ Gopi = So ww orem =Das Asn nnd == 1 ‘Sones em th cla tres ems coand aa be ot omh ner TiCieonmana Sons see of acting enn et ad ee cleins e nmand e eo T ‘andthe eect the1 What is GCsolution? 14 Features. fe eae 2 Software Overview 21 GCsolution Basics s+. sseseeseseeseseesessesesecseceeseeeeseeteseeneseeeneened) 2.1 GCsotuien Apptons 3 2112 File Types and Daa Expo ile Tate 4 3. Performing an Analysis 34 Starting the - Window 39.1 Taming the GC Sytem OFF 392 Taming he GC Power Of and Extn GCostion 4 Next Step - Data Acquisition 4.1 Operations in the Window 42 Changing the Analysis Stop Time During Analysi 421 Stopping te Anais 422, Changing te Aralysis Stop Time During Anas | {El LabsSolutions/CCsotution erence: iim43° Setting Up GC StartiStop Actions -..ssesecsesessesesteseseseeeeseeneeenees 43. Seng OC Sart Panes 432 Povoming GC Awomatie SrtpShdoun 44° Changing the Data Sampling Interval 441 Paameter Reba o Dat Satin 442 Senge Detector Baw Rat 443 Soting the Dect Samp Rate 48 Performing Dual-Line Analysis ce 451 Changing the Arist Line Oanty "2" 7 452 Seletng Uns or Each Artal Line 2” 453 Pefoming Display and astute Seting fr Each Line 28 454 Analysis Using Dire Signs 28 455° Analyse Using «Dal Aut-Seper » 456° Perfoming Siigle-Line Anais wih 4 Dub ine Contgution 30 46 When the Baseline is Unstable fi 461 Changing Colum i Termpsatue using nstunent arate Stins| 462 Performing Cleanup 463 Pevoming Bank Anas 47 Registering Column Information . 5 _ Next Step - Data Processing S41 Operations in the Window ..0.c.scssseseseceeseeesseseeneneee 38: 52 Data Files Handled in the Window ... 8.10 Operations in the WindwtoCre Bath Tals 0 113 Refoming Bak Procsing es 72 Performing Continuous Post-run Analysis . 1A Displaying Window to Open ach Fes 6 722° Selacing Dita Files Ved ty Clea Bach Tale ss 73 Batch Processing Parameters . 73.1 Senge nection Volum and Mul Icton Counts 6 732 Uning Two Liner to Perf Hatch Ani 6 733 Sotingthe Basle Dats File a 7A Using Real-time Batch Processing to Perform Additional Analysis 7S Using Advanced Batch Processing Functions «.....0..+. 151 erfominga Sytem Check Before Bate Processing o 152. Pefoming a QA/OC Chen Chesk Aer Buch Prose “9 183. Soting Acton tems « 184 Seting User Programs 70 155. Outputing Batch Processing Revs in ASC Format 70 756 Adding Desired Sample ffomrtion 70 1M {NH LbSotutions/GCsotution Reference8 _ Report Functions 81 Printing Data Processing Results. 82 Creating Report Files. 83 Advanced Report File Usage . oe 831 During Dat Acquistion am 832 During Res ime Bach Prcesing 75 333 During rowan Bach Paces 16 84 Example of Report Layout Arrangement 85 Adjusting the Report Layout fae 851 Foting Pe tem Fonts * 352 Adjosig Mull Pit le Ses and Postons 8 853 Placing Pinte on Mlle Paes 70 854 Sotingthe Pgs Size Margin and Or tems 0 855° SetingtheHeodecFouter 0 8.6 Checking the Print Image . 87 Print Information Types -..ssesecseseeseseesesecseseesesecseseeseeeeneetene 9 User Administration 9.4 Reviewing User Administration <2... eas S11 Whats Vcr Adrisistation? 9112 User AdiniseatonAppcaton 9113 User Admiisraton Flow 92 Using the User Administration Function to Set Available ems... +.e+sese+eeeeese+ 93 Logging in and Setting Password Limitations ......c.ssseseseeseseeseeneeeenes 94 Registering (Changing/Deleting) Users 9S Registering (Changing/Deleting) Rights Groups... 9.6 Changing Passwords 9.7 Viewing the User Administration History 10 GLPIGMP Support Functions 10.1 What is GLP/GMP Support Functions? 1011 What sGLPGN? 012 Sccunty Sport Funstns 1013 Avs Ta Suppor Functions 1014 Vaidaon Suppor Farctons 102 Performing System Chechs s.esesseseseesesecseseesesecsereesereeseeeeneees 1021 Pevorming Sytem Checks 1022 After Replacing Conan 103 Performing Program Checks 104 Performing the function check « coe 100 104.1 Procedure fr fncton hee 100 042 Leading he fncton cheek dt peup 10 LabSolutions/GCsolution Reference [ll Vv10S Viewing History Information ......cssssscscsescsesesesesesesseseessesesesess 1OE 105.1 Viewing Progra Star and Fnshtfomaton (OuputWitdow 10 1032 Viewing Method File Updae Information (Aut Tat) tot 11 Operation - Windows 11.1 Displaying Windows and Bars. 108 V1) Window Types Appearing in Program Windows los 11.12 Displaying Aplcaton Windows 16 112 Customizing Windows ..+.+.+.++ see assdtta 1121 Changogibe View Sz 107 1122 Changing he Application Window Display Format lo 1123 Changing he Common Window Dela Format 10 12 Operation - Tables 121 Operating Table Columns see = 109 1211 Selesing Table Column os 1212 Changing tbe Wt ofa Table Column 1 121.3 Changing he Table Column Display Condon Cable Syl Setings (1) ho 122 Operating Table Rows an 1221 Selesinga Tate Row ui 1222 AddinpDeetinga Table Row mn 1223 Changing the Table Row Display Quay (Tale Sie Stings 2)) m2 123 Editing Table Cells. 43 1231 Selsing Malese Celle us 1232 Copying Cuting Pasting Clouring Cll Dts 3 1233 Ersering Values it Cells a3 1234 Collate Entry Aas Funtions (Batch Tables) a4 13 Operation - Files 13.1 Important File Concepts for Operation . cee 1s 131.1 Systm Cofigursin ile is 1312 Method Fie us 1313 Report Format File 6 aia Daa Fie ut TLS teh Fie bs 132. Using Files (1) . ae 9 132.1 CreatngaNen Fle hs 1322 OpeningaFile(}y 20 1323 Seungaile 120 1324 Savnge Fleas Temple ny 1328 Cheokig File History Tfoenaion (1) 1a 133 Managing Fites Effectively. : 12 1221 Whats he Dat Explore! rs 1332 What Pee? 122 1333 Creating New Project Fok) 13 1334 DeletingaProjetFolée 1B 1335 Csiomizing Data Explore Display Dats be \V__ ME LabSotutions/GCsouton Reference iilTSAt HH Uniea Den Gy anton ee coon ea aa tee aaa aeMlIaE: 114 Opeanganiee) es 1342 Copying File ine 1143 Moving Fe 6 144 Delage the 1145 Chang Fi Names 1 BAe Gheling Fe Hist ntomaton iar 1147 Comering ie Fora ir 135 How toSearch Files ..-..-cscesseesseessseessesssecsseessesseesseessseesses DD 181 Usage Vay o ron fr Fe exces we 14 Appendices M1 When Troubles Oce4 «ees eee peetrettfcet 11 HAL Using ep 131 AL Uaig the One Mama im 142 Reinstalling GCsotation 121 Ilig Gian i 1422 Uninaling Calton i M3 iting DAO ay 1424 ing Ado OC Uns ee eae 12S Conetons tad step tc tat 1426 SyromConiguaton Satine i 143 GCsalution specifications 150 144 Error Messages -12 ee Labsotution/GCsotution Reference [Vi‘Vil ME LabSolutions/GCsolution Reference Ts. I Features s2picsonware {Gcsotution runs om Windows, an its advanced security and mul filenames andthe drag & drop funtion, Jing the latest Windows technology task eaures are supported. Ic allows yon to use long A variety of unetions are available dhrough simple operations Assistant ba CGiides you s0 you can easily perform analysis even if you ae a novice tse, Data explorer: Allows yout perfor file management though intuitions operations Batch table wizard Allows you to easily crate a batch table for series of analysis Inadkdtion, other Functions that improve the operability are eectively lid out so that you can make the best use of them. F Retiale GLPIGMP support features Security suppor Provides the proper security fr diverse busines laws through the user ministration Fane Audi tril support ‘Stores al the information on deta acquisition and processing, and manages the updating is ‘00: Validation suppor Provides suppor for hardware, software, and method validation % Compatibie with network environment i-one file structure Has all the dat-related information (analytical conditions and report formats) i the data ‘compound strcture 535- file allowing yout casily perform fle wansmission and data analysis ouside the analysis vem: laboratory using the LAN, ‘This fete is leo wsefil for GLP/GMP file management > Applicable for high-throughput analysis ofa large number of data Aplisable for high-spsd Allows youto acu data ina minima sampling time of mace seal Applicable for analysis of allows yout simultaneously analyz two samples in the dual line configuration, large number of data: ‘The maximum configuration fr analysis suppots 2 ines with 4 detectors, $F rite compatbity ‘Compaibily with CLASS- Allows you to load CLASS-GC1O method files and data files without converting them. {G10 format Compatibility with the AIA Allows you to read and write files in the AIA ANDI format, which is one ofthe international ANDI fora standard data formats, ‘Note: This etre ato tls yon apse ilesin the GCslton format tothe CLASS-GC, Data may be saved in ex format that an be usd on other commercially avaiable software (HilB Labsotutions/CGCsohation Operation liam$F Various functions for identitieation and quantitative processing Avarety of quantitative cal- Supports 6 different caleulation methods, inching the external a intenal standard meth ‘culation methods: oe |A. variety of calibration Supports 7 diferent kinds of calibration curves, including straight Hine, line graph, and cues exponential ealeultion curves. Flexible eeaton of calibre Allows you to manually ad or delete dita in adtion to creating date through series or tion curves batch analysis Algoritim with established Uses the peak integration algorithm ofthe Chromatopac sres. reputation Report format with high Mesibilty “The Microsoft Wonike report format allows yout rete exible custom reports easily and ciently. ee LaPsotutionsGCsolution Operation lm 2. I GCsolution Basics “This software consists of thee applications: “GC Real Time Analysis>, , and 2.1.1 GCsolution Applications Aft installing this software ont your personal comput, the following thee program icons will appear onthe seen ‘Clicking this ion starts an application that i used a ener iste and device etings, to conto instruments ad device, ad to perform single or batch run. (Clicking this icon starts an application that is used to eeadacquied anal- ‘ysis data and to perform calibation carve ereation an data processing. ‘Clicking this icon starts un application that is used o, doing ‘meth file or ate file that ot used for analysis alysis, eit Note: The [GC RealTime Analysis] and [GC Analysis Editor ions rede for the numer of GCs hat are cure connect ‘304 pron cmnputer Fr example, th second GC units icons wil be [GC Ral Time Ansys 2] and (GC Ali tor 2 Note: When anaicr rogram is stated in fl sreen mode he e's program ices wl Beene ivisle, Reeves oF minimize the ‘After contrming thatthe GC unit has been turned ON and initialized, double-click the [GC Real Time Analysis 1 con to call up the screen, The following window will then appear nial, select “Admin scr mame and cick [OK]. {ce the smal aro on height display ats) taser ramet Sect“ Aai ‘Since the pasword ha Bt fon entre soto maerte anything he ‘The application will sa. Note: The and Report Format File ‘Sores report format information such as layouts toe used fr report ous and (extension ="ger") exiled report settings. The window is used on both and sercens LabSolutions/GCsolution Operation [NH 45 . I Starting the “To analyze samples and acquire data using the GC unit, star the “GC Real Time Analysi> aplication. 3.1.1 _ Preparing the Hardware “Rach cola he OC to prove asi gs detectors, ke es, rote eases fr eas “Ten ON the PC and erpberal device (ino will startup) Noto: Formreabout GC uit epration narutions relerto the Users Manual the GC Unit 3.1.2 Starting and Logging in to the Applica- tion of wer umes. Seket“Admin” eis ese (Reference Manual 411) / Mb ver sectings wer rae. e| ‘tok te mall aro onthe ge w dpa a Tat i Ati. [ince the password hs at Boen ene dont ener anhing here “The GC analysis program stats up ae the (Reference Maal p5) Note: Tocther stupa password for an Admin” evel wet ot a6 use) use te User Admiisaion™ window (pa 412 (HilB Labsotutions/CGCsohation Operation liam3.1.3 Setting Unit Conditions Used on the Screen “Sistem Configuration (Reference Maral p17) Chek tem Config ‘aoe For any GC mde er an the GC-2010, dousiesick the GC on, The GC Prop: ey screen sll spear Enter the illaion ior ‘Use [Auto baton atomataly ens ay wi in main om hereon {Congued Mauls} te, excep aut-samee, Wit ‘sing et arow vo delet unused ants om he te ts commication price the GC-2010 4 set pepe the unt cnet 10 the {GC-2010 can be dct sutoacaly ‘Orc al sngs ate compete, chek Set For mor aban colin information wets, for to “7 Regtring Colum information” For ana mete sing mali clames, mfr aston “Amaia Using 2 Lies (jer to °4.3 Anal Using Dual Ato Sampler”) 3.1.4 Operation Example Analysis Conditions ere, the operation low is shown using the flowing sytem evatiguation and each insruments analysis conditions, “+ Analysts Samples -# Dawa Processing Conon, Conngoncets cnt! in than ae used os sta Use the falling parameters to det peaks and pesem dae saps im processing Sandor Spe] Conccaton ea npn porters [mpropanot [20 pm Parner Sei Wa Tisha Taso [00 em [ere TMV [sam aeoot [200 fia [es pa Ase Sa io TaN [Min pera [1009 coun (mA Hciain rca Abie RT ‘Quanitve cele method: Ester standard using prakareas Calton curve: One alivation point oo repeating “Aue-smpler- AOC I Sample etn volume Spiess ection (SPL) “Temperate 200°C Spe lt mend Si (Split 10) Fre ionzaton dtctor (FID) ‘Temperate 20-0 FH Rowe rates mn Aso rts mn Nake oat a in ‘Coplay clunas DEWAN 12mS0s8 mm. umaniee | Lo sim “Ges cranatgraph GC2070 {Calum oven temperate 55°C (min hod). -120C {@rogramming rat: 10Cimin) Palys ine 6a [eet ‘Cari gs He.3 ome. in feed car velay mes ee LapsotutionsGCsolution Operation HN 5. 2 Starting Up the GC “This section explains how to create a new method file and wo st instrument parameters forthe GC and autosampler, as wall 8a method to startup the GC using ial setings hase on the method fk. 3.2.1 Editing Method (Instrument Parameter Settings) - (Reference Manual p57) ‘hick (Redraw) ipay He me rogram dagcn te graph feample parma [lnecton Une Tom: peue] = 200° [Spt ode] ~ Sp [Caer Gs] - [Liner Nelety = 30 emice {spt Ratio) 30 a0) [Tot Flow and (Co ‘umn Flow} will te ecculted tse 00 ‘hes seings. Aller rants se defi rate Se the tine progam for inten ts emp. pesurpurze Hw rae {sien SPL use 7 (lll LabSolutions/GCsolution Operation(ck [Calms oven Gia Rear dapay tester ah fre progam date te graph [Temper] (en 7 {ial temperate) st a wesc ofa ae — ie Enter temperate program stings here Parameters wad etal ep. ald ines min, Progam me Wweimin, Fialtenpertire: 20, Retertion tne: Ti Glick (Dever iL ck (Rear] wo depay the se ow sate program at. the sap ‘anmers wed ere [erpertare] ~ 200°C = [Make-up Faw] = 0a! [12 Flow] ~ $0 min. = r- [aie Flow) = 500 mi? — [St Tine] = 6 min. ™ A ofr paaters use tte oo ‘statues te oan ar u ‘Set ech ow eset ‘vale’ ine ean re ‘When the window. For mor abou new fle reton rer to “13.2 Using Files (0 Note: When dts couston is ofarme, te method ama sve fncin wil bette (asking Youi ew data should oerarte the old dat) and the mest ie da wll be overwiten by new de Iyou watt ws the eed method ile under enather ane without ceting a new metod fle rir to performing dat acqustn, save the eiteé mend under anoter nae by selecting [Save Meth Fl As] inthe [Fe] mera ee LapsotutionsGCsolution Operation ls3.2.2 _ Starting Up the GC ‘GC. worn andotberinsie) — [Tastunent monitor wil awtomateally FES] | mont premier wil be down) | appear Conta [GC System] ON and add ech nscurt, wt fr [GC Stas] angst Read Check manor ‘aloes sting values foreach unit ‘GE wil a op usiog to net parameter wae. Since GC step is conte in dow exe] FTF ano GE samyp has not ben dese order —> temperate —> dette tempore: |_| gaed click [ON] on each nis fe enol may nat start yp o decor may |_| ent ont, sutart ON immediately afer GC sats up. Formore about GC ator when startup. reer 0 "4. Sting Up GC SerSop Asons” 1 despite being corsl stp, [GC Sta] does ne change 0 “Read” or each it sting end marr vale re exces ifr faa he GC se dogons ction to check for problems Pr mon about the GC aldo fiction, fer to “1.2 Perfor Sate Cheeks” 3.2.3 Performing Detector Signal Zero Adjustment and Slope Testing ‘When deste, te instrament monitor can Be hidden. Note: The insrument monier diy can be nriced Hetncendiphyed and Nien wing te {insinment Moir 95) baton onthe wot in esi CY) is Aiation, best farce Inge bassin ‘Use sera bar fo ew pe Drag the spliter © ‘owe rlot agjst mtr eine se Refer “4.1 Operations the - om analysis sat to clicked se Rn) Assistant to plovsan, poses ar i not de The notaved when ew method Hie wee sted, cr alr eng an exsing mth He, [sonata For mor abou chancing te onl time, refer t0°s.2.2 Chane the Anais Sp Tome arin Aas Note: en pein ml a ti atte Sr monte Ait ag er ss ts Sew oe mes Jon one Note: sony pa hen] ton be witcher sorb dar san eprom Using (Pil] = [Open Reference Dat ile, the existing chromatogram dt canbe read a2 “Chomp view ses backs sound (HilB Labsotutions/CGCsohation Operation liam> 3 Performing an Analysis .4 Checking the Analysis Results 3.4.1 _ Starting up - ‘To san - and check the result ofthe data aeauisitio, double-click the data fle inthe that was quired using data sequisiion - - (Reference Manual p57) iets ie bee Stow ie lata Slate! lal elcid le) a fi Pe, ; if cromatogrim ow tea peaks ty doublecking i ata ead into it ie ao check pea eet saree eae “SGC Pontran>~ Data Analpsi> (Reference Manvel pT33) Note: Fr mae aboot operons in GC Psu - view area 3.5.1 Changing Peak Integration Parameters and Performing Data Post- run ‘Urncessry ck esol ween areal vals small peaks are of ecesery an uses Pes (aes hk fo ener sn deste ‘staat to be used for quanta. Methor FAK mode, Nv lsk Tig in] ab Ee nie “S007 for te [in Arcueign fam vate, [Fai o View) mode, diet tea ony ese peat Note: I ot suse with the pak gration ess nd yeu Ws 10 undo eum t [Et mode and eer the peak iepaton parameter and perf pon analy, thei, pen the te dt agin without ving the current, postr ania ast bon ptfmed in Et] ma, the need daa ca be undone 1 the origi ats (Right-click the “Meth view ara to Asay» pop-up meu. thon Sle (Cancel Ei} For mor about al th peokineration parantry, foo Refrnce Manual “15.1 Poa train Paramters and Peak eration pots canoe tet carey, fer Reernce Mana 155 Problems wi nares Pes neration™ 15, [lll LabSolutions/GCsotution Operation Sit. 6 Setting Parameters for Creating Calibra- tion Curves ‘As in the previous setin, ths seston explhins how (0 set up parameters related to quantitation and idenifiestion, in the GC Posirun> ~« view aea, as well as how to create a compound able based on the acquired dt, 3.6.1 Setting Parameters Related to Quantitation and Peak Identifica- tion ‘Dovble-cck vw ae ae] to diplay magia ‘ice Exel Sn AL tor paranaters ‘aeration. For mor hon al the quanttation ean identi parameters, mfr toRefoonce Manvel "18.2 Peo dentin”, “18.3 Qant thon Meta ror mor abo testing for wach anita mesh and gasping, foro“ Quanta Parancter Seige Le LaPsotutionsGCsotution Operation lm 143.6.2 Creating Compound Tables Note Note: ick (Composna tab in Meo ‘nerd asd on the flowing nkrmation aa a Tne | cic Ba mam I=mormer fasetnn [20m Nagy me fatay star —— [rare — fap int [sont “The (Name), Type and Re. Tame] data nse ae requ. Concentration valtes wil te neces for quintiave methods oer than arc normalization, Seung only th ounber of ealvaion pos {ourber tees) wl be necessary. Unless mint stings are esi ar ech compound seings peconmed inthe (Quanto ill atomaveally be ete to ncesary tems with “Deiat” sting Note: When [Est mode scum to [View] sods, poston analysin willsomat cally be perma. However, m9 cl tration curve wat plot, 0 uamtaive real wl be dplayed onthe peak tle sen afer postrun anal ‘The ttn time ales sown above have ben obuined wing the cu ro ays and ean be read nthe [Peak Tal] tab inthe “Ress ‘ew area The op an pane Fron can be uct input de Fo able totale heey preventing any impute, In te fate above, he bl te oer eaanged fr eplrtn. igh the compound able wo dla 8 popup menu, ‘Then slet ublecsphy cndion, Le. displayed rhe and spay ore sng he [Tae Sy) command [Typ is used desigmte an irl standard substance (ISTD) when sing he intra standard asa qunttave method aswel retention tine standard peak when using relate retention time for peak detention, Here since st reads devia 364 kere wd3.6.3. Saving Qualitative Quantitation Parameters and Compound Tables “To perform analysis using the edited data procesing parameters, the edited method is saved asa metho fil, Note: Inthe reviows section a method sore ia a dle i sa proces parser. The mth for the dar file is exported oa method il using [Save Method), ‘Mote: Ths das file alo Been changed ay ile Thee, when xing the CC Pot cree ial ox vwilsprear sng wan svete dts ke Hrs, sce he aad sample acquired dats se aly toduennines methed, the das does not ned to be saved For more abou therelationshipbeween meth files ana fies method refer “5.2 Date Fes Handled the “Daca Anofyi> Window" 13.1 Important Pe Concept fr Operation” ‘Displays dealt meiod He name obser dt aq ‘ioe Deft val (le ame) ‘evs Mota: tn previo sections, since the screen wes ever ei (he file “Alecol ge” ill open ois ers Ith sae filename wed in [Seve Method, se cone wil ecu To solve thi coi, dala box wil pcr slag if ou wat clase eile aed “GC Real Tne Atay sider overwing, Te (Save As] dag box shown hove wil apts Ar saving the file, pron data acyson wth ht mtd by desing and dropping the method eon fo Dum Explore 1 sereen and designate [Sample Type] as (Standard lepine calibration = DL sews ee “Sample Login> (Reference Manval pa? 17 ll LabSolutions/GCsotution Operation SitNoto: Whos GC options suspend or when anther meth is downloade ft downlod the stunt parameters and sta the (6 ellowing the proved described in “5.2 Surin Up se GC”. When asia he procedure described in pesous sets, the instrament parameters for file“Alcool ge do ot peso be changed. ihe GC has been sere nasi can Be stared imme dis Note: If he [Auovncrement] checkbox the “Sample Login window has ben sleet fle mame or he dt is ttemaicaly sighted ar “AloholO2 ge, fthiechchoe har not oe lected th same ile rame(Ncohl00 ged) will be we Whe sng the procedure described in previews ection ifthe ile “Alcool00. geil pen i the - screen even though remains open inte GC Real Tie “Analy eee, hereby causing le cont. I thi cass, «dialog bon Wil apse king if you want fit lose the le ie ‘ avg the method fle apn inthe C4 Post screeno you wana open th ile 8rd any Hoe, since the pron ist chek th clinton curves beaut no sting i quite, th ile i open a aon For more abou operation i the wind, refer to “5.9 Opereton in the Wind ee LabsotutionsGCsotution Operation NN 1s. 8 Analyzing Unknown Samples method that has a calibration curve eeatd for it, analyze an unknown sample in the same manner, and then obtain quantitative resus 3.8.1 Performing Single-run Data Acquisition Use the same procedure described in “4.3 Performing Sigler Anas to perform data acquisition. ‘arly sample an [Wntrown) sare, ‘Use mete with ea ‘tration veto ‘bain quantiatse ‘alesltion ess “Sample Login (Reference Maral pA) “The quamittive calculation results canbe checked inthe post-un analysis program's - Reference Manual p57) a [searanmanmenaal = GC Pontran=— Dat Analgsi> (Reforonce Manual pT3S) 19 [ LabSolutions/GCsotution Operation iii. 9 Turning the GC System Off and Exit the Window ing 1 Tu 3. ig the GC System Off ‘Turn the GC system OFF and contin on the -Tnsument Monitor that the column oven tm petatare has decreased nearly to room temperature and that the gas flow used for analysis, suchas of cari gas, detector gas, and make-up gas, has been med OF, For mor about GC ation stings we when the GE stem i tre OFF, refer to 4.3 Seti Up GC Set 0p Aeon Treiman monior_wil_aaonsticaly ‘Click (Sytem OM || appear Canim [GC Stern] sto OFF 3.9.2, Turning the GC Power Off and Exiting GCsolution TOPE Wl Be sipped. Remuve coluna fram te ‘Once power OFF. saply oF anasis uses 6C.treauies Click (Clos in oppescigh omer af ech open post i ‘snd tei program, ze L “Tum OFF the GC and accompanying devise, a Note: Aer th GC system is uned OFF, wil ke tne to tum OFF the Mow a pss, sch a th carer ge. This tie period wil Window Tile ar, sans infomation, end ‘ipl songs window appears, wing vighe] —[Sstines for [Slope Tex) Information sti dy ting lick mena in =Chromatogran= ew me [ero Adu), (Sea indo ae display “Display Seti» ference Naa p74) ‘hd expand ar ean Reference Marup #41) ‘be ptm er, Tre apie ange Spy rio. Upper acai aid “Ch ator ie ae, lower aes designed nsrunent is de aS Played se tb format Pele mse stings owe fr dat = “ (Reference Manual p57) RTA] > Reference Manual p70 “The slope value is one of he pak itegmionprnters sed to stennine cromatogram peak detection envy Ung {he slope test, nose on he signal ascline ean Reread andthe optimum slope vale casine. -Seting Slope> (Reference Manwal p72) le ek (0) 1 wet tos er Sy tee “The aro adjustment commited i sett he GC and the deta signa tase level iad e0. SHG Reference Manual p70 ‘A temporary data file is ereated with chromatograms obtained ftom the sta of analysis to clicked points, and these chro- smatograms are read into - view area can ony be opened as “read only” and the [Sop Time] dats cannot be changed, “This section explains ow to change the analysis stp ime daring analysis, 4.2.1 Stopping the Analysis ‘While performing a single-run analysis, click the [Stop] ion onthe [Single Run] Assistant Bar. At ‘his poi, chromatogram data sequsition will sop, and a dialog box will appear asking Ifyou wank ‘o sop the GC program, such 3s fr temperature programming, Data obtained before the analysis is ‘oped the wsed for the chromatogram. ‘When performing butch data sequistion, lik the [Stop] icon on the [Batch] Assistant Bar, and a ialog box will appear asking if you want to immediately stop the current batch data sequston (in hick ease, anothor dialog box will ask you want to stop the GC peogeam), oe you want to sop ‘he emie hatch acquisition after the current data acquisition has complete, Note: Click the (if con onthe toot inthe acts window tha ic pay daring ‘ouch dts aequistion, ania sag box wll apa asking I'you want op the caret Batch ows du austin, rif ou wat to op the eae bach data seguston Changing the Analysis Stop Time During Analysis Change Stop Time> (Reference Manual p48) [Dever wd [Sop Tim ie wil be rst Note: Ie st mali time shor than the aol anasto, ta aquisition wl top ea ine and a ‘Aer ht the oniaton window wil come wt sav the ew analysis ino metho, Lab Solutions/GCsolution Operation ME 22. 3 Setting Up GC Start/Stop Actions 4.3.1 Setting GC Start/Stop Parameters Parameters related t stating/stopping the temperature contol and carir gas contol at GC statpishutdown ean he St “To proket the column, er tine tered om string cui gat Ts: oan temperature conte Enter time requied fiom cliching [Syaom (nto stopping tem pene conta Glick hin check bow when suring the GC to tt wp wih Puram used when GC wes lasatopped Ener une sequred from sopping ep ature contol 1 sop 602010 (Reference Mana} bisintaal cia Pinca as Now. ‘Check wheter dato isON when staring up the GC 25 lll LabSolutions/GCsolution Operation litte4.3.2 _ Performing GC Automatic Startup/Shutdown ‘Aer alysis has complete, the GC ean automatically be shut down. fied day. 1 the GC can he are up or shutdown am a speci- “Auto System OF F/ON> (Reference Manual p183) ick Fook [ate Sssten| OFF} cee De | Note: The GCM ony allows automatic sarap. Asante sutiown Sema spond Mote: To perfec auo-shatown stings during atch processing, sti te winlow avaiable to prvest an unexposed accident by snther ly oprtion ado protest aa rom malicious options. ‘Chk (Canes Ll] por-p ‘mona fom tase bar ot fndntera password (Click - [Detector ~ [Base Period, ‘Bascom the thinnest column that could possibly be used, the basi unit of the chromatogram sampling interval is desig- sate, Thal Value | 40 mace (GC-2010) 100 msec (GC-I7A, GC-1 700, GC-H4B:C) (Options — | 4, 8,20, 40,60, 80,100, 200, 00, 1000 mice (GC-2010) 2010 1000 msee (GC-ITA, GC-1700, GC-14B:C) Resom- | Regular capillary analysis, ee “40 wo 80 ase mended Val- | tigh-specd analysis using narow bore column: 4 08 mee, Note: Fry GC me ote than the C2010, ae small than 00 see fr hese ate, he esion fi orale > -tnsirument Parameters> view area [Detector tab [Sampling Rate] ‘The cnomarogram sampling interval is designated based on the column aa analysis conditions Toil Valus_| Systom configuration cach dtacior's base rat ‘Options | fase rate 4to WDmices 1 4020 imes the base rate Base ate 100 oe more mses 110 10 times the base rate ‘Resom- | Analysis using packed column 40 to 480 mee, rmended Val- | Regularcapillary analysis: 4010 160 msec Highspeed analysis using narrow bore column 9 16 msec Note: The sl leet ho designated ampling he lrg he data ile capacity. When the pk wih i large, eco amping rte $F - [Integration] tab - [Wide] ‘This parameter i used to perform chromatogram peak intepration. To detect peak, Sea peak half vale TRevom- | The 1/41 172 of the actual detection peak width isthe standard forthe peak hal value ‘mended Vale | Analysis using packed column Sto 10 mce vues | Regular capillary analysis 0402 mse High-speed analysis using narrow bore column: 0.04 v9 6.2 msee 25 [ll LabSolutions/GCsohution Operation lim4.4.2. Setting the Detector Base Rate ce abl value, refering 10 the commended values in he He Shown on he prev as age | mo - [Detector] Tab (Reference Manual p47) 44.3 _ Setting the Detector [Sampling Rate] (paced ab] Fen hoe te FD} ‘ik Tnsrament Panos detente EI = ‘Reterio recomended ra ae ‘ales in able en pre- =} ows pope a enter sping te ale “Instrument Parameter View - [Detector] Tab (Reference Manual p110) LL LabsotutionsGCsotution Operation lm 25. 5 Performing Dual-Line Analysis GCsolusion supports duane analysis, where two system lines (injection unit > cofuma —> detstr) are {GC unit and synchronous analysis can be performed. 4.5.1 Changing the Analytical Line Quantity to “2” Even when there are two oF more sts of “njston wit > column -> detector, selecting eter singletne or da-line con ‘guration will depend on the physical GC gas piping. Therefor, system configuration canst be performed automaccaly “The numberof analysis lines wil e designated using the following procedure SGC 2M Proper (Reference Manual p22)" u 4.5.2 Selecting Units for Each Analytical Line ‘Seting numberof tins “2° wil espa te for Sem Configuration (Rfrnce Mena 7) | Oss Le 27 MMM LabSolutions/GCsolution Operat4.5.3. Performing Display and Instrument Parameter Settings for Each ‘ise rightclick mena in view a 8) play [Desplay Seuings] window “ (ference Mama page 79) Properoe (eforence Moria page 480) Pero esting scone die cofguratin. (Reference Manual p57) Sols an set instrument parameter foreach spy ie we. ines. [Colum a (Genet are common for Note: Gctoltoncan conta up 13 shannl fr [Attic Line} aed | chal for [Analytical Lie} The chanel | oe [Anaya Lined] is call chamel inthe Analytical Line 1 (FIDI) Nota: To we thc method arbtch processing, this exam let uch Stings(p205) window yp Line ony nee ‘te detector dierent signa can be obsned ly on he ry ie | ie 4.5.5 _ Analysis Using a Dual Auto-Sampler ‘To ffcinly perform analysis of mtiple samples that une the same analysis condos, you ean employ’ method that wes «dual autosampler and to ofthe sae type of cok. In this ase, v0 samples are injected ‘ytical Line] and [Analytical Line2] ave used simultaneously to perform the analysis, he same time, and (Ana= ‘Ener dan bere iw [Deector} bin the “lone! Pence Note “Tose his mato for bch processing. eles batch “Ss (p286) window + [ype] ab [Line & ine 29 [lll LabSolutions/GCsolution Operation4.5.6 Performing Single-Line Analysis with a Dual-Line Configuration ‘To perform analysis only om the analytical line I side witha dual-tine configuration use the following procedure ‘To perform analysis only an the analytical line 2 sid, reverse the settings. lik tis | Analytical Line 1 (FIDIY eck bo. “Tose his metho orth poessing let atch “Stes (298) wind - Typ tb [Line | ss). ‘To wc ony one sutosanpler comes a dhs ine on which analy wile performed, connect to he nail Hine ha es ‘eamsamplr inthe Siem Canraion> (7 Win, (Reference Manual p17) (2) Salct [Ami cal Line] tose for aly, 0) openly doe © Dae snd oe te et ne ooo (a Mars Motel LA LabSolation VC eotution Operation KE 30. 6 When the Baseline is Unstable Immediatoly afer starting the GC, the prviously used analysis samples sill remain in the injcetion nit and columays) Because ofthis, the bascline may hecome unstable or ghost peaks may appear even after anew analysis is performed. In such ‘ease, condoning the GC (including the column) and increasing the temperature for any empl columnn() ate eetive 10 solve the problems, This method ean also he used to remove any samples in the columa(s) when analysis fails de to ineoe- rect sample injection, ee, 4 1 Changing the Column’s Initial Temperature using the Instrument Parameter Settings For example, when te column temperature for analysis is eto SSedeg>C (hold for 3 min.) > 120edeg>C (programming rate: 10-deg>Cimin), change the column intial temperature to its maximum temperature, 120<4eg>C and perform cond tioning, sett emperae pe Cheek te ‘After sli sums stable, Restsk [Down foal Panes) te tam 0 org ewe 10 temperature Po Note: tn dis example th column temperature is changed det. However, you ca al use a GC satay metal where dhe temper tore was changed an sve as acter me nhs es, simply aga op the GC stat eto from the window tothe - [Column] Tab (Reference Manual p43) Note: Be sare orgie the comet column information, reftrng tothe column package’ explanations an ther references. Specie cally bese eno Hength, inner diameter and max. usable temperature or information abs how tach a columa to the GC, fet he Urs Mama forthe GC samen 33 [lll LabSolutions/GCsolution Operation ittLe LapsotutionsGCsotution Operation lm 34. I Operations in the Win- dow ‘Dmg mowe over —Chromat- fame vw are and select lower es chomatogram apy ane, ‘Gee nigh-click mena in wes) trea select [Dsl Stings] window. “Display Seings> (ference Moral pe 175) Properies> ference Mama page #1) “Undo Zoom ops Displays sample intra, 7 Decrees ine sity airing ‘Changes [View ai ode Repmeesing automat cally pertoemed f mode amet tem (eat ‘Te split to cha appr ond Tower deply aren sizes. Upper ara ix “Chromatgran Sow oe ere sR vw Sr and lowersight ie “EMeind> vw ae. Data Anagsie (Reference Manual p15) Copy chromatog daw ‘tpt ar paste ito other Ales asan image Dvblecce ech vie fava ile to. aomate ‘eeween magnified and Dispys peak dtction| str pin yen pint (ob and basting Note: A righchok she mene apron fr ech em is nae na to using the igh shat mm in the view rer th tbs nd spl inforation tea inthe and view ae, Note: One ~ 1 pon the second dt file Note: The Mth view ara show dts roesing paramere in the dt ile, not nh independ tho le ‘+ The Data Only] time progam buon etd in the vow are = [gti] das no exist on and = - [Meth] -[Dat Pressing Params. then ea detection, peak entiation, arte cleultn, or clibration uve cretion wl be permed conssuvely fom data cauisto. 38. ll Labsotutions/CGCsohation © eration iii. 2 Data Files Handled in the Window Daas files ae handled inthe window, data pro- cessing method stored ina datafile suse. This section explains how to Rand the ta ile, based onthe GCsolutons file For more abou the le sachet 11 npartan File Concepts for Opraion 52.1 _Importing/Exporting Methods (On a phase whore data processing conditions are reviewed, the acquired datafile is re-analyzed on the window, or ‘when editing the meth file to perform post-an analysis of other dat files individually, dhe data processing method data (cxcadng the instrument parameters) will overwrite (be imported to) the dat ile method's data. (When multiple standard samples’ data is required as calitration information, a calibration curve cannot be crete from the single dat item’ data analysis) “The Methd import can be performed using [File] - [Load Method] 5.2.2 Import/Export Report Formats ‘When clicking the [Report in Data File] icon on the [Data Analysis} Assistant Bar, datas read into the report format and the Report Generator window appears Here, wen the report format is saved as is ater editing, the report Fema stored inthe datafile wil be updated. Then, save ‘he datafile, andthe updated report format willbe saved inde da ile ‘To perform report format imporvexpon to or Fom the datafile, used [ile] - [Open Report Ferma File] or [Save Format File As}. 5.2.3 Data Rollback Tn he dat ile, the data processing method (ie. the original med wsed fr recording during data acquisition) has been duplicated, aswell a the latest method ta be ete in the view area's peak detection point mar, baseline dis Note: The Fat] made required io ait the ilgetos ine pom, 37, lll LabSolutions/GCsolution Operat5.3.3 _ Setting Integration Time Program Examples ‘When using the integration time program, peaks that cannot he extracted only trom the peak integration parameters ean be extracted through visual operations tocegration Time Program Setup Procedure Temporarily stopping peak detestion) ‘write not essing (Zon ba too aed wile oning on [Time] oo nore program, tale, drag mouse over ve ae, easing rouse ution, This will aoe ally eta on rh ‘Wath dead ime peri, mewn stops once ard then resumes Unnecesary peat such solver peaks il ot Be sete Click (Amz) w a | tie sty AL baston LabSolutions/GCsolution Operation EN 38. 4 Setting Peak Identification Parameters Peak identification refers tothe data processing used to identiya particular aquired peak among the compound peaks in the analysis sample. Usually, pak idemifcation and quantitation are performed simultancousl 5.4.1 Setting Peak Identification Parameters ‘When perfoeming peak idenitication and quantitation, fist enter each substances type, standard retention te, eoncentra- ‘ion, window an tho Import his eats using - (Fle - [Load Matos} “When (tral Sand) is designated as 3 quntiatve tectod and when ternal tard cepocets) ee des aed as [Reference] set [STD & Ref] Note: When performing idenifeation of an intra nant compeind peak, repaniss of the (Metieston Method stings pelea he masimam ars or hia ‘wil auomataly be iene 1 he intra anand comp 5.4.2 Performing Peak Identification See or er or Moa. ee Oe eee automatically “The data processing results canbe checked inthe [Peak Table] in the view ara, LL LabsotutionsGCsolution Operation lm 40. 5 Setting Quantitation Parameters “This section explains how to perform quantitation using each quantitative calculation method For parameter ens fo each quanta caleulaon method. ero “IS Ouanttaton Method, “154 Coliration Cur 5.5.1 _ Setting Quantitation Parameters ‘eto and perform stings Noto: Whew changing the prac ulus late the quantitative caeulaton syd inthe [Quaniaion] ab e[Compoul] wb, lation information tat his Been epee wil ered. Meth changes tha resi epoing a seliaion cure shold ‘bs porfomed inthe [Fl [Loud Method 4}, HRB LabSotutions/CGCsohation Operation ile5.5.2 _ Setting Up a Compound Table Sethe standard values used crete a calibration curve foreach substance, sch a [Name], [ype and [Ret Time Formos obo the bai preparation operations sed incratingclibraton cares, fer to “1.8 Sing Pare for Creating Cali: ioe Cores hk ‘Emer aecosan] [ote das based on guanave cae] Righestik [Compound tle © icompours} || dats toe when|| tation matod. Enter valer fof | dls pop-sp me a, soupig (Name. [Type and Re. Time] Use to" pororn main oting operations or abe Tage Sint f | For hase poration of thle suchas colar dla conition (dopa rn 0" hidden) oF ne adton or dele commerce seusbet ian fort “12 Operation Tabi” Te postean analyse nat done yt can te [Can- cel Ei) to undo ed ‘is [Table Spi] wd ‘te, lay con epey on ‘dion (aphyed or iden) Mote: To cate a now compound table, fist, et pms hare nese fr pk Heian and ution in the [Quatt- to], Const selst he [Compound Tel] nd seth ramets hat are nse) fr pak keno andcal- ion ure erin Note: Exc forthe [Nam Type]. an [Ret Time] parameters, fr parameters tha are dpe wit the [Qunitin] a stings a hat ae not yet een et rst 5 "il, the ana] ws sein aa wl anomaly be se 5.5.3 Saving in (Exporting to) a Method Fi Se Te ee ee eat pe ret peer oe je el Ie a : Ile cee deere sett ata et eat eons cee I cp ee Le LapsotutionsGCsolution Operation la 42. 6 Performing Column Performance Calcu- lations 5.6.1 _ Setting Column Performance Calculation Parameters immer value. For more aba column performance clean sting params, refer Reference Manual “.7 Column Performance Param 5.6.2 Calculating Based on Column Performance Calculation Settings oo eee am se Cet Se ee foes “The data processing results canbe checked on the viw are’ (Peak Table} Note: fie clunn perormance mater valu coma isnt dsptsed onthe Calibration Curve™ cach [Sample Type. | | with check marks wil onpatas QA? Oc tew dau. [crs For epular arais samples ae elas sled no two kinds: nda samples ‘ess. But all spe ype ae se fr OAC setings. Set sed ype bush ble Soke OAUE etetaion uning coer as bne when @ ses of sre ‘ample dna processing ison, oir ‘when bach rossi done Tier Cris valve for ch sonpoun QAO Window - [Criteria] Tab (Reference Manual p$3D) Note: The QA'0C calsutioncan be performed ony wing ham | and channel 4 (Le Lie chan) ean contigo, “Tisclclaon cannot be perromed using chanel 2 and3 when multiple detector ae cones Lie For more aban Q4UQC ctedtion, refer to Rference Mammal “158 Calelaton Meads ee LabsotutionsGCsolution Operation lm 44. 8 Referring to the Variety of Records Used for Data Acqui: n ‘The datafile stores not oly analysis data and ata processing methods, but als a variety of conitions such a system con- ‘guration and instrument parameters used during data acquisition, This data fle ean be ead inthe (Reference Manual p78) Note: The aeration ter in each ui sein re dent ‘alo operation pertemed by ote: = Method vow - [Qasnitatie tb edclicking on he [Sele nfo] bao, 5.8.3 Referring to Status Information ‘Status inocmation display i tbe analysis was performed correctly based on the instrument parameters Note: This inton only vale on he 2010. LL LabsotutionsGCsotution Operation NN 45. 9 Operations in the Window °3 Performing an Anais intodces the procedure to crete a calibration curve while acquiring data in the seen, This section here describes how to cate a calibration curve using the window, ‘Secer calioe eure Seaihes Between View] an theme between aged and | | type (eompound or up) [Ed) method mages. Who tnd calbron ire 10 switching fom [View] © iso: [Edu autatcally pox ‘Use spite to change diphyrati. Rght ara SS vow ea upper et area cabietan Cure sew (graph, Ira nner ses, etal of ower tt fie te cba fle ee> iw ate and igh alfa view arc. “ (Reference Manual p20) ‘nk gata fle te 0 a {as eaten po. rely fue len =Date Fie Tee view ar, Note: Besides the rightclick honsut mon in he vie th an appropri ighlick sotto is also vale in the view area (fr each graph aca information aca ele ae. ané on the ad Methnd> vow setae Note: tn the Data File Tree vw se, dt ed or rating clan caves wil dnp Fr cack clan carve level. The calito curve level utes comespond concent numbers 110 16in the compound uble wed to designe he snared sample concen. Note: Bich post-run analysis 59 can alo be used create calibration curv inthe “GC Poseurs To repel © altraion carve “Selet combination of clibation select (Ste itz Cale aton Cure] sf reat ea cron clibain cis, 47 {NB LabSotutions/CGCsohation Operation im. 10 Operations in the Window To close dspny dn, we Habcck mom of eaten, fver area it Pe “able> ew ars. Displays information on curently ewe ceo netgrm pele Dat Comparison> (Reference Manual p235) + Example of upper-lower shit (ase the sme procedure for left-right shit) [Chvomogran wil then shit or srged iste. [cick [Base Poin) wo sect base poe Click [Seale Up] [Seale Down), [Cheomatgram wil hen steam ict or dmgeed stance (A mes) ee LapsotutionsGCsolution Operation NN 4s. I Setting Quantitation Parameters - Nor- malization Method ‘This section explains how to st the parameters required to perform quantitation wsing one of these quantitative methods: ‘Awa Nommalization, Comeeted Area Normalization, of Correct Area Normalization with Seale Factor 6.1.1 Setting Quantitation Parameters Select quan method. ere, Cor reed Area Noma ‘anton selected) ‘Select ster pa toto oak hight te for guamtiaten, Ener“ fr Aron Normalan and Comsced. Arca Normalization, Enter sede fcior ert to ie for Comected ‘Ars Normalization with Sele Far For more about guawtatve metho, rer 1 Reference Manual “15.3 Quan Meso 6.1.2 _ Setting Compound Tables Enter the standard (values) foreach com- a [ponent that wil be usd to erate the cali= eases ‘ration curve on the compound able ‘Afte all settings have been completed, eae ee ‘0 ener [View] mode. Dat will then auto smatcally be re-analyzed based on the dat processing parameters st inthe view area, 49, [NN LabSottions/CGCsolution ieee. 2 Setting Quantitation Parameters - Exter- nal Standard Method ‘This section explains how to set the parameter required to perform quantitation using Fxtemal Standard asthe quantiative method 6.2.1 tative etd. er stort Send sele) tenor po eihtto ‘ner mor ofa tration level [0 oF Cab Love) I For more about quaniuatve method, fr Reference Manual “15.3 Quamaion Meso” Formore aban the ype afealraion cures. feo Reference Manual 15 4 Calibration Ore For mor abou wigting meth rf to Reeonce Manuel “153 Quanta Meth 62.2 Setting Compound Tables Enter the standard (vss) foe cach som- pone har wl be wed ce he a beatin carve Note: Quustistion can be permed wing roared manda samples for each compound He, prfor the eins forthe number of prepared standard Samples. Fo he conection values ‘of compouns tht ae not nlaed in samples to be quntiated, press the {Delete key onthe yhoo nr oc sea Wane 38a SE meg cc UL LabSolutions/GCsolution Operation [NE 50. 3 Setting Quantitation Parameters - Inter- nal Standard Method ‘This section explains a method to set parameters required to perform quaniation ting Internal Standard a a quantitative method ‘eles deed qu tive meted (Cer, et Stn. ord soled) Sect citr pal sono pak height bration levels fr oF Cali Lev % ar ture. stkel [eure ri Teh ener concen ni owe for gun ive aes, es he elvan foeftly yes tvagh Zoo pet Enter weighing | ‘method vee For mare about yunttaive metas, fer w Reference Mawel 183 Quainin Meso oro abou te pe ofcaliraton curs. fer Reference Mama “184 Calibration Cure For mor abou waging meth refer to Reference Monel “153 Quanta Meta 6.3.2 Setting Compound Tables Here, how to set compound table dais explained sing quaniation of the following compounds ‘sing the Inter Standard method as.an example CComp.A- lateral standard component Comp B:Quuniaed using Comp. A Comp C-Intemal standard component Comp D:Quanttated using Comp, C As ‘Seteampound Type} ws or ISTD] or [STD & Rete Se stun sampls ino stone {atoms sandr component. seatings have boon completed, click the [iew Mode] ee ptm to etum wo [View]. istD:intnal Sand emponcnt ose 1 IStD & Refencrnemal Standard Sroteee pee Bet the ae ar [ISTD proup ells fo com ound to be guna and Inca sanded component tour forguaniation. Note: Muli intra standard components con be signed. 51, [ll Lxbotutions/CGCsohation Operation illMote: A peak which ype [STD Reference] ao be ws a referee pes when ning ative etetion tines pk elif ‘on med Note: Quinton canbe pr Tormed using prepared standard samples for cach compound. Here pelo the sotings for [pare the number of prepered mic oe $e priieenaty oe si om gone Joey en ete nt ick (Com pound], Kale! Wal = ‘wen preparing 3 standin sums wo quate he 3 compound, eer (Not ‘sed for conceiraton alae compounds ot isle emer samp ‘etn known sump IST tour (eral standard coped aunt by flowing the step below. + te toi sean ‘Set the unknown sample’ ISTD nour (terial sedan cane ‘omen mound in the «Sane ng winow’s STD ‘Amount AI} (See Refreme Mana page 146. ‘Wen sing mpl ira standid comporent, ht lic the [ISTD Amount #1] Fskt te display the ISD ‘Amount> window (See Refer nce Maal page 292). Then See multiple teal standard component amount in a in When pefring ath Bch Table> wind’ STD. ‘Am column (Ste Refrene Nana page 285) (Oaly when the sample ge is et 10 {Unknown wal the somngs come efste, I te same type is ef [Sard the ‘ctmpound ble’ scene acs ‘wal be Wied and the vale od here wil be ignore, LA LabSolationNC olution Operation KE 5253. MM LabSolutions/GCsolution Operat . 4 Setting Quantitation Parameters - Stan- dard Addition Method ‘This seeton desribes how to st parameters required to perform quantitation using Standard Adkition asthe quantitative method 6.4.1 Setting Quantitation Parameters ‘Since an unspiked simple also considered @ ‘pikedsample. ep, “1 une sample 2 Siren andar sampler = 3 cation a For more about qanttatve mathocs, for to Reference Mom “15.3 Quamin Men 6.4.2 Setting Compound Tables ‘The Standard Addition requires to set the standard sample's [Cone 1] to wnspike sample Inthe example below; st the parame ‘ern the compound table shown inthe righside figure, Cove. 1: Unspiked sample Cope. 2 Spiked sample of 100 ppm Cove. 3 Spiked sample of 200 ppmn 1a) 20 ae tesaea tad sea. aiAdat fe deere acleccete ‘To create calibration curve, est, stall unspked and spiked samples [Typ] to [Standard] and use the method fle saved ia {he setin shove fo pec data acquisition to use existing data, perf pos-man hatch processing). Aer tat, wse the sethod file storing this calibration eurve to change unspiked sample [Type] to [Unknown Sample] and perform postun alysis, A quantitative calelation result can then be obtained, Note: To prirm pst ans hanging he spe [Type sgn it when peoing pos-un bach processing. 5 Setting Quantitation Parameters - Man- ual RF Method ere, a method is described to manually ener fators to perform quantitation. This method is used to perform quantitation ‘sing Corrected Area Normalization when each compounds sensitivity actor fealeady known, 6.5.1 Setting Quantitation Parameters tate method (lee, Conectd Isselesed) ‘eect iter peak ono peak bight te for gutta Set (Curve Fu Type) ‘o (Manual KF), nr sonsetnton ie Torque For more about quanta methods. refer 1 Reference Namal sales. “15.3 Quan Meso 6.5.2 Setting Compound Tables Enter the standard (values) for exch component ‘hat wil be used to erate the calibration curve on the compound table. ‘Afr all setings have been completed, click the ee SEY sn ‘age. Data will hen automatically be reanalyzed teased onthe data processing parameters set i the Method view area. ick (Com mtr fete ie each cam rus [RF] na (VO) cle For data setings required fr other items inthe compound table use the same procedure as used for other quantitative meth- ods Note: Enter the Coeced Area Normalization’ sev et ia he [RE] calunn. Aso, whe sg teal Sandal sd ake Standard methods, et he lope vals the [RF] ohn snd Yoerop tr ia the [¥()] elu. Facto of second ot mar precision canot be entered LL LaPsotutionsGCsotution Operation lm s4. 6 Setting Quantitation Parameters - Expo- nential Method ‘This section explains the important stings required when performing quantitation using the Exponential Function. ‘This method is used for quantitation where simple concentration and sensivity values ae not proportional, such a Saetec- ‘ion using a Mame photometric detector (FPD), 6.6.1 _ Setting Quantitation Parameters For more abou! quanative mets, fer to Referee Mana unianve vals “15.3 Quan Md 6.6.2 Setting Compound Tables Enter the standard (alues) foreach component that will be used to crete the calibration curve on ‘he compound table. ‘Aer all stings have Been completed, click the et SEB om mode. For data settings required forthe compound table's cotter items, use the same procedure as used for other quanstarve methods. Note: Aner creating calivaton carve with the [Curve Fi Type] desis [Exponent the graph Asay in he Calibration Carve wind wlchange to sta! ognthmie dl: 35 [Nl Labsotutions/CGCsohation © eration iil. 7 Setting Quantitation Parameters When “Grouping” Similar types compounds, suchas homologues and isomers, can be grouped for which the contents can be obtained. This method is called “grouping” Grouping is efccive w use when you ar casing al he peaks 1 perform quantitative calculation for each group, and ‘when collating all impurities contained i amin component into one group to measure is total amount, “The section explains how ose the parameters required to perform quantitation using grouping, 1 Setting Quantitation Parameters When “Grouping” ‘Sols dosed Gua tative meth ce me Fit Typel. (of Calis, Levee, and sere needed for Selected quantita: tive method [ere Exteal Stand sete) For more abou guaniativ mtb, fr to Reference Moma “5.4 Quantaton eta Note: Two options areal othe “rowing” cing: ‘ou Calvan ‘Quuetiston 1 pertormed creat callvation curve fr cash group by tli he grouped campouns pak ara ope Tenth vas ConcetatonStermation ‘Afr retng weal crv nd petering cuamaion far cach compound. the grouped compound conection val ‘esr taeda the rons conenration ale Note: When performing group calito, the sme concton cr kd ll groped compounds. Therefor, te compound t= ection cr ae val differen fm ech cher the group elitionretod eat he wed ee LabsoutionsGCsolution Operation NN ss6.7.2__ Creating Compound Tables Faso on the select quantitative method, eter cuseieicos ae ce the folloring parameters ito cach component rend ‘WD oe field of the compound table ‘Also, wien using grouping, enter the same [Group 1D #) forall compounds to be prouped inthe com pound ble. I [eg — Ton Inthis example, omp.A and Comp B are grouped 18 Group 1D #1, and Comp.C and Comp.D are srouped as Group ID #2 Note: When perfrming soup callraon whee aibaton ce ics fo ach rou, he cncantatin velass o ot od to be need te Compound Table» window. 6.7.3 Creating Group Tables ‘Afte ll settings have been completed, click the [View He ‘hen automatically be reanalyzed based on the data process: {ng paramcters stn the view ae. Clik (Group) wb Note: When using (Cons, Summation, Whee the of lth srouped compounds eoecenration ales i used as the {0 cancion vals, conentton vale do not need be entered in the [Crop Table] widow. Ter at group ane [Goapele [Name cola foreaeh (Group D Tre tunis amgio sn otation vale for eek eroun 6.7.4 m Note: listing Se (Graup 1D rth desired Math view ara ean alo be wed odes soup me 57, [lll LabSolutions/GCsolution Operation,6.7.5 __ Checking Quantitation Results for Each Group Check omit m Le LabsotutionsGCsolution Operation lm sx. I Performing Continuous Data Acquisi- tion ‘To perform continuous data acquisition for multiple samples, use the Batch Table> on the Window to Create Batch Tables acc ow clats wo one das aeqltia(igle-an ays), Ear nse- ssa values ineach bth ow sch as (Metbed Fi] and [Da Fil] nes ‘fer iting lsh ode st Select neces et ing commands fom abel men, ‘ines di le name atolls eg, no eed ener Can automatically er sie datafile name, 59 ( LabSolutions/GCsolution OperatCreating Batch Tables Using the Wizard - (Reference Manual p283) nt method ie Click [Next 1 go w next page ‘When dove, ik ih ‘When au le ae ere avn finton selected, file ame anaot be eo tat cl “Input Col Data.» (Reference Manual p275) ‘Selig (lpat Co. Dat) om ighclck mer Aislays.a window one Col infrmation all at nce, Can use this for [Vial [Sample Name], [Sample and (Dot Fae] tems Note: Shimadins coneational chromatogram das processing software (CLASS-GC'0 includes unten equivalent thi sotare’s ‘ch processing fection, With his finetbn, te some vias sample inestion tepeiton can be stn ch rows This ova, however eles one ime spl ijstion pr ro Therefor, bth os wl be retod a et fr the br of warp n= ton epetiions. When spe jest ipl ins rom the sme vis se the Inpat Col, Dat> wie il rmbt cry fancton rate bleeding copy and parte) faction perfor enser dat setnge. Absa whes wing he bach bl wie st ssening sample jection ection, maple ba ows ea automat be cet the sme Vi LL LabsotutionsGCsotution Operation NN 6061 “Sample Type> Reference Manual p291) ‘When sample pei [Stender sel (lie Calbaion Curve] for ina nde sample select (Ald Calibration eval] fr the flown Sadatd smpes ‘Use [Save Bch As Template. command in (Fe) mer to sae Bach ile tempos eabling ase {iN LabSotutions/GCsotution Operation [ite7.1.3 Performing Batch Processing ‘Aller the batch table settings have been completed, perform batch processing, Mena and totbar tors vary depending on sect! window, i, Butch Tble> or “Dats Acquistion” Displays te da for ostion ty ne parmsersia rw {Table 6 Window to Open Batch Files Bash ae ‘lick (Open) to esate Bate be wing slot ta fle sample Note: Dragging and droping dis ino theft ble can ao be used a anew bach row toch ea of te ale 63. [B LabSotutions/CGCsohation Operation iilMote: Ifthe cure! dt ile name infirmation sdf rr tht od in he dt il the fleas Bon e-em) the crent ua irae wil be ctr in he ath le ‘Using he [Save Bate As Temple. command inthe [Pile] menu, you can sve your own tach eas & template, enabling you to use agin note tine ‘ostanbtc processing usc method th than ‘hat saved in ta, digated by bch able Displays the da for Note: Toctisinguish rom ch processng performed using dts cguston. which 1s describ previously butch processing described er is sometimes aed “potsun buch processing” (Tis uncon sequivalent a uncon called “atch cheer” with Shad cnventinal chmatogram ts poses Ing prot) Displays metho ke sox pasion Note: tems cosine in hte les dsplye onthe G1 Real Tine AnassAnassis ior ard seen aa the same, Bocas of this te Ste tings uid ors ral ime atch can aloe wed fs postu cha i However, when lpn lesen postr atch he lion ters tht ar elated to the OC wll not be played. Als when ts ile at has sen reac 8 posta Bach He, an may ack le, eer he de vues ce noc entered the Following ems To user this ea an says bath ie, the file in he “Bach Tale» wind the GC Rea Tie Analy Anais Eko src ems: Vial, Ijction Volume, Ml, Sytem Check, User Pram bi dit gus tion Note: tn analysis uch ile whee [ren lene automaticly with] has ben designate, on automatically creed di fe nme ‘wl be entered mothe abe'sappicabl cl fr ac elem processing, Decne: the da ie mares ein reed m0- ‘ails, when priming posta te prcesing wing analyse batch he, this processing i performed or i seied fom the prevous caine buch procesing To prim pst bteh processing forthe obtained da ay ine us lite fnction tse ananassae under a ferent ame ach med i acqed. Cerise, Bessa ach OSE information asus when dats a proces oon sv thd il, st shee om hs cd file teh fle wsing - [Tol - Save Batch in Dt File As. ee LabsotutionsGCsolution Operation NN 64. 3 Batch Processing Parameters In ation to single-n parameters, the Following parameters can be set fr batch table ros Parameter Deseripion Method ile name For batch processing, a method filet use forse ime aalysikpostrun analysis is dsig- ‘ated for cach row. For post tun batch processing, the designted method file imported to the data ile’ intemal method are. ‘Sample Type “This item i also ove of the singl-ma seings. To change the sample type For postu ‘eernce Nomatp29ty | Sa processing se the batch tbls funtion Injection Volume For singl-ran analysis these ems ae included in a method. Ina batch tle, a seting Mulitn. ‘method canbe selected. Rafrnce Monae (p27) Run Mode Detaled run method canbe se, For example i data acquisition or data processing is pe srencs Nomaipcoo) | Foe on invita rowsin the ate ae Syste Check ‘Can be activated for each row. (This is not displayed in the window.) The system check Terme omaipray | tlscan be wsed Tor eonalling the progress ofthe bach processing, ‘User Program Extemal program run that can be desigated before and after batch ow runs (Gor postan erence Monatp29s) | atch afer batch ow ru. ‘Action Batch progress contol stings can be entered based on she QA/0C serings (oe page #4) erence Nomaipovsy | MESS check esl. Option ‘Sample infomation in alton to dhe sample name and samp 1D ean be added Refrence Maraaip 302) ‘The desired column te mame is nt displayed select [Table Sey] fam a ighelick menu ods it fo move ien4s) up oF down Uloftorsigh nthe ble) Fon can sn hechangod Points: + Display only the necessary items. + tems with a higher reference fhe- queney are in order from the left (You can see these items without using the sero bar) + Reduce the font size and cell width asmuch as possible “Table Stle> (Reference Manual 446) Note: ‘Sine uch able’ sie sting daa save ns tach ls da can eee and sve So that wil easy Lo We ae operations 65. Ml) LabSolutions/GCsolution Operation7.3.1__ Setting the Injection Volume and Multi-Injection Counts Set the sample injection volume a mult-injetion counts ina batch table using the following procedure Note: The mato fi's sample ijotion Ylune and muiioe- ——_ (Reference Manual 296) to suns wil eased as eu ac, (Click the [Settings] icon on the [Batch Analysis) Bach Table} Assistant Bar call up the [Settings] window. 2x Select he [Type ab. 3. Remove the check mark from the [Use Method Inj. Vol- ume & Muli-n, Counts) check tox. 4. Chek (OK), J. The display condition (displayed or hidden) for injection volume and mult-injection items canbe selected using the batch table syle stings Noto: Suing inthe “Seng window ae stored fr ech batch ‘le. your bora) roubely uses bach abe sings fo ‘tes such as bijection vom iu save that batch wth its registered otings tempat 7.3.2 Using Two Lines to Perform Batch Analysis Paro ain th cen wih oct yang salient wih onan the vind, T.- Cisk [sri cn on he Bach Anyi} Bash Seng (Rfrnee Manual “nen areal up he [Snigy] wd. rs 2x Select he [Type ab. 3. Setoct [Line 1 & Line2], Noto: Tis eton wil appear dimmed i theron ystem com Tiguan has not Keen Set ap, and indises you cent select it Note: If secctng [Line 2) only Line 2 wil be wed to perform ch processing Note: The Batch Table Win cana tr this sting, ‘When selecting batch processing that uses two ies, the hatch table rows number display will change toa [Row number + ‘Line aumber) format, je *I-1", 1-2", 92-1", 92-2", and data eit and processing will be performed Wo rows at a ime (Gynehronous sta, Le LabsotutionsGCsolution Operation NN 65Noto: Sine dus eis willbe performed ro ine you se the [ier Row] faneton two Rew ros willbe seed between ‘eect aio 99. To we the [Delete Row} func, you mast sel vo coret ws a8 ap To perio tse operations “nats chose [Sess Ro] fm righ mem extn the crn ow inet ice the new comet air af 08, Note: The following tte ble items have setingimitinsFor both nes (ots eas wo rows or or Line 2. + Linkin far bot ‘Sample type. method ie vel system check, sr program. acto, + Limitation rine 2 ony ‘unde ony [races] - [Dat Acquistion] aed [Dam Processing] can be wed sess mode) 7.3.3 Setting the Baseline Data File ‘A~bascline data fie” data called “background chromatogram’ or “differential chromatogram. These chromatograms are suburacted fom the targeted chromatogram during data processing. This is used to remove blank peaks as well s any com- ‘ponents that deviate from the baseline in. porticular patra, asm be acquired tire ing basting ea Dore} DewO1_o026co DEwoi_0036c0 ‘DEWO-004GCO. ‘BASELINED32.6C0 —r LesseLNE p22 Gcp_} “To process data with only one reabtime batch processing rns the parameters so tha the baseline data will be acquired ina batch mow oe the row whe the baseline dita is bins used, In this case, since only chromatogram datas required far the hase- line da, se the parameters so hat data processing will na be pe= formed in Ran mode to eliminate any unnecessary processing sh as report output - Reference Manual p290) Note: Inston the tretors hve, the loving fonctions ae als stable Kan mode + Muss pstran bate 046) iat a celsine tate "> Emr hissing oly fer data prooesing 67 [NB Labsotutions/CGCsohation Operation ile. 4 Using Real-time Batch Processing to Perform Additional Analysis Another rea ime batch processing ask can be added toa hatch queve during the eurent real-time batch processing. ‘Aor performing the most recent real-time batch processing, reabtime batch processing on the existing atch Mes repistred inthe bate queue willbe performed consecutively in reese tion ode. ‘Analysis batch processing om the items inthe Hist wil be pot Teme from the top- Once an item's processing hens i will he erased rom th is ‘You can ado delete ay batch ie rom te bach queue, ad chang he proces rr Batch Qucus> (Reference Manual p28) Note: Aes ingle ren anaysis ich hats isto in the gac wil not be ptm Note: such quewseiags wl be erased when you ex he GC RealTime Atlys> applet, Note: Tadd batch ow tothe uret bth wb clk the [Puss ion onthe Assist Ba Tn he pase bath be then, dl, ad eit fnctions canbe sedan bath ows whose data processing i puso. To resume resing otha aes, ek the {Patel icon agar Note: Ifa hc incompletely topped wing the [St] con os he Asia ar nthe raed fam hello batch om amo ‘he information wl cea, sch tthe QA\QC Functions eter checking, There, some ations may ie re hone resent when sing [ae ee LapsoutionsGCsolution Operation HN 6suty Using Advanced Batch Processing Functions 1 Performing a System Check Before Batch Processing ‘When performing real-time batch processing, the [System Check] funeton ean be performed for each batch sow. [System Check] will be performed immediately bers data in the batch row with this aneton designated is processed ‘This stem check fonction i the same as that aetvated fom the menu - Instrument] - [System Check] «System Check window (se Reference Manual page 148). However, aly the consumables check, GC check nd system hhck esl printing satus ean be set hee * Ucthe window t poor the dtd stings, ‘The system check will not affect batch processing progress at all when criteria checking is not selected with [Action] (eseribed ater. 1 2 Performing a QA/QC Criteria Check After Batch Processing ‘The QA/QC function will perform statistical processing on a sris of analysis sults and other pressing. This function is only available with batch processing. ‘Sethe anpmprite section of Bference Mamual 9 104 Sched Action Window” Use the [Batch Analysis/[Postrun Batch Analysis] Assistant Bars [Settings] icon - [Settings] window - [QAQC] tab to set the use ofthe QA/QC fanction (ie, wed or nt used), QAVQC fet output fle mame nd ile overritmerge conditions. Noto: Alo pefoms the QAQC enter checking coin seins for the met tng. Note: Using the Q4.QC enter coon stings he QA/QC cleo timing ane etd fom cher thet wena of ential sample ype daa processing rise rhe tie the bach comple. (> Ref: Q40C seringstsing parameter xe 75.3 Setting Action Items rom the batch ble’ [Action settings, batch progress contol (stop/pause) and exteral program startup performed based ‘on QUOC or system chock ertera checking results can be st. * The Actin] stings canbe perfomed independ fom he er roar ens ee ae). See she appropriate section of ference Manual °9 104 Schade Aston” Widow” 9104 ~ser Program’ Wiad Note: when checking crea tom the QA'QC rests, click the (Execte QA/QC} check Box onthe (Bath Analysis [Beh Tae) ‘Asis Bars (Seung) ior - [Sens] window -[QAQC] Wh. Aba, when checking eter om the sem check el, select the system check fncton for ach avs. Sem check can only be pred when el-me bach rocesing Is per= forms) Note: Re avarths,i7QAQC saleulaton or syn chk seo heck era snot son up ach ow what ation stings ave alo hoe eterd th res the ete checking wil Be"No Er paseo) Note: Ifstetingan exceral progam here nirmatio sucha dita il eame cast be Sent the ropa. To dos, plintay st ings requ sucha specifi the le name to 69 (HN LabSotutions/GCsohution Operation lim7.5.4 _ Setting User Programs ‘A program wo be stared here snd afer batch ro run can be entered int batch row’ [User Progen) el, ‘Sev he eppprite section of Bence Maal °9104 User Prgram> Window ‘The to kinds of user programs below ean be stared separately fom an external program started based onthe previously [ASCH Cant} Tab (On he [Batch Analysis}[Bateh Table] Assistant Bar [Set] fen -[Setings] window - [ASCH Convert] tab, set the ations ‘to porormed when outputing batch processing results ia ext Format, @D When saving» batch able using [Fike Typel- fei, the batch whke will be saved intext forma, This tent ta can aso be rend in, 7.5.6 Adding Desired Samp! Information “The [Option |] to [Option 5] fieks, which are usually invisible on the window, can be used to add sample information, ination to [Sample Name] and [Sample ID], Up wo 3 charatersean be entered ino ech il, which wil be stored in a daa fle when analysis is performed. Each option item canbe renamed on the [Batch Anatyss)[Batch Table] Assistant Bars ~ [Se] icon - [Settings] window ~ {Option} ab, Note @® ‘Nong th sump name and sample I, thee opin tem can used sh esearch Keys {Upto 63 characters cane entered into he [Semple Nome] ed and up o 3 careers cn be etre ito the [Sample ID) el ‘Sw he appropiate section of Reference Manual “91.7 [Option ems Ta LL LabsotutionsGCsotution Operation lm 70. I Printing Data Processing Results “To call up the Data Anaysis> window, cick the Assistant Bars ion and drag-and-drop the desired data file ‘om to open the file “Report (Reference Monuap303) Use te Following procedure to prin the report for that datafile. Data reports with ested formats will heeded, while data roports withoureistered formats will e newly created + Inboth aes the por frat wl be payed with dt in, ‘After pasting or editing the desired appropriate pint item(s), click the Assistant Bars [Print] icon o output the data alysis result report ‘You can use a report format tomplateto easily perform report outpu. nth eas, data wil also be read inthe report. Thore- ‘ore, when sing template to ereate a report, the data analysis results ean be printed immediatly * The rents can leo ait or 71, {NB LabSotutions/CGCsohation Operation illFile New (Reference Manual p #54) Perform a print peeviw fo the ‘soba. ‘Select [Seve Format as Template] in [Fe] mena 10 sve your own report Tonal 36 temple, lowing Te pas When sng atom le a rpot il fama (70) with [Save Format Fle As). ican be used for da {eubtlon and bach processing Note: The ved format wile refed data le tht hsbc ed int mor, Save the format cpl ave sd le, @D Output» report fora data ile using repor file use the folowing prosedare LL LapsotutionsGCsolution Operation lm 72. 2 Creating Report Files Inaction tothe method describod inthe previous scion, the following methods can also be used to crete a report ile (Cliche (Report) icon onthe Main Assistant Bart + (Ror Genero cn abo Be arte inthe GC Real Time ArayieAnays Baio sce, I th ex, tat thy sling [Repo ‘Geno te Window mn, A report format template can be used rete a report file Seles [New] bate net epee Distal S103 [2 ‘The eport ile will be saved ater elting Select [Save Format as Template] nthe Fil] mena sve yoar own report format a @ tempat, awn Dou toe fo fe pits 73. [El Labsotutions/CGCsohation Operation iil. 3 Advanced Report File Usage Using “Report Generator, besides reading and printing dat file, the ereated report file cn also be used for the following ata processing operations. 8.3.1 During Data Acquisition Post-ta processing report output after data acquisition ao ao | Aras ings + Mets ie Sample Login a - Reference Manual 140) Le LaPsotutionsGCsotution Operation lm 748.3.2 During Real-time Batch Processing ‘Report out afer each analysis bate row ran, wl c SD A) sents Real Tine ira ase ‘ral lick cick borer Metin ie ‘Sestings in Batch Table Wizard> window Pe tne vara ese opr fi ‘Toutputal ofthe reports ‘Remove all [Process] item check marks in the Pesan ‘Amis Reporle Note: The wis function and Run made cannot be sels nthe postin Bae able LL LabsotutionsGCsotution Operation lm 75. 4 Example of Report Layout Arrangement Chick and dag mouse ‘lagonally where a pre fon al pasted. So tu window whenever the item is pasted Here, you can edit format information, inching the ‘rit item's corre size and position, Use a fomson of "Adhating Msliple Print om Sizes amd SS Portions (dsb later) 1 nly lin lip prin ions {2s and pstion with ech ther andi yond nt repre om recs D —_Pretellowing sce wis re equi wo pint each tas ein itm using the standard Font and size Ties New Roman, mm Piiten aan eeara [Bfpsencesvaion | Axon smn [ Bolsa ‘Ao 10 man pnd he ng ng isang ane) [Taf ‘Apo 70m te who Ati shes FJ) Peak Table “Approx. 140 mm = ‘Apo 60 a i oda ass anda) [ Blower tote tse pp 1 [ezine cine ‘AoE 10 ina wh Se awit Heder norman) [ Be sesrncmaon ‘ppt 18 wn LabSolutions/GCsolution Operation [NN 788.5.2 Adjusting Multiple Print Item Sizes and Positions 1fno print tems have bec selected, then drag the mouse to enclose mule print items. Those print tems will hen Be selected, Clicking mutple pint items while holding down the [Shi] key canbe used to select multiple pit items ‘Once multiple pin items are selected, they can be dragge and moved simultaneously, making it very easy 10 create a well ranged report format asing the following layout menus Also, print item display layers an be changed inthe [Layout] menu Layout Menu Function mitt Moves and aligns the lel sdes of select! rit ters with each oer. | 3a] sicwrcane ‘Moves and align the right sides of elec print items with each oh, Moves and aligns the tops of selected pint items with each othe. | BB stientoon ‘Moves and aligns the bots of seleted print items with each eter Sa ‘Align the wis of elected pret items with each oben. [EB ss Same Sizeteight Aligns the heights of selected print items with each ote | EBsate same sive ‘Align buh the widths and highs of seleted pit items with ach other OnderBring To Front ‘Moves the selec layer fra pin item tthe op. ‘Ordered To Back ‘Moves the selected layer fra prin itm othe botom OrderBring Foreground ‘Moves the selec layer fra prin item one level up. ‘OrderSend Background ‘Moves the selec layer fra pin item one fvel down 8.5.3 Placing Print Items on Multiple Pages Note: The lt List> window wll appr via the Repo Generator} mena = (Disp) = en Ls Aint of print items on mile report forms pages wll be displayed in a tee format ach prin item data can be checked and heir Properties ean be ete, Sltem List (Reference Manual 9324) 79 MN LabSotutions/CGCsohation Operation iil8.5.4 _ Setting the Page Size/Margin and Other Items Use [Report Generator} ment [File] ~ [Page Set] 1 call the window. 8.5.5 Setting the Header/Footer AL, Use Report Generator] menu - [Display] -[Header/Footer] to call up the Header Footee> window. 2. Selecta position to aid information from among [Lett], [Center], and (Right), 3. Click the desired information button, and then a command to add the desired informatio will appeat in the selected positon fed. 4. click {OK}. “Header Footer (Reference Manual p321) LL LabsotutionsGCsolution Operation lm 50. 6 Checking the Print Image Click he Preview] eon on the Assistant Rar (Report Gone] sub bay + nitante tnt “ (Reference Manual p379) 81, MN LabSotutions/GCsohution Operation lina. 7 Print Information Types “The fllowing ems canbe printed among the ims contained in data files. Pie ban (or “imap Bicone [mm ctu dan ms [fren [iene cinsamtecammiy [om [ns “isda i chai me Dw en) me [illcemn Chonan re dame ma Balm emin te | emg aki ron a Zlesivaion cave oven including calibration curve graphs past Piesecnes Daa ma em tg eh i = Tee 70 ae [soit me In thischoer sa ial rin tem sting method, chromatogram, peak be and ealation cue item songs ar explained @ tn setion wo he dat ie dats repay th long repos can also he rn Analysis method data method file curently used for and method data ofthe data {mated print) be printed via the report fancion for each analysis line or each method fi Batch table data (batch Batch ble sorting deta being used for the canbe printed in fixed format print) Refer o Reference Manual page 263. LL LabSotutionGCsotution Operation Mm 2. I Reviewing User Administration “This software includes a “user administration” function. Users can use this function to limit the use of Futions and peo- grams to specific individuals to protect programs and daa ‘By llzing this funtion, your laboratory can conform with GLP/GMP, sock as for analysis environment and an and management. This section explains the overall concep of the user administration function. is data 9.1.1 What is User Administration? “The vcr administration fnstion wil adminsr the following ems: P vser ‘When this software is install, an “Admin” usoe with complete accoss (Le, system adminstation sights) is registred, ‘When you us the user administration function forthe fist sme, use the “Admin sting to restr one person Who USE his sotare as aus", Enter the following stings to registra user: Parameter Description Username | Enters user name Since the same name can be used only ove time ia this software, you can eater Your aame ia the [Full Name] field and an abbrevisted name or alias in the (User Name] ld Full name Entra name tat indicates the meaning of the [User Name] Password Entra password to be registered, i wed Group Select groups whore the wsorbalongs. The user can use al functions that hither group has he rights tous. Instrument | Selst the GC unit that the wssr ean wee ‘To use functions tht require their use righ, the usse needs to ener hiver repsired name and password in the [Lovin] window displayed when each program stats up 1a name or password entered in the Login window is diferent from the one reitered the program will not sat up. 85 [ll LabSotutions/GCsohution Operation lim& rights (Group) “The Rights seing can imi he unetons tha canbe used sing fe UE aminstraion function. “The fllowing groups withthe Fights shown have been reisered, Registering a user ta group that has the necesary righ’s cables the ser to have the same usage rights Change system configuration (Change systom chock settings Perform system checks ‘Group with Method Developer rights Change system configuration uit methods alt repor formats ait batch tables Create templates Perfocm system checks Perform data acquisitions Perform data analyses ‘Group with Operator rights Perform system checks eit hatch tables Perform batch data acquisitions Perform data analyses Note: A wsercan belong mor thn ne group Tn this ae tat ser wll hae al te iphts of whicherer groups helo, Note: The sstem sts wl hve complete gh Note: A now group with hs dire sights canal be ret For more abou eraing nw righ zens, refer °95Reiserng (Chazy Deli) Rights Gros ee LaPsotutionsGCsotution Operation NN 549.1.2 _ User Administration Application |When performing wser administration, selet the lev! of administration you require rom the following: User Registration Passnord Administration Program Administration F performing User Registration Use the User Regisation feature to laity who the wes are and specif which GC units and fnetons each user can ws Uns Admin” ser Tosa his software registers an “Admin” wer with complet righ. the User Administaton function snot azeded, any powson can use the “Admin” usr name when the software is installed (oo password and [Easy Login] mod). To use this sein, simply click [OK] ia the [Login] window at program startup, and all users will have complete sage rights + Users cam be registered the user registration feature is needed, the GC unit and function allowable by each user can be limited (Le. usage ighes «an be specitied). Also, complete rights canbe given to al egistered uses as system administrators, to wether usage rights {nthe same way as hsing an “Admin” user. ‘ethics, wer ane can be rd in this inforton without sing aswcrd, Using this ear sb ingress te lati compard with ing the Adon cing. $F Performing Password Administration ‘A passwords wed 1 iit the olware to patclar ses ‘# Does not use passwords Eniering only a core sername inthe “Login> window and leaving the (Passo ld blank will enable the program 10 rt. © Uses passwords. the registered password isnot entered corey inthe [Password field inthe “Logi window the program wil no stat 85 [ll] LabSolutions/GCsolution Operation ittNote: Eien when pasword ent isnot sd fhe [Easy Login] moe (expe ae) has bon reset user mms eny seguir. ‘Terre, based on th wer tae concn marageent evel a ceria evel of security can be aie. Howes, since ‘he “Adin” esr tame completly known ser am, sting the pastors manor when using this nme, Even when password is reused, eseting te [Easy Logi] made wll oviea mre secure envionment $F sctet single-user or multiuser mode, Selet whether each users usage rights are administered fr each progam. 4 single-user mode Tn single wser mad, fer sc first lags in iter the “GC Real Tine Analy Analyis Eto “GC Pot win dw, no further lain procedures will be required ale that to sr oer programs, Exiting all programs indicates ha the ser has logged out ofthe system, Although this move facilitates operation when someone uses a personal computer, if one user has logged into the system, ‘other users hen donot need to fg in and ean immediately use any programs. 4 Muls-aser mode Inmuliuser mode, each ime a program is stated, the login procedure is rquired. With his feature, a logins required cach ‘ime a rogram is strtd, whether to star the “GC RealTime Analyse Analysis Editor> program foreach GC ani, or when sarting the program multiple mes under the system configuration with multiple GC units connected toa per~ sonal computer. This feature allows cach user loging into be administered separately: Since the logged-in usernames are recorded inthe history information and usage right setings ean be performed foreach ‘sor, the advanced fonction usage willbe enabled 9.1.3. User Administration Flow User administration wil be performed inthe Following flow: LL LapsotutionsGCsotution Operation NN 56. 2 Using the User Administration Function to Set Available Items ‘When using any finctions related to user administration, all up the windows. Admin” wer i sem instar compete Sage a) ath wer éminsraton nih Soke (User Adminis vetion| a8 the (Fe) ita wer wiow wer administration ight Top a he User Admit ‘ion window ony has Pusswor ab Note: The siege etre her wil eco tet from the next ine the proprant widow ted od ih, ‘@ Functions available inthe window ‘User Adiniraion| igh? Function ya _[_¥e Remarks ‘Set general user administration parameters, v Register a new user Vv ‘Change wer registration nfraion 7 ‘Cant dees a ser euely logged in nor the “Admin” wer regisered at software etalon, ‘Create a new rights group. Vv “Change group regitwalion information Y “Cannot delete the group that the user carcily logged belongs 10. After hanging stings, new stings become effective fom the next time the program is sane, ‘Chage he pasword V | Reenar user can change only password Tigi Series Y ‘Conve event logs ASCH ks 87 ME Labsotutions/CGCsohation © eration iiltations . 3 Logging in and Setting Password Limi “To use the user administration function in this software, st the login method and passord imitations, User Administration [General] Tab (Reference Manual p420) a program i sated ater nam ber of psewont effective da, ndow appears 0 change pase ‘nod. noe changed. usr cance “a (Reference Manual ps11) ipSolution alu ‘ty moe except Easy Logi] made Note: Lapin th wr nme het ha ser aminsraton ih aly ne program wind open ee LapsotutionsGCsolution Operation NN xs Tr check, [ee Name can be sete fom pln is a login. From next fin, peet- Dis logge user ame eau eto. TF wneteckeds toxin roqufel each ume rogram stan ‘Minimum number of pasowerd haters. used for wr regis ‘on and user passwort anges. I mutiuscr mode if de User Admin window called up with mine program window open the [Single Use] heck bo wl become nective al the mode cannot be charged Call pth User Anniston window asi, but with. 4 Registering (Changing/Deleting) Users Users cn be registred not only to imit who can use this softwar, but also to understand each user's program usage con sions, [Users] Tab (Reference Manual ps4) ‘Click (Delete. apd hishlated ‘eran ia wer lis eked, ‘Chick [Ada) 10 display ings re same as “User Proper lo. Tener pssud wie fo 200 fimmaton. Password ena Ti tested, sytem aise mgt be fo tat Specfed en te setings vill "Bese | [Genera abs [Minimum Regaless of [Sele eng] te 8, Password il ‘Groups setings, wer wil av spay with“ wa ‘Sekst_ dese [Grow Lis) and move 1 [Selcted Groups} using Tada>>I, User wil hae ‘e's Hah eect dered emo [Selected Trsrumen ems] nk move [Irae em Use} asng[< (Reference Manual p19 Note: Login wih user ume at ht usr adminton ih. Note: Ifatompingto reper aed deleted sera ani in tho-Now User window, dil bx will pear asking iat wet should he etude wser ame beeper asa ne wer, 89 [lll LabSolutions/GCsolution Operation litte. 5 Registering (Changing/Deleting) Rights Groups ‘When this software is installed,» numberof standard rights groups ae setup such ss HW Administrator, Method Devel ‘oper, Operator, “This section explains how to eestor (changodelet) a rights group. o “ - [Groups] Tab (Reference Manual p17) ‘Click [Dele] and sgh frp ane guy IS Seer (User Admins: tein. im the (Fe) Ch [Ad w day NY exe Goup i Select devied em Gor [Mishs Ls) and move 16 [Selesed Righs) "using [ad>]. Thow right we vee tthe group, or mare abou pes of igh that cm be slat and typeof softer ster ris ron, to Ref rome Mama “12.14 Autor “pean Auboriad Grow” Sele deed om om [Sekced Rights) mod ove (Righs Us) ting (Remove q | [IF lg dat not ed, can Be tox ile ae iepat to commer | | dad, Spreodhest sata sch as MS Le LaPsotutionsGCsotution Operation lm 92. I What is GLP/GMP Support Functions? 10.1.1 What is GLP/GMP? GLP is an abbreviation for “Good Laboratory Practices". GMP isan abbreviation for “Good Manufacturing Practices” ‘Roth rms ar usally usd by thee abbrevistons alone. ‘Many items and fanetions are common for GLP ane GMP methodology, and this software also uses hese functions. as GLP? GMP suppon funetions. Using this function ensures liable inspections by using tehriquesto secure the public openness of inspection details Todo so, all inspection operations are standardized through dacuments, and inspection progress conditions are all recorded and swore, Procsion contol is also systematically peturmed with the reliability guarantee section folate from the atu inspection section, boing checked periodically ‘This software's GLP‘GMP support functions ae as follows: + Security Support Functions ‘Operation imitations withthe nsor rights Current user display Hindow lock function caving analysis run (to exclude other users unexpected operations) + Aude Trail Support Functions Data file structure including oll analysis related files and satus information File history view using the ait tail function User usage history (Login/logowudata writes) Data rollback Method expart + Validaion Support Functions System check (harchvare validation) ..GC-2010 only Software alteration check Column performance check 24/0C fiction @D_—_GLPCMP are guidelines laws for performing correct analyses ard inspections, Even ifthe use of GLPIGMP isnot specifically req for your nbratay these faction re wf andere fr poring any options comcty and smooth. Also, rem if some finetons are ot nl among the GLP‘GMP stppo funtion in his software some functions ae til eecive for GLP-GMP For ample using the batch anlsi dat ile mameaut-gmcraon fine (ce pe 29), cah dat fle wil be ‘ames 5 0 be ws fri casiiction management allowing eu to solve a number af ta management robles. I his lena, 2 wer nme asd forthe wer administration frtion (which elude inthe above-mentioned aston) nso be see, Although you are not requited to use the GLP/GMP suppor functions, they strongly support GLP;GMP-elated operations that can easily become complicated, lading to les efficent work 93 [NN LabSotutions/GCsohution Operation lim10.1.2 Security Support Functions & Operation imitations with the user rights “To clay the fat that the reliability guarantc section and actual inspection and analysis section ae completely separate an to prove that standardized procedures ae sed for operations, GLP/GMP wl imi the factions that can be used via the user adminiseation funsion, ‘To clarify a user when hese uss program, the user administration funtion uses username and password confirmation ‘sata program. This sealed the login proce, ‘Tho wer name and passwoed compensate cach other, thereby effectively limiting the usage rights fr cach user Note: Using ony one inion fective, however + Only et up the “Admin” wer nae for ee wr and hen reptre ptenod: Thre isn record here of who sty srfomne he operation, Als, each wt option rights tings ab window yout storage Fitton cao be ed + Rests multiple usernames wth no password Uses can we ay us names esl and thee iso ecard who ately pt @ Tre operation liitations using user rights re smportant Fr security, however, they are ako efletive im preventing wrong nert- ‘sons and edicingar-tows require nea operations witht spaying unnecessary functns. See “9 User dination $F Current user display (One ofthe GLPIGMP requirments st display the current username in each window. ‘When logging in using a correct username using the user sudministation function, the user ame will be displayed in each window’ ie rea, Soe °9 User Amina $F Window tock function during analysis ran o exclude other users’ unexpected operations) (nce you log into a program and you leave the personal compte unattended for whatever reson, a third person [a popap mena with ck right operate it with malicious intention, causing data | ME, th tsk bars icon eae oo + causing day) ee (Cemce Lack) and integrity tobe lost. eee window = (Wid) (Lock, ‘To prevent this fom happering, windows can be locked ‘when you go away fom the personal compute TF looked window dale stk baron Le LapsotutionsGCsotution Operation lm 9410.1.3 Audit Trail Support Functions Fata fe stcture inciting mnalysis-related files and status information ‘A data file consists of acquired raw data (chromatogra), data processing method, and data processing tests, The method file sed for analysis is copied and this method becomes the orignal data processing method, Furthermore, the system configuration for saving analyses condions, method instrument parameters, status information proving data acquisition was comeetly performed, and monitor value information from the GC will also be saved. When a pt is output, the report format i saved Likewise, when batch data processing i performed, the Batch abe i ao saved, (Once the system contiguration/nsrumoat parameter data'stats and monitor value information are saved, they cannot be changed. Other data wil he overwrite during postin analysis, However, the data processing method wil be writen in {he latest method aea and the viginal data processing method ill ot be overwsiion ad provected. Soe “1 tao ie Constr Oration $F rite history view using the audit trail function “The mod file and datafile data changos can be recorded at log. dita sing the ait ail inet, the file orestor ad ast changed use name and Ist update so be recorded on each ies window = [File See “1. Important Pe Conc or Operation” $F User usage history Loginlogoutidata writes) “The username as well as login and logout events an shir mes willbe recorded onthe “Output window’ [Log File tb \When use administration information is hangs, the change isory logs canbe viewed onthe window's [Event Log] tab Ser «Be! ah Ta (Rfrce Mami 9) F Data rotback Inthe a Reference Manual p39) the orginal (i, during data acquisition) and atest (i, ‘when post-run analysis is last performed) data processing methods are red. Using the dats cllback fanction, the original moth is overwritten by the latest one a the late method is returned to the ‘one used immediately before data acquisition, ad then post-run analysis is performed. The processing results will abo then tbe rotumed to their original status Soe “525 Data Ratac F Method export ‘Amethod sored inthe datafile canbe expe a8 a metho file ‘After performing x data rllbac, use this function to save the data file's method as fle A metho file withthe same dat as the original can then be obtained. See “$2.1 Importing Exporting Meo’ 95 [Nl LbSotutions/CGCsohation © eration ill10.1.4 Validation Support Functions 4 system eneck hardware vatidation) .. GC-2010 only ‘Sew “102 Parfoing Sytem Cheeks GC check and consumables replacement period detection canbe performed hy activating the GC's system check funtion, ‘Repos oftheir resls can then be printed or saved as files. Ser tbl So < (O4OC] Tb (Reference Nara p01) LL LabsotutionsGCsotution Operation lm 95. 2 Performing System Checks “This software inclads a system check funtion to check the condition ofthe GC. Prioe wo performing data acquisition on the GC, be sue to perform a sytem check and verify thatthe GC conition s appropiate. 10.2.1 Performing System Checks Data Acqusition> (Reference Manual p57) 0” Reference Manual p23) sons and pene condition Dips previous system cok esul (Reference Manual p151) Note: This wevon only uaa on he GE-2010. 97M LabSotutions/CGCsohation Operation iim10.2.2 After Replacing Consumables ‘Aer the system check has completed, there are any consumables whose check result is “Not Passed”, replace them with ‘new ones as soon as possible Data Aeuisition> (Reference Manual p57) 0” Reference Manual p253) Click Ree] w est replace core tnnable coun nnnnenneenenntatntnnsnenttne ‘cach Hens check canton (hooked oF System Cheek Result» (Reference Manuel p148) otehecku).| Note: Forte consumables check, resold ar used for comparison. These are dt entered ina winow displayed va “System Contge ‘uration -[Conigret Moles] -(Poperies] ib forthe unt with consumables [Stns of Stem Check] to, Le LapsotutionsGCsotution Operation lm 95. 3 Performing Program Checks ‘Sole (Chock the Pr ‘gem Files] in the [Foot mena ‘Aer rogram chock comple cook ress pp eae Note: To sve the ssa of the prog heck, we Nowe’ [File ~ [Sve As] oe pra the ea sing Notepad 99 [lll LabSolutions/GCsolution Operai “This software includes program alteration check funtion tha is sod to chock whether or not program fleas been ard, - (Reference Manual pi) check result ts are islet. i. 4 Performing the function check (Chock oso that the installed program is operating normaly using the following procedure. 10.4.1 Procedure for function check A, Use the following GCsolution funetion check data group: Daa mame Upiied Cheskgsh | 000629 1350 [Check wom _[ooosar rss] CheskOT ged | OF OG TIST ‘Check ged | 00629355 Chek ged | 0005 2VTIST CheckRep gor OHOG TT RIT Note: The dots usc hore freien whenever the fincton checks erfomed. ach time, lo the at the Projet fe onthe ard rom the CD-ROM, * €6Cstution CheckDa (hen GCslaon hasbeen installed to C1GCslaion) For ling the foto heck di oe "10.2 Laing he fection cc da roy 7, Boatle sik the GC Poston icon onthe des topof Windows, from Stet Pot Fol), 3 Sele we Totndeai {Cesk geht the bash ‘she 5. Clk on the Sen on. Batch pest ill be cai cut anda ep willbe pind ou Check to ae whether {following ror result agroes withthe outpa report su LabSolutions/GCsolution Operation [NN 100$F evaluation criteria Gcshon same ys he fnton eck hen te leer pings and nes wed in step He above te ‘execution of Check gch is completed successfully in step 2y above: and the results agree with each other in seep Fe above. GCsoluton software funetion check reslt ‘The date when the fc shock | preenel ped tee Teer ez/Awg2000 ‘printed results must match this one. fee ieee nc cee oe I, ERE aera aa ea pal (ae ce ete apaeitae feet eee Nac eet (Bet Name Peak au tiae | “Cimon Ieraagiaor riser TBM on arnsorrarseons ea ett = we see 105.000 187008205 re 10.4.2. Loading the function check data group Click on Run... on the Startup menu of Windows, and directly start the program for loading the function check data zoup (setup.exe), which is located inthe CheckData folder o the GCsolution CD-ROM, Note: automaticaly. Since this seen is wo usd he kon the Ext ton terminate it 101 HN LabSolutions/GCsotution Operation Sitti Att the GCsoltion CD-ROM has sen iar inthe CD-ROM dvs fe Laboluions Gcslauen Sep sree wil ps‘Ener EChmckDaaSeup on he Name textbox, ard cick othe (OK buon. (The = port ares sensing onthe lean oF the CDROM Eve 2. The Weleome window will appear 3. ctick om he Next button inthis window. ‘The Start File Copy window will appt. ‘Te ins rogram wil automaticaly dtc te les ‘ion where Croton isntlod Check se whether he destin ofthe fst be ‘nsled matches with he locaton where GCso¥son isin. Click onthe Next button inthe Start File Copy’ ine dvs: The Complete Setup window will appear. ‘Click onthe Finish button to finish the setup proce dre, LL LapsotutionsGCsotution Operation lH 02Inspection Report for GCsolution Now Dates Mose! Signature: Serial Nas Geek tem ‘ation Tease Spam cie/GCaOID aay | Syten cieck raanion ak Pes Fall Thesk ms Gonsinabie) co bec th Osram Cenc cate rent Dien Cheskitems (GC chek) Cite sear Dow Deco cations Le verge Lpetectior rom (Jrton uri Boare ROM Cerveomen [ower adc Chron ui toe aD rina tree Llosecortgh one Elion cont Cosrctrinite Deals (ithe judge Fa) Geek hem aon Tadee Program cack ‘ek of esi ands [Pass Fal Deals Oe jogs Fury Geek em ation Tage Turton cack Cia of intro Tas Fall Deals he jndgeis Fa) 103 [ll LabSolutions/GCsotution Operation Silt. 5 Viewing History Information “This software includes an

window that records users who sar and finish programs and thsi dates, as well as an ui trail function hat records metod file change information. 10.5.1 Viewing Program Start and Finish Information (Output Window) ‘Swisher window. (cutie ana (Reference Manual p18) LL LabSolationNC solution Operation KER tox. I Displaying Windows and Bars “his software includes the two main programs: “GC Real Time Analysis, uso to set data acquisition parameters; and , used to perform analysis onthe acquired dat, Fach program seen consists of multiple aplication and common ‘windows that contain varity of functions, a8 well as other type of windows called “bars” that provide a numberof aux iary functions, 1 1 Window Types Appearing in Program Windows Mainly, windows ate classified into wo types, pplication windows tha provide main functions and common windows that provide auxiary Funetions ‘You can call up common windows in an application window as part of the application window items ‘oolar ions are used @ Switch the common i dows’ spay satus between displayed and hidden.” * However the slay eats fo the toa mast best sing ‘he [Toola] command in Be [View] mon Conon windows are soetines called “win dove” aed srcimes eal "ha. This simply comes from thee wien’ val inpeesions, Since all windows (exept fr the Tie Bar and ‘Men Bar themschss that fame the atl wie ows) can atl be displayed as windows (xe Agar on right) > window types (Totbariconsreterence pages in Reference Man GE Real Time Analyaie> GC Rostra ‘Application Windows “Data Aequistion> (P57) “Data Analysis (P35) (P209) (PISS) Report (P305) ‘Common WindawSTiars losrument Monitors BY P34) bua beer (lle cou Wake llr nw Bh 105 (ll LabSolutions/GCsotution Operation Sit11.1.2 Displaying Application Windows “The following windows displayed ina program window can he open or cose wing the aprations describ below F Using the Assistant Bar: |When you perform operations using the Assistant Bars, tbe stat up and switching of application windows, as wel as the switching ofthe Data Explor file tabs wil usually be performed automatically. $F starving an application window using [Window] - [Show Window {Show Window] commana ao ope, cls wp selected appli cation wind TF aleay ope Sitchs othe selesed aplication win, Window svching commands Swih to. any open aplication window displayed here $F doubte-cticking afte in the Data Explorer ae testech LabSolutions/GCsolution Operation [NN 105. 2 Customizing Windows 11.2.1 Changing the View Size ‘Some aplication windows consist ofa number of “views” that can he displayed in several sections divided bythe Split. ‘Thosizes of those views in each window can be modified using the operations bol. % Using he spritter DDoblectck bee 11.2.2 Changing the Application Window Display Format Displaying in window format Select (Casade) w as play viens ovr 107 (NN LabSolutions/GCsotution Operation |SiteF Displaying in tab format 11.2.3 Changing the Common Window Display Format Displaying in window format Drago double-click tt bar to smich he dpliy peo ie ssndow em between docking and window formas. Sine toler does ma hava bar, drag or double ik an sree excep theta on a sich he fra. % Maximizing the Data Explorer Deselect he [Allow Docking] command inthe Data Explore’ right-click manu, Common windows will hen be hand the same way a8 appliation windows, enabling you to display them maximized, side by side (Til) or overlapping ([Cas- a@@aa@aaa a a i LabSolutions/GCsolution Operation [NN 108. I Operating Table Columns ‘This section explains how to work with the columns ina tbls using the program's view - [Compound Table] tab, as an example. 1 cell with a atom tie dsgtayed seated ‘etinostgray-colered ! folume” Cann a flee or move ach inp lt of » tik acl to sels an etre column, Drag talile consecutive ttl eal 0 ele al hone slurs slant ‘While holing dow the [Shi (Ct keys, lik mobile conscunse (ise) 6 alls slot oly hoe colamn. 12.1.2 Changing the Width of a Table Column T Pace ear on tle ell torr and casoe wil charge 1 ths Stape. Dag cursor to change ‘con also change ‘alin wi [Rows] colann wilt Perr whi slcctiag mutile (out not delee oF «columns and can change wid rove) fo all thone columns sia netsh 100 NN LabSolutions/GCsolution Operation iit12.1.3 Changing the Table Column Display Condition (Table Style Set- tings (1)) [Right-click the table to display a pop-yp menu, The last (otto) command in this mena i [Table Sie). Use this command {o designate the rable column display status (splayed or hidden) as wel a the column display onder Note: For some views played inal iat, dh Table Siyl> widow wil ot havea [Colin Onde th ‘Use [Up oF [Down] batons © selet per or lower tem Gahtorien uble, ‘Setting Points: + Display only necessary items. + Locate items in higher ffequeney order, rom the Tel, (That way, you can view those items without using the sell ba.) + Reduce the font size and cell width as much as possible “Table Sisle=- [Column Order] Tab (Reference Manual pis) Note: tn he ide HomsJand [Display Roms] fis, slet consecaive is simuanousy lick he st itm an then the Second ‘ne le holding doen he [Shit] Ky. To eee ert ems smulanonusy, ck he deed ems we ollie down the {Ce key. The mule elected dems can be opera al st once wing the [Add] or (>] or [=progias window Method view - [Compound] ab, a8 an example Topmost gry colored row ie the" om” Canoe det ach inp fed oF | abled 1 cal i the (Rowe) column is etllod isk avo mamber elt sleet an emi + Dag multiple cnstetive row number ells to eletall hte roms britney + While bldg down the [Shift (C4) keys, lick muiple carscave (scree) 18 ‘ater cell to elet oly hoe rs ick (Row) ul tions ile etl ‘eles ene abe ‘ect two eons sinltanousy segue fr ding. Inch ease, ght the leo display pop mena and sete (Select Row] commndo extend the select range to ita he eect We ONS. 12.2.2 Adding/Deleting a Table Row ately above the 08 were cursor is pate tioned cursor postioned Sr moves up the 08 ent, 111 [ll LabSolutions/GCsotution Operation |Site12.2.3 Changing the Table Row Display Quantity (Table Style Settings (2)) Although you cannot specify the exact umber of rows that canbe displayed ina tbl, his number can naturally be adjusted by hanging the Font type and size used in he able using the [Font] tab inthe “Table Sile> window. desi fot ie, Setting Points: + Set the font size as lage as possible. + Select a font ype that is easy to read even when set to a smaller size Table Sele= [Fond] Tab (Reference Manual p47) Note: The cel Aight wl utomailly change based onthe selected ot sie. the fot sz i se sna, he name splayed ‘owsin the able will icase, However, since he ell width has ben spied independent wid will at ehang ease ofthe foe is. Wen nscessry, ke he ctr deeb a /2..2 Chasing the Wao Table Column hang he ll — ee LabsotutionsGCsolution Operation la 112. 3 Editing Table Cells 12.3.1 Selecting Multiple Cells ‘Dag moe dagoally to enclose fll of Hold down [shiny key and ck cells diagonals ‘Copies ent ube ecu ingle row to Coa Copies selected cl Deletes sled eo ae (dts Clipboard, Reps cll da lok. fore weir Et] mae. ‘Aer selecting edit are ighclck tie to oi Play popap men, Note: Ihe data pst destination rasa thn the daa pase Source ar testa ase are i termine by the sure are ‘Als, ithe destination ae ie ager than the curse ae, the source data wil bs asad repeat wil the destin ata ic ria "Note: Dut copied oe Cliphoas can als be pst int commercial speeadibtsatware such s Micros Excel 12.3.3 Entering Values into Cells Data canbe entered diet int cells fom the Keyboard when he cells are editable. However, some cells havea special data entry forma, and for those cll, special fanetion is spportd o alate data entry in each Format ‘See below about howto enter data nto bach table cells in the atch Table> window, 113 lll LabSolutions/GCsolution Operation SiltDee Trample Deseripiion ‘Window pop-up ‘ype ‘Ale selecting a el, click the arrow button atthe (For complicated stings) fight of the eal, and an appropriate pop-up data ‘entry window for that cell appears. Ia this example, the file election window will ppear "Aer selosing a cll, alick the aivow bution atthe right of the cell, and a drop-down selection list appears lick desired item in this is. Drop-down Ist ope (For selecting from many choices) Fence eroiret ‘Alor selecting a cll, click eitbor of the aarow bak toas atthe right oF the eel to increase ar decrease the cal's value the designated step value. To enter data witha diferent step value, use the keyboard Spin box ens pe (For entering specie data) center vale dicetly it the cell Cheek box pe ‘Glick the check box ths well oatach or mows (For ONOFF ents) the eheck mark. Pr = 12.3.4 Cell Data Entry Auxiliary Functions (Batch Tables) $F For anatysis batch tables “Input Cok Det Reference Manual p275) all p wright ens adsl put Col Dats A indo eter clue sfoomaton ll tons wl appar This ture is avaiable for {Nae (Sample Nave) (Sample TO, nd [Dae File Nene tans $F ror postrum analysis batch tables Adal Rows with Dats Files Gallup @ perso menu and eect {Ad Rows mith Data Fes] A window le automaticaly eter ds le appr te sample iefomatog daa pe (le oll apes File dats wil be sin ‘can alan changed Note: Can also drag and dep desire dt fle batch abet a ch row t table ou. ee LapsotutionsGCsotution Operation (NN 14> 13 Operation - Files T3. I Important File Concepts for Operation 13.1.1 System Configuration File ‘The system configuration fle data wil he read only once at program Startup and stores the connection conditions between the personal computer and GC unis, as well as installation information for each instrament that are connested to the GC. |When mukiple GC unis are connected to the GC, this file will be rested foreach GC nit ‘When clicking the [System Configuaton] icon en the window will apnea. Setting data entered inthis window wil be saved in the system configuration file ‘Thesirucure ofthe syst configuration file will reflect the GC's instrument structure with ine analysis performance System Configurat Sometimes silt 13.1.2. Method File The flloing information i stored inthe method file System configuration file Revorde cm configuration file data to check appropriateness of the instrament be: parameter sti 1 (checking curently connected instruments). Instrument parameters Stores cach instrament seings dat that has been entered using the view inthe srsen Data processing parameters: Records calibration curve data, column performance parameters, QA/QC parameter, and pea intepration/guanttative parameters, compound/proup tale da, lis LabSolutions/GCsolution Operation,‘As with the system configuration file, some of the instrument parameters are set commonly for both lines and some ae set ini- vidual for each line Note: Although concep oe ines equal one GC ste, some devices sch athe column oven are wid commonly for bath Tine, rd enalsis wl als begin sinulancousl on ot ies ‘On he other hand, data processing parameters wil be used to ro c=ss chomatogram data obtained from the detectors, therefore, ‘ese parameters willbe et foreach detector. Note: Only te QA.QC params, hoover, caf Be st For the iat chanel 8c. 1a) force ‘The separate parameter and data ranges used for each GC, tne, and detector channe are important concepts to understand with this program For more ab ho seth intraent parameters weer t9 "3.2 die {ng Meso steument Parameter Seine) For mare au how 03 the ds processing prameers mfr 0 °S 13.1.3 Report Format File “The report format file stores report foumat settings data that is used to prt analysis esas. For mor abou the rot forma file setings et, fe 108 Report Facts” Since epors are output foreach line, designate a report Forma file foreach line. Therefore, one report can include print items for data up w thre detectors Note: When using th sume ort format or bath Lies | and 2, he same er frmat can designated. Note: When thee are mip detector chs o Line Ibe st dig ep at ifr lip chans Le LapsotutionsGCsolution Operation lH 11613.1.4 Data File ‘When performing data acquisition, the system configuration and method files use at that tie, chromatogram (peak data) actually acquire, and data processing results ae al saved in one datafile. Note: A sept fvmat file i sve in dt fle for report cups A bch ile (abo) i lo saved in dat fe orbtc processing ‘When using 2 simultanous ins to acquire data, «datafile is obtained foreach ine ‘Also, when using mutiple detectors (chanels) on ne line to acquire data, chromatogram and data processing result files foreach channel are created in one dat file, 117 [lll LabSotutions/GCsolution Operation‘Asshown in the Figure onthe previous page, a metho fle has wo pats: instrament parameters, which are each line’ sectional atinbutes: and the dia processing rethod, « collection of all detector channels information. The daa processing method is intrally culated to record both the orginal dts processing method used for data acquisition, andthe Latest data processing method whose parameters hve been updated to perform post-run analysis later 13.1.5 Batch File In this software, conditions to be used for multiple dat acquisition and deta analysis have been set inthe batch table in the ‘Batch Table> window, allowing continuous data processing to be performed. “Tho bath file stores the batch table and entre batch scttngs data, Soe “7 Bah Processing Only one itm of eabsime batch processing (Btch daa acquisition) ean be porfrmed in the - window (sve Reference Manual page 303), the data file's report format willbe used enabling you to bring up the previous report conditions. In this ease, daa will be read in automatically when opening the report format. This data can also be exported as a repr format fie ‘+ “The bate file stored i the datafile can be used asa record, Since this data can also he exported, the batch fle obiained when batch processing is last performed ean be obtained, ee LapsotutionsGCsolution Operation NN 118«2 Using Files (1) “This section describes the asic file operations that ate common toll appiation windows, 13.2.1 Creating a New Can also set a temple. Car shay erage ae Tes sng Selected tpl, ae ration Cv windows “File New (Reference Marval piSd) ‘Now ies canna beet sing te wil F[ cick [Seee.-7 - (Reference Manual p50) 119 [N| LabSolutions/GCsolution Operation Silt13.2.2 Opening a File (1) Timdas sonsenomaT proves le forts) $e alo supped. sd Operation is re same as sing [Save As + With ie mime, sing an extn. preva seed le) ‘> Data will be overt, Note: When atempuing wo clos ior plication window wih Me daa eta new filed) change, a dig bo appears t= ing wheter or eat save tele data [Name and save a file following the steps below. LabSolutions/GCsolution Operation [NN 12013.2.4 Saving a File as a Template ‘Any ile can be saved a a template and then used ater Note: A wmplasisa filets he some os this softer eg is (uch, perform and method Hs) and isaved in «special ‘splat fl. This file can seo bowed a copy source le when ring anew fle, The prosede to sve fle as ene isthe same to change le na cave itunderanothername: However, sine mving ales aemsplnteisan fective means oF preveing rouble suchas overt ile ta mistakenly suse rete and use sandr empl Files Righickok died le 13.2.5 Checking File History Information (1) (Check file eration and update dates using the following operations. gE Deseription/Adaltons FEM Tie atmo TT] a [9 | Bletine erator eration ie pda daa, ‘Comment VL | V] ay | Can be used as. file search keyword, asia || Desai apdaad Toga wi be sve or each method saris the method ie and data ‘ample Tfimation | Sen inemation ued For data aquiiion (ample name, Sample 1st) Tet | Fist of method batch report Toma, Racine data ie used or data scasstion. 121 Ml LabSolutions/GCsolution Opera. 3 Managing Files Effectively “This software uses the window displayed in each program window to perform file management 13.3.1 What is the Data Explorer? Fite management is performed using the appli ick hae wo evi the Data Explore ‘wedow esl sts (dapaged or sac. eat Matton tte @ = —Sam. Bue ite ys. Sa tiaia! Sy cee “Data Esporer> (Reference Manual p37?) 13.3.2, What is a Project? Inthe . ‘The curent project is displayed asa releence projec in the [Project in} list Reference prjects can be changed using the [Select Project) button. Note: Up wo ten recently access projects ate sedi the (Project in). ‘Therefore, itis sometimes csi owe this sto sch projets ding egal operation. Note: When this software fs msl an empty projet (Fl) wh the sane "Projoct I" il bested ar dail Lab Solutions/GCsolution Operation NE 122‘Tho current projet i effective inthe entire range of each program's win- doves. For example folder intaly displayed inthe Reference Manual p05) BASELINE. For example, when designating a method file for «batch table in a reference project, a closed reference projects file wil he ‘designate, Then, ifthe bate file nd metho fl are copied a newly eeated projet nly the new projet isnecessary 0 referto the combination of tho two files. Because ofthis, ia set of method, batch, and report fle ata ae copied toa new project, ven ifthe current project neds 0 be erased (eg, due 0 insuicient hard disk space), no problems will occur (since the current proc’ file was not desig ated. Also, if backup project is erated for each projct before i is deleted, itis easy to estore the project's environment Later ‘nce 4 complete files stoned inthe Bickup project. Moreave, analysis conditions that were set na eftence projet will not be influenced by anyother projets’ changes 13.3.4 Deleting a Project (Folder) Note: The [Project] mem willbe played when te o display a popsp menu, where you can sevselect display items. The preview canbe clngst by cage it th Your muse Same stings a in Windows Explore fin, sich es sample ome displayed as efoto, Data Explorer Proper (Reference Manual p02) Note: The sing daa ener here wlhe sve foreach user Therefore, the ie ta rae here wll at be payed if ageing wilh treat eae Le LabsotutionsGCsotution Operation lm 124. 4 Using Files (2) ‘This section explains how to operate files using the 's Me, ‘An application window uso to read the fle data will bovome active andthe fle data wil be displayed, FileType Window Type Method ile “Data Aeauisiton™= “Alyss program =Calivaton Care Pos-rn prograr Dasa ie Drag and drop file onto an aplicton window. ‘When dragging and dropping a desired file onto the application window were the i's data is read in, functions equivalent tothe fllosing operations wil come ative and theft data wil e splayed FileType Drop Destination Equivalent Operations Method ile | (File) -[Open Method Fis} Da Analy {File} [eoad Meta Dats ile Daa Anal TFile}- [Open Daa File Calibration Curve>* | (Dat) - (Ada) “Da Comparisn> | (Fil) [Open Data File ch Tabi [Fait - [Ad Rows with Data Fes] Report Generator | (ile) [Load Data File] Basch le Bch Tabi {File} [Open Batch Fite Report Fema file Report Generator | [Fie] fOpen Report Fi] * Drop ono the ie 125 lll LabSolutions/GCsotution © peration iii13.4.2 Copying a File project toe Note: Files can bo copodbeence his softwar Data Explorer window andthe staniard Windows File Explore by daggng at droping tbe copy destination onthe sme dive pefoom the dag and top whi eléng down he (Cu ke. 13.4.3, Moving a File Righetik sours Project or mon and File Wove> (Reference Manwal p01) Note: Tiles an fe moved sence his stir “Das Explores window and the standard Windows Fil Explore by dagging and * ge gem ASCII fle "x AIA ANDI fle => TOurpar Toms] button appears only when See op tems to converting 10 ASCIL. Select which items ill be outpat from data fe ‘ck check boxes oF itemsto Be out an eet Deter wed between values ‘now dct, “Convert Data file to ASCH file> (Reference Manvalp398) When consenting file eat vi Shiadats CLASS-GCIO w 2 GCsouon fe, he fllewing dats wil erected inthe now fe: ‘Conver Sourse For. | Conver Destna- Description | ‘mat tion Format CLASS-GCI0 data | GCsoktion dna file | Convers the CLASSGCI0 data fle and chromatogram refered to in fle this data fe, a GCsoluion data le ‘CLASS-GC10 ehro- | GCsokuion data ile | Convers & CLASS-GC10 chromatogram to 8 GCsolation dats le maogram fle Note: soak tale wl have nada entre and mod wil ete deta CLASS-GC10 ‘Gcsontion method | Convers the CLASS-GC10 method files data procesing parameters method file file and instrument parameters to a GCsolution method fil ee LapsotutionsGCsotution Operation la 26. 5 How to Search Files section deseribes how to search for files using a variety of keywords. File searches can be performed fom the program ‘windows! main window at anytime. 13.5.1 Using a Variety of Information for File Searches project (fdr) toch Use sample norm {only forges) File Search (Reference Warual pI Note: For each serch emit erry op own is Box, you can skeen among the vious fhe serch omtons, After eotering a search condition, click to sta the ile search 129 | LabSolutions/GCsotution Operation iitInthe lower part ofthe “File Search window the following search results display view will pest, rd, upmand or Righ-cck He hs ‘nnd ‘ 1 splay mena aetna and select (Detail ‘aera aay ‘lick tn}. Disp fle infor rut fr arenly higihed ein i (can ag and top Sie rt application Seach nda ‘tik (hee. ee LabsotutionsGCsolution Operation la 130. I When Troubles Occur 14.1.1 Using Help 1 IFyou have any trouble: ‘uFyou have questions about technical {erms and parameters: ‘hick he ep ou Soa (See) paar ae] from he Help enw Theos a> ‘sind wil peat rte conenty active window (GC Help Window) ‘whe he sme torn is mentions in endow wl appest 131 EEE LabSolutions/GCsolution Operation Ss14.1.2 Using the Online Manual Clik [Online Wan ‘ol tn the (Hep) Tae Adobe Acrobat Reader t9 view the {GCosation’s Istrcion Manuals (Open ‘ens Manual and Refrene Mana) "You can such for You can juny 12 desire page Reference and index sens ae spayed sing Dookimks (, ble oF las ant iked for quick referees of eaten) ‘eae tons Note: Viewing the Online Manus ques nsaling“Ade Acona Reader 4.0 Ifyou iy he eps enone above Wiha rst ‘nsaling Acrobat Reade. a dialog bo will appear prompting etl Note: Adsbe Acrobat Reader 405s stor on CD-ROM. Follow the ps teow tons + Place the CD.ROM no your ompuer’ CD dive The GCholuton instalaion pose wills up Cao and then et it + Doubleclick the [My Compton onthe desttap. Next nik the CD-ROM icon ods popup mem, and set (Open) + Double-click he “crore exe le onan the CD a flow the instactions dled on he seeen 9 comple Note: Formorabout Adobe Acobt Reade 405, refer tthe Adobe Acrobat Ree 405 software's Online Users Guidand the Adobe Conor’ eet Homepage Note: Although da stored inthe GCsslution Ooine Mena (Refeence Manual) is the sane asthe Help dt, we recommend at you se Adabe Acrobat Reader 405 when pining for Beer gual Lab Solutions/GCsolution Operation ENE 132. 2 Reinstalling GCsolution “This section desribes how to reinstall the GCsolson software. Sofware installation is usually required when any of GCso Inton’s applications starts to malfunction 14.2.1 _ Installing GCsolution Note: aro endaling Colton whe stars malluntonine fo some re8sn, et, unsall he eet CCslation sare To Note: The nial di ix stored on CD-ROM, When exzctng the GCsouin stl program, he install d's compres ils wil atmaicly He exacted with he install ise’ special program and ion copied tthe om’ hard dik ‘Tis sata will ao operate if you merely copy the CD-ROM dt the compu hard ik without exacting Bese 10 Foo the const instalation poses Note: To insti sofware, the Windows NTA system mast dy be inte asthe compatrsapertng sem (8). ‘Shee thi sofware’ isl ite des nat ean the Wins em, when YU se YoU compa, please be seta the ‘Windows system is instal the Windows systm inom on our computer, ofthe Windows pte dose nat operate cucety isl th Windows stem n your computer an exablish a eanect petting evitonment Fst Ie adn, Itt Explore software version 3. higher mst alread be instal. tumour sanpatpowe A Windows arp, seth Gon isl die int be CD de. tomatialy start up andthe window will spe Fate install “i€soluion Setup” will aE Cra] Noto: Ifthe wind docs nt apn auomatialy Sle the Task Bar's [Stat] nena Ra} The ener E:Seup. oe" te dled window [Open ext box, click (OK (Hse, the CD dive is signed as “:") 133 [lll LabSolutions/GCsotution © peration SinInthe window will appear Tn the window, lik [Nex]. ‘The window will then change the window click [Next ‘The window will hen appear Le LapsotutionsGCsotution Operation KN 134Usually, select [Yes] here, Ifyou know you will never use the Help dat, o if the version of Internet Explorer isnot cor rect, select [No] After selecting either one, cick [New Note: If ou click [Nex inthe Install HTML Hip Sytom> window, snd ‘he

messge box appr (Fate 0 the ght lick [OK] to qt the installation. The, reting Wo “742 Fang {D0 ntl he DAO (Data Access Obj) snd opin the GCesation insllation gain. ‘The wind onthe sr an in the [Na] el an th sr up inthe (Compay Trance NEP “The window will appear 135 [| LabSolutions/GCsotution Operation iii‘The GCsolution software wil be installed into the folder shown inthe [Destination Folder] field in the “Choose Desina- tion Location window. Usually. ase this splayed folder as its. Note: To change the destino folder, click [rows] in the Cone Dest ion Leston> window. “The ). A message hox will appear stating “Copying program files.” as program ile instalation begins. Note: To cancel nsallaion, click (Cancel “The cst St wind i at “To contin the nels, lick Resume}. The Exit Setp> window wil ben disappear andthe insiaton wil comin, “To comply stop the slain, chek [Ft Sep The st Sep> ‘window wil thr clos andthe ntlation wlstop. ‘The Gotu sempton ps. 1 the instalation Hnishes normally, the Install Cmpete> window will appear. 9. tn the window, click [Finish]. The window will chen close, completing the GColution setup, Selecting Yes, I wan to restart my computer now] will avomatcally restart the Windows system. I yu sole [No, Iwill start my computer later e sure wo estat the Windows system before you frst use the GCsolu tion software, Le LapsoutionsGCsolution Operation lm 13514.2.2, Uninstalling GCsolution L, From the Start mena, point to [Settings] and select [Control Panel]. Double-click the [Add/Remove Programs] icon c> ‘The window wil appeae 2. From the lst box on the [LastallUninstll] ta, sleet [GCsolution]. Then click [Add/Remove Note: To dete he OC sotings ented p42 stalling Adina! GC Uni slot (GCsp beta - (Akon ae low the same steps hoveto delete GCsolae, 137 EEE LabSolutions/GCsolution Operation Ss‘The window ie wil change to window asking i you want ee all used taro ies 4, “The window appears and the GCsolution application is deleted, ‘Once the uninstall forthe GCsoltion application hes completed, the [OK] button in the window docs nt open alomaticaly Sele the Task Har [Start] mona Ran} Then er “ESetup.e” nthe dplyed Run.> window’ [Open ext bon and lick [OK (Here, the CD dive is sented a8") 2. Click [DAO Install in the “LabSolutions GCsolution Setup> window, ata Access Objects (DAO) Setup” will sat up and the “Weleome> window will appeat 159 [| LabSolutions/GCsotution Operation SilInthe window, lik [Next]. “The window will then change othe “Select Components window. 4, the Select Components window; click only the [Jet 3.5] check box ad then eich [Nex] ‘The window then changes to one where you can select the ata formats oa 5. Remove alt check marks and click [Next> ‘The DAO installation begins, and when finished, an Information message box will appear wD ee LapsotutionsGCsolution Operation lm 406. Inthe window will ape Brit cn ieee feu) os ia Se DAO a Erna] Note: fhe wind doesnt ope automaticaly Sle the Task Bar (Stat mona Ru} Then ner ESeupe" in the dilayed window [Open ext box, and tick [OK (er, the CD dive is sgt as “E:") 141 {ll LabSolutions/GCsotution © peration iiiInthe window will appear 3. click te [Nex] barton in the window. “The window wil be opened. 4. nthe oan window, ik NEP) ‘As program fle istllation begins, « message box will appear stating “Setup is searching For iastalld components." ee LapsotutionsGCsolution Operation lm 421th instalation finishes normally; the Install Complete window will spp. 6. te tna Compl wind, click [Fi The cna Conplete> window wil an cls, completing te ‘caclen up Stet enw reat my computer no wl somal sat te Widows ye. Yossie [Neill tat ny computer arb se es he Window en bf ou i athe Con tion software 143 N LabSolutions/GCsotution Operation |i14.2.5 Connections to and settings on the GC Note: The device names ofcomunicaton prs (COMI. COMD, ct) de not aways match the ana port namo the Fa of You pt eval sompue (he symbol ICIOM andthe or aes f mle stand ons, ify) becaus thy can be hanged sing the (08seing. a communication otis added sing an optional Board he signed device mane varies depending on he spcifien- ‘oso tha board ‘Arse cormniztion prt has boon ete conection the GC may not be mae propery Tn this cass, revew the insrstion ‘ara othe pesnal corp, OS, and aed boar. Note: To conc the AOC20 10 the GE-17A, GC-ITON oF GC-14B1C, harm apcal ink ere (PC-STN) mus be povidone he CBM-I02 Comict sesso 1 of te PCN Wo he concn marked “OPT LINK" onthe er panel of he AOC sig the opel ik cab F Forte ce-2010: AZ, Connect the connector marked “RS-232C” on the rear panel of the GC to the COM port oa the personal computer using the provided transmission cable 2. Turn ON the GC to display the LCD sercen. ‘On the windows displayed ty the flfowing key sequences, (rune) [ENTER) (GC Configuaion) [LENTER) (Transmission Parameter) ‘Then set? the Protocol LEVELS Baud rate (bps) 15200, + Trewpand down cure keys re wet tole between tes tele ond ight cursor ey ate sed o eet val and he ENTER key Isto neti he eng. ‘Once the setings ae completed, turn OFF the GC momeniarily and then tu it ON spin. The setings of tansmission prrameters wil ead valid, & rortne Ge174 v3,6C.1700 T. ‘Linge ngte etmminin ble connec he COM port he poe empl cme maed RS. 252 te ea pel fe CBM102 2, Using the optical link cable, connect the connector masked “OPT LINK” on the tear panel of the CBM-102 to that ‘marked "OPT LINK” on the rae panel af the GC. 3. Using the FUNCTION 15, set the transmission parameters for the GC as LINK PROTOCOL EXTEND BAUD RATE 2400 COMMUNICATION OPT. PARITY. EVEN stor ars, 1 FILE FORMAT 14CH ee LabsotutionsGCsolution Operation lm 444. Using FUNCTION 14, set the parameters forthe purge APC and the APC forthe detector on the GC. 5. After the setings have been completed, tum OFF the GC. Then turn it ON again. ‘This will make the settings valid F ror the G-17A v2: A, Using the supplied transmission eable, connect the COM port on the personal computer tothe connector marked “RS- 252C” onthe sear panel ofthe CBM-102 2. Using the optical link eable, connect the connector marked “OPT LINK” on the rear panel of the CBM-102 to that ‘marked "OPT LINK” on the rae pal ofthe GC. 3. Using he FUNCTION 1,5 wansmison unmet fr te GCs flows LINK PROTOCOL, EXTEND BAUD RATE 2400 COMMUNICATION OFT. PARITY EVEN STOP BITS, 1 GC-I7A MODE N 4, ater the setings have been completed, turn OFF the GC. Then turn it ON again. ‘This will make the transmission parameters valid, F vor me Ge-17A vi: . Using the supplied transmission cable, conneet the COM port on the personal computer to the connector marked “RS- 252C” onthe rar panel of the CBM 102 ‘A dedicated optical lnk intrase is requited for the GC. Using the opis lnk cable, connect the connector marked “OPT LINK" on the rear panel ofthe CBM-102 tothe conecior onthe opal link intr‘, 3. Using tte FUNCTION 15, the wansmission parameters forthe GC as fallow: LOOP PROTOCOL EXTEND 4. ter the setings have boon completed, turn OFF the GC. Then turn it ON again, This will make the transmission parameters valid F rormece-tse: AZ. Using the supplied transmission cable, connect the COM port on the personal computer tothe connector marked “RS- 2320” on the rear pant ofthe CBM-102. 2. A dedicated optical link interface is required forthe GC. Using the optical link cable, connect the coanector marked “OFT LINK” on the rar panel of the CBM-102 to the connector on the optic fink interface. & For ne Ge-tsc: L, Using the supplied transmission eable, connect the COM port on the personal computer tothe connector marked “RS- 282C” onthe rear panel of the CBM. 102 145 [EN LabSolutions/GCsolution Operation |iUsing the optical link cable, connect the connector marked “OPT LINK" on the rear panel ofthe CBMC-102 to tht marked "OPT LINK” onthe rae pane ofthe GC. 3. Using the FUNCTION 15, the transmission parameters for the GC as follows LINK PROTOCOL EXTEND BAUD RATE 2400 COMMUNICATION OPT, PARITY. EVEN stor airs, 1 FILE FORMAT act ‘Alter the stings have been completed, turn OFF the GC. Then turn it ON again, This will make the tansmission parameters valid, $ For omer GC models: Using the supped trnsmisin cable, connect the COM oro the prs computer 1 the connector mated “RS- 2320” on theres panel of the CBM-102. ee LapsotutionsGCsolution Operation lm 4s14.2.6 System Configuration Settings After the softwares installed and wiring between your computer andthe GC i completed, enter the it ration) stings (stem configu: Doubles [csotwion Anat. sss eon ‘The det valu, “AS” (Reference Manual patty | assy cere. ‘ck (OK), wath admis” oo isk Sy er Config ea] con New srument> window ll appest oly a inital sens mtb entre “in coosct the ADEDD wo He GC-I7A onthe GCA a0 faye the ™] button, + Column information registration (when using the default value (CRPI-S25-050 or CRPI-W/12-100), simply select either one), ‘open the window wh the GC Papers window fer he communication oct as heen et, and then rer the hardware information aban, Note: Column infomation ss prameer oq fo automatic pesca Tow mai coat. Abo, maximum temperature stings are rogue to tet th ohana. Be sur 1 ene th eotet okamn infomation, For more ab colmninfraton seins, fer to “7 Reptering Colum Information” Inauition, the folowing st + When using an auto-sampler, double-click and transfer the autosampler from [Available Modules] to [Con figureé Modules}. + Forany unit ter tan the GC-2010 aud oer GC med, pen the Wind: Speck Whether ot he AOE Is valle and spc the opti Ink por number oor I) othe CBM to which the ADC ws cones are also required + Double-click each unit on the [Configured Modules:} ree to change individual setings + Ener settings different from those entered using the [Awto>] button > To istribute each unit to either ofthe ines when using the dual-line analysis configuration > When not setting any unison the [Available Modules] tee tothe (Configured Modules] tee For more abou duoc ase etings, fer to “45 Perfoming Duin Ans Note: When ctrng an tional GC asl ivtranon snl system configuration sting (240) Fin sti the Canalis rogram with ke [GCs Aas on, an then use the sme proce sed oe phe Fk OC segs, [A thie ins, be sure 1 selec the cost comirnicaton pert or he OC unis conned If he sre commun pore selected fr maliple GC units that have boca enced othe sc computer colic nay acer causing the unis wo maliae= D __Aferat se setngs, rom svar reinsllin to he abovementioned eng, have bon competed, tis esommende tat you este 2 ckyp coy fal ils in he “Systen” fle eat low the ode fr this software. ‘Specialy since GCSysterConigs fg (or stnamen where | rug) kes conan the syste confguton ifr ‘ion, you can esl restore the cniton sine immed fer instalato by wring theses hak to he “Syste” older ser snag the sofia, Note: Tht he minimum procedure 1 restr the cn ham being los or dstoyd i imponat terete a hackup copy los raed Hes, nln ny inal prt ast es, toes obsined mameatly ster nealing the solar. To prevent 149 B| LabSolutions/GCsolution Operation iit. 3 GCsolution specifications Equipment connectable: + When the GC-2010, GC-I7A V3/V2/VIL, GC-1700, GC-14B, or GC-14C* and up 1 two AOC-204/205720d nits are conteoled, a maximum of 4 detectors each (3 detectors each when the sumpling time is 4 msec) may bbe used. When the GC and up to four AOC-20/20s/20d are controled, 2 detectors/GC (1 detector for each Fine when 2 lines are used) may be used. Note: The GC-14C ds for he Chie mak ny Note: For any GC model eter thn the GC:2010 the CMB-02 is equited fr pt 2 canals pr un when the 2- compatible with high throughput analysis + Single Batch analysis + Additional Tnteruptve analysis “+ Analysis time exteasion + Saupshet Data processing: + Identification methods (windowiband method, absolutelrelaive!mult-e erouping) > Can be feed back to the retention time in the compound table and then corrected automatically. + 6 quantitative calelation methods (based on areabeight) > ares normalization method, corrected area normalization method, corecied area normalization with scale ‘actor, intemal standard method, extemal standard method, and stanéand addition method + Manipulation the result is sutomatically reflected inthe time program, “+ ata comparison + Calibration + T kinds of calibration curves (ovhether or not they passthrough the origin and weighing (1/C, /C2, V/A, V/A?) are selectable) linear, point wo point, quadratic, cubic, mean RF, exponent ‘+ Number of ealiteation curves (16 levels x 10 points) > Calibration curves can be created manually + Concentration or area/height ean be seleced forthe X-axis ofthe calibration eurve, + Creston of report format + 10 reported items, > System Configuration, Sample Information, Method, Chromstogram, Peak Table, Grouping Result, Calibea- tion Curve, Picture, Text, and graphic object linelrectangleelipse) + A layout across multiple pages is supported, and 22 kins of standard templates ave attached, + Preview ive retention time method, and manual RE ee LapsotutionsGCsolution Operation lm \s0File: “+ Method file, report forma ile, and atch file SOP is supported with the template file. ‘+ Data fle (the following information is stored inthe compound structure system) chromatograms, data processing results, methed, report format, batch, system configuration, and status information + File conversion (CLASS-GC10 format, AIA ANDI format, and ASCH format [output only]) GLP/GMP support: + Password security ‘+ Operational restriction related wo user administration and authorized group setings| + Locking fenction ‘+ System cheek (GC selfdiagnoss) ..GC-2010 only + Status information log... GC-2010 only + Software coruption check Ault trail + Data rollback + Alin-one system data fle structure ‘+ Column performance calculation (USP. J, JP2, EMG, EMGSO%, AreaHeight) + QA/QC (statistical ealeulation) Operational support: + Assistant bar + Data explorer + File search + Batch table wizard + On-line man Automatic support: + Automatic creation of dat filenames “+ Automatic saris ofthe GC... The GC-148 only provides automate star. + Automatic stop of butch processing ‘+ User program startup by PrePostrun or criteria triggered run program function in each bate Tine 131 [ll LabSolutions/GCsotution Operation Silt. 4 Error Messages owes ove, ou wo ow owe ows ‘Not Enough Memon Case: Theres incon memory or the stm to fon prosesing army Too many operations scans sun Analysis can eque mere ear) dan vale emg: Clos unnecessary pplication. this des ot so he pole, booths PC he esa the soe ‘Te fe aeay exis Crue: The ile mame rpc ater onthe deve Remedy Specify dieret ten execu the comma ain. Carotid e ile Case: The spied ile carat be ound othe dive Remedy: Use Daa Expert or Windows Explorer verify th exsene and action ofthe i. Execute the command sal, sping ths coucet Me and aca, Dis al (Case: Thee insuc pac n the seo save the He Remedy Delete wesc ils or ack op le se up peo thei Cenot open Method Fie ‘Case: The Method File may bint inant GC window this ot he as, th ile my be crap ems |. “Ty execing the commun again ater clesing the ote Wino 2. We crorcccum agi, the meth les probably corrupted Close all applications end execute Windows Sean Disk Ten teste new method is Connot open Data ile ‘Cause: The aa le maybe in wen anther GCsoaion window: I his isnot ese, he Hl may be erupted Ree | “Tyerecing th commun again aercleing the oer wind 2. Wc eccr agin, the dats le probably corpted, Clos all aplication nd cxeete Windows Sean Dis Cannot open Bae File Case: The Bach ile may ben ase in nether GCsotalon Wind Iehis aa te ese, he ema be erp Remedy: the err aces agin. the Bach les robb corte. Cos ll ppeatons, an exceute Windows Sean ‘Canot open Repo File ‘Case: The Rep Filemay bein wen anoles GCtolation wind: ths i ete cs, th file may be ord Rema Ihe eo seus gaint Report Fils prababhy corrape Close all apctons and exsute Windows Sean Dik, Then cesta new Report File Lab Solutions/GCsolution Operation NN 152ow aves ows 30 san Cute: The Costigan File ny be usin mcr GCaction window. thi i ot he ce, the te my be sermped Remedy [the eur ecu again, th conigratn Sle probably compte, Cs al spits and eco Windows Scan Dik. Thon clos Windows and ebot. Ith cor sil oss, te pation not anaing prone Ty the soliton dese below Cosa sytem applications. Using Explor, open he fllowig dco whi iscated on he ve whee the software stalled. Assume dat his the C: dive} C3GCsaluion Sst In this fle, rename the Sytem Conipution File “GCSysemC omfg fg” 40 "GCS semen) oki He with seamed ext ee drt me). Fall restart the Anais Applian. The Systm Configuration File willbe cre with df vale ‘Not: This me dees alo he System Configuration stings Once normal epzaion i str l f e System ‘Conigution stings must be entered sn, Noe: For more dts on this priced, refer any PC o operating stom mansls which describe Window file ‘pera oars nexpaensd Nindons user do nt sem he pertins ‘Canon eve Method File “Crue: Ether he Matha ils comapid other iinsliscnt memory: Remedy |. “Ty sovg anaher Meth fl 1 this secs ten heist il cored Clos all applications, ar cxccte Wino Sean Disk The ret ne Math ile another Method le canot be saved thre maybe insulin memory Close allunaeeseysplicaons Carnot ave Data Fil Case: Esther dhe ds ile sop or hee is insite. Remedy: 1. Ty sving another aa le 1h Wrnows Sean Dak, 2 Wanoter dats le cant he sad, here may be insulin memory. Claseall neccesary appieaions. is scsi hen the ist is corraped Close al apetons, and excmte Cann sve Bh Fe ‘Cane: Fstber dhe Buch ie corre, or the nse meer: ems |. Tyevingansther th ile, IF thie access hen he it il secoraped Cle Windows San Dk, 2 Wapato Batch leant be sed the may be nsfcet menor: Cla all uaseceary apletons plication, ‘Cant ave Report ile ‘Case: Ester he Report ie scott, oF tres suit memory ere: |. Tiysevingaother Report Fle, This is sucess thon he ist Fis carpe, Clos allappicaion, ond execute Windows SanDisk, Then create new Report File 2. anoter Rep File cans be sve, hee may esi meray, lose al unnecessary appa, Cannot sve Configuration Fle ‘Crue: Ether he configuration ile cored thre licen eee Remedy: |. ‘The configuration ile maybe copied Clos all applications, then execute Windows Sean Dis. St wp 2 ew configuration andsave itt overt the existing ‘Thee may be suicent memory Cloe al ances splistans ‘Cane: Changes have been met the Mato file. Conf whether to save the hangs or lt the file without ving the changes. Remedy: Noneone ons ane aus one ans ona on Le LapsotutionsGCsotution Operation lm 154 ‘Case: Changes have been made toe dt le, Confirm whthr tov the change cr clove he He witha saving the ‘langes. Remedy: Nene Sov cet Bach File ‘Cause: Changes have been made tthe Bate le Conf whether sve the changes olathe without ing the changes. Rema: None Met ile i at fd Remedy: 1. esi te ph rv and flr, 2. Mei the Met ile ae at ie ena four ‘Case: The spied dat ile coud note Found. Remey 1 ee te pth ve afters 2 Verily he dat flee ah fl i nt on ‘Case: The spsified Bach ems: 1. eo te pth rive and folders 2. Mei the Batch ile mame. Report rma ile snot oud ‘Cause: The spciteg repr fomat ecole mtb oun ere: 1. en te ph ve nd folders. 2 Vey the ep fxmat name ile count be fount Configuration ile is ot ou ‘Cause: The System Contiguasin Fle ol a be found. Remedy Reinstall the softare Spit the Configuration Seings asin ‘Cann open Fle Case: The spite le could not Be our Rema: 1. ety me pth ve rtd, 2 Verily the lerame. Cant ave Fe ‘Case: Either he leis errape,o toes insutcent meer. Ree |. Tyswinganaher ile,Hiie tec hen the fir le eorapod. Close all applets sede ‘Windows San Disk, 2 We ot le canot be saved here may be inset menor. Close al unecessary aplication.op one, our one om om owe on ows oe Cause: The spo ile ould ot found Remedy 1. es te path eve an folders 2. Verily the lena Seve Dat File? ‘Case: Changes have ben made fo th ta il, Remedy: Conim wheter to ve he hangs or lose the le witout saving the anges, CLASS-GCIO File has tee sore into GCsotion File, ‘Cane: The slat le was a CLASS-GTO formatThis ness hat he fe was scl comer ae pene ems: None Failed to convert le fom CLASS-GC10 Type ‘Cause: The sels ile was ia CLASS-GCI0 forma, ut oud mat be converted othe Ww i oot. Remedy: Reboot the Cary agsn. ee amp ai pin he le may be compte. you sl ave he CLASS ‘GCIO sofware, verily where ile canbe opened in that version ‘his leis convene Fm prevow Mets, You mst svete a een ems, ‘Cause: The "Save" command ceo! be se fora ile that us just boon convened rm CLASS-GC10 format ers: Save ile wid ne sme wing the “Save Ac" commare ‘This ile i reat-nly. You must save to dierent lena, ‘Cru: This i ae edly tbat No changer ane hee Remedy: ithe save the ile sing a diec ie ame or cane he Save opin ‘Aflerame camo conan any ofthe ollowig strate. \ #7 ‘Case: The le name wisi chaste. Remet Te haracters |" <> |“ ama he wen Windows ile ames Dante thes caractersin he le Specified dive docs at xt Cone: The wrong eve wat pei Remedy arth comet ive name Specified dcctory docs at xis ‘Cause: The wrong dict (Tle) was specified ere ater he ert eer, Sysiid dectary does ot exist. ret directory? Cre: The pce dciony doc at xi Rema: Click on OK t crea the dca, o ikon Cancel canes te operation Failed to crete decir, Cause: Te testy ould et be cet Ree 1. tie the comand asin 2. We cmorr-ecus, ec the folder wing Esplree Insti spe ‘Case: Thetis neuicet sce on he ve species the le cana be sve Remey: |. Thespesia ion the hard dive empty he Rest Bin 2 Back upuoreessary ls and delete fa the dv 155 EEE LabSolutions/GCsolution Operation Sisone one ans nse Cae: Ee th died normation docs note in ie, the ei ori Remedy: Exec te comatd aun. the eno 1-ocus the ie maybe coma Cle al apctns then ‘route Windows Sem Disk ova ile tp Cause: The wrong pe oF Me wa sped Rema: Check tele pe hn sles the eorect ype of ke ‘Tis leis caenty ne ‘Cause: The file icantly being sed by saber wind Remo: Clos th window tha carey aig the file then open the il in, ‘Tis leis curly use Ope and read ony ‘Cause: This le is cure being wed by anther rogram, brit can be pened asa edly Rema: To pen te Me tetany ikon OK [Na When the files oponed witha eel atu any changes th file cant be sved withthe “Save” ‘command To sve the changes, ave the le witha ifrnt ane ing the "Save A” command. To open th file ‘lange and sav vith He same nano, ok onthe Cancel btn cose he aplication which sig the Hea ait the crn pressings completed and then open the file gan ‘Mkeratvly ifthe le riba readonly the read-only rit cold be removed ote i thon exc the ‘commando open the le ‘Tis ile is rite protetd ‘Cae: Ether he es big use nate ppaon othe ie has ean tba preventoverneingthe ae Rema: 1th le being wed by ater pion, close that agp: tn ape he ete ile abe read-only. he rest nly tba could be ove forth le then exe he coms too the fis “Tis ile erie potcted. Open and rn oly Case: Either hei isbsng sey another aplicion oF the Fike as the read-only atibt. Conon wheter 1 open the Bless ead ny Rema: To pen te Mes teal, lk OK, Nate: Whan the files openst-with he read-only abt, any hangestothe file ent he tvs bythe “Save” ‘enmard To sve the changes, ave the le witha iret rane wig the“Save Ar command. To open th le, ‘lange and save tithe same nano kon the Cancel btn clase the aplication which sig the leo ait tthe carn pressings cmpleted and ther open the le aga ‘erates ifthe le riba is Ran thereon abut oul be rroved fr th fil; then excote tbe ‘summa oop he ile Fite with sme ams aloady exis, Cre: Ano file withthe same names the specif lemme xn on th dive. Remeey Specify terete 2. Specify dierent de Overarte? ‘Case: Another ie having the sme are asthe spi name eis tha ie, This message isto verify whether tosive we ne by ovening texting Hi Remedy: Click OK tose the file overurting the existing He The information nthe existing files xt. To sve the ‘leah terete name, ik Cancels the save he le wih he "Save AS" command LL LapsoutionsGCsolution Operation [NN 155owe ow oa ow ous ous ous Cue: Ether thr isinslicion dk space, the leis crite Remedy: Treas he amount of avalable sce o he ikon execu the coma gun. To neous the aout a svalile rae 1. te spesied dive son te had dive empty he Resyle Bin 2 Back up nereesy ls and dle thon fom the deve “camot rea om fi ‘Case: The ile is corp Remedy: Ext the command again. the same eo osu ls al applications then exes Windows Seen Disk Failed ope He Beeus to mat les ae ope, Pease chose uns iles, ‘Cause: The masimum pune pen files is stemined by the tem. Thee may Be sient memo. Remedy: Clone unnecsnry appa, ae lo nina im ‘Crue: Ava el the rings minimum wa ner Remedy: Cesk the allwable soting rng then eter a appropriate vals. To ba the rng 10 GC Hel ‘se above maximum Hn ‘Cause: A va above theange maxima was ened Remedy: Chek the allawale sing range then eter an arora val. To bain the ngs fro GC Help ‘Unable al ‘Came: Anns vale was etre Remedy: Check the allomable eting range or mania umber of carci then clr an propriate va. or information, eferto GC Hel. You cant change this nfrmaton. Your hangs ae inaldated ‘Cause: Anatempt was made eit an seve a parame bathe wer doesnot hve the iho efit at parame Remedy: Cheek he sr nh nthe Ur Aina ea Failed crete window Cae: The sks soma, o thee it insaicet memory. ems |The dk may be corp Clse all applications: then run Windows Scan Ds. Then execute he comand agin, 2 Theremay'e insaicen memory. Close all unecessary aplications. 3. Reinstall he sofa ‘Camotinvoke apieaion ‘Cause: The application could not be srt due to stem problem. Remedy: ry ain. rhe emoreau, hse al patos, a estat Windows then ty Wo eee he command ‘again tthe ost occurs esl the cra No chromatogram i ate Cre: Beaute chromatogram isnt ope he pci processing eld not procod. Remedy: Ope a dat fie, dpa he eroatogram oe processed and selec ‘Carnot aces ogi ‘Case: The og le could nat be sccse Remey: Verity wheter the wer an ae=sthe Log fle diet 157 MEE LabSolutions/GCsolution Operation Sssan oun owe our asso st nse Foiled owt Opemton Log Case: Ether thre isinelicien space onthe pied dive wo rite tthe ile, the wer dos not vee ht to sss the Log le fle. Remedy Verify whether the we a acest tothe Log ile stn ‘To creas th mount of vale pace nthe drive |. Te speci drive ion the hard dive empty he Resyle Bin 2 Bock up aereesuy ils, and delete them fom the dove read backup fort les ‘Cause: ery mom he ese the GCsoution i opened, th comets ofthe og es te comes and backed up. The log ile ise isdleed. Remedy Te compress lg fe rein ema LOA yen\Inomh} ak he Log folder oF te stare insti det Starting to cempres lg fle. ‘Case: Every moth he est ine the GCslution i opened the comets ofthe ges are compresied and backed up. snc L.G(yeanimont)ich inthe Log de fe ona Remedy: The compress lg file is sorein a ie insalstion det. ‘Cant rete file on dink ‘Case: Either hte is insuiient memory, thee nse disk space, rhe dk is wrt ote Ree 1. hee is inicet memary, close unecesry apliction. 2. Vai wheter thee is iii pce onthe Hrd dine “To creas the meu of vate pace othe ar ave 1) Tr thespcted dives onthe hard dive my the Reese Bi. 2) Back upunecessary les, and delete hem fam he dive 3. Remove te wre ter nbure Failed to Loa Dymumie Linke Libra. Cause: The Dynami Linke Livery (DLL) does rat exist, otras be corte, ems |. Te Hlemay be corte, Close al appitins, sl then exsewe Windows Sean Dk 2. Renal the ota ‘Termin by Use Remedy: None Failed copy ie ‘Case: the theres insaiciet pac onthe coy destination ve oan ppliston using with he same mame Remedy hee is ince i sce, nee the vale dn pace ‘Cos the aplication that is sng the ie wih the deat le ae then copy the He Falledo dle le ‘Cane: Father he leo delete des not ext oF is i ted by an aplcaton ere: Verity te existence ofthe ete delet. Cas the plication hat is sing the then delete the fk Foiled crete new projet folder) Cause: 4 projet (oon of the sme name may aay evs Remo Try esting the now flr n= frat fldernae ‘Tis projet (ode) aad exis Case: A projet (flr a hsame are aed exists Remy: ry resting the now flr sng frente nae LL LapsotutionsGCsotution Operation ll | 5%ove oe ose axes ows ose oxen Failed dy Help Cause: The Help le could tbe ound Remedy: Vey thatthe GCreerensc. ch nd Ge_erh files exist in the GCsohion PROGRAM fol. 1tey stot se found, rt he ave Insurers nt connec ‘Case: The anata instrument is ot connected the PC Remey: Verify tate instrument is switched ON nd opeaing normaly Check te cable nd connections. ‘One you ppl aut il math le, you cao ancl he eetion. Apply? ‘Cane: This wing states thatthe at til fnstion cant be incl once thas en speed fr & Meth Rema: Selct "Nor" to speci the Aut Tal function rhe Mata eNO" ence Flesoe operation canes wer ‘Case: The file save operation was cance in progress ems: None ‘Cannot open Bastine Dats Fle ‘Case: The date ile maybe nwo atther GC wind: I this is wat te case, he le may be erupted Reme 1g excatngthe command agin ar losing the other indo, 2 ifthe er acears psn the data le is robably coped, Clos al apiaions and execute Windows Sea Disk Cun: Acrobat Reader mst bein ldo rend one nan ery Isl Acrobat Read along. the procedice writen n Opention Man Sov cue Report Format in Daa Fle? ‘Came: Changes have been mado th repo frat pat in ct fe, Remedy: Conim wheter sive the hangs of lose he window without saving he change. at File shen oovertnto ASC ile (Cane; Thin means thatthe Gaus dat ie was accel converted, Remey None Fall cont ile om Data File ‘Cruse: The sel file was in Coton rat cold nee conven tothe new fil fom Remedy Reboot the PC al ty again. the temp is api, he ile may become You ca vey whether the ile ‘ante opened GCsoaion | al Files bon onveri nto ATA AND Fl, ‘Case: This means th the GCiutons dt fle was suse omnes Remedy: None Fall comer fle om Dat File ‘Cane: The select file wa a Colao oahu could nee conver the new efor Remey: Root the PC ane ty asin. the temp sai h ile maybe compe. You can ven whether he ile ‘ante opened GCs AIA ANDI Fi as bon conver ito Das Fil, ‘Cane: This ean tha the AIA ANDI ile wa aecesflly conver Remedy: None Fail to comser ile om ATA ANDI Fie ‘Cause: The select le was ia ALA ANDI oma, but coud nae converted he nel oa. Remedy: Reboot he PC ar ry again. the atm fais gin he le mas Be coma 159 EEE LabSolutions/GCsolution Operation Ssone ones rain aw Data prt inthe a le use: 4 di sro occured during dats souistion. Remedy Ipssibs, do vt prem any ott operations during austin, Disable ny sercemaers and pamer ‘The sau gis ot ound inthe a Tie ‘Cause: The sats modules no cad inthe syste contgurain athe ine of aa suston amot be sd in toed, Remedy Verify thatthe relevant mods ae comet config when perfrming dt scquison, Peak ntpation Pas ot en va ‘Came: Peakinepration has ot hen performed for stn Remedy Uni th peas ave bonita iter uanitain or manual peak procsing an be prrmed Perfo pek negation rom the Qulttve men in he De dais window ak Metin hn ot been nck ‘Case: Peak identication has nt ben performed fr his dt. Remedy: Ul he peaks ve ben ied. eter gusnitaton nor mana peak processing ca epee Perfo peak entiation ot the Qualtauve edu in the Dat nals window. Ta GCsolon, pak Ke eens pevfomed automatically ding the pe eration proces Quine Prosesing has ot been nveke, ‘Came: Quattion ha een permed fort ct Remedy Quanta ha he Quaisve men in the Date Anais wind. Cause: The data asthe gutted without callvation curve Remedy: Ether cet calibration curve wih Batch processing or rex one in the Calvan Civ window (ee the GC Hap fetter Wap enfcaton hasbeen perform Ith ed have no been ent, ‘tthe quaitaon paar nd guuniaton abe so th peak eteaon ean be eopducted then ode the Cao Teal Saar Pes ‘Cane: The pen ssid withthe nals as nol Been dete Remo the nema Stender Method i sled asthe Qunttave Meo, the neal tnd peak mst bo etic i order to eterat elation crs are eel onsen Inthe Compan Table ea he 1D hm th tral stander (ISTD or ISTD & Reterece: thon heck tht peak migeaton al pak sentteation fave en condi fr ht ID he Do nai wn Irth peaks not sen dtc, change the pak itgraton ramets, Tete peak hasten dete, but ied oe dete check the iene parameters. panic. iareferece ton wast crs hat he on ada matches, Palle dey peak ‘Cae: The peak was no ene ems 1. Vey te retain tein he Compr Table 2 Cer ta the pk rea fmt the iim peaks. ‘heeft em, Cane: Nothing hae hon ete pin Rema Paste he eprom cost nthe rpot ot il in he item ropes, sl “Prat om.” Cue: A significant cor occured daring pek detton “Thre maybe nsicient memory Remedy: Clonal nnccssary appar. ee LapsotutionsGCsolution Operation (NN 60anon. oner, oor oar oats art Cause: The pk Type isirconse Remedy: Check the Type inthe Compoand Tablet pict, when the Tera Sand Metin is pst an ‘rua stead ected. ‘Averaging repetitions fron point exceeds (10), ‘Cause: More than 10 sands spi these ve ems: The manimum umber of repetition for averaging is 10. When using. tte, select Standard inlize Calton Cure) a he Type cla te preva aiaton tre. tern, new sand il nnn te soragod_ Normal the Fist sandra the Hach Table soul italic the clan care oie ring Pea Integration proces. ‘Cause: Peakintpaton was ot completed dt isuicieat memory. ems: 1. Execute peak tegration aun. 2. Wiiecrorraccus, sory the pk itegton panies ard mice the anor of pak a be detected Dat file nt eps. Remedy: Te caiman point des not ei or the speifidcalieaion curve A calibration curve anna be eited by removing scairaton pot Ite Calivation Carve wind, al ante libration oi th alia ure. Or [presale the cali curve ing baich roca ‘Theres no Sample Anau ‘Case: The Sample Amount as not een seit and guantation cao! be ero Remedy: Ber value than 0 fr Supe Arson. Fo Batch Processing. setthe Sample Armoant inthe Batch “ube I the Data dnt wing open the Sale etnmato, an spect Sample Amount. The qataton requtesa don facto Veni that is aes ntsc 0 “Te fel concerti oan with he allowing equi, Fina concenraton = (Concern akeuated rom calibration curve} (Dlation ater (Sample Amon) ‘Thr isoselested peak ‘Cause: The peak o Be proceed ha ot Ben select Remedy Select tbe are! pak Caleta concentration fr al compounds? ‘Came: Confirm whet seul the concentmtions. Yes" recommended Alhoagh his oo oid i te data isassoviatod witha standard te prosesing ake vey ie ie. ems: None “Tere so detected oak. ‘Case: No peaks have been detected Remeay: Voy the pea tegration parameters. Dares the Wid a Sloe ales othe peak tect, Caue: The pres of generating the GC pranets was cancelled adhe parameters Were al updated Remedy: Tere inno Compound Table, Crests 3 Compound Table Inna Standard Compounds) requred wicn wing Inemal Sandal Mead ‘Case: Alou the Ira Sandied Meio was see asthe Quantve Meio hee sno itera andr sted i the Compl Tae, Remey: Specify anintomal sanar in he Compound Table, The Type shulé eee ISTD or ISTDAReL 161 EEE LabSolutions/GCsolution Operation Ssoun oar ona Cute: The manera exceed te min nab can be rotted one chrontoga (100), Remedy Reduce te mune of peaks processed by using oof th following proces Increase the Slope vale inthe Peak Intgrition Parcs. ‘Using he ONIOFF function ina Pe Integration Time Program, suspend peak dtetion nan ara of the chromatogram ‘whee no signiicue peaks ete ‘The set parameter aerate tall shane ‘Cane: Coniem wheter to copy the pes intertion parameter heart hantel ll he esol Remedy Tis ne dpe Reserved fi tee. ‘Ony one inet standard ean te reps in a TS group ‘Caos: Mute nen stands wer signet single Soon. Remedy The ISTD Grey mamber specie the Compound Table group ompands by STD group Spey erly one intl standapor group. Quanta is pefonned wth he merlot group. “Thr orgie intra andi th 1S group Cus: No itera sania was gist to the up. Remedy: The ISTD Group nanber specif in the Compound Table groups om pads by IST group. Spier one incotl stance group. Quan i pefonned with he neal standart group. eral standard compounds nt required ‘Case: the ral Stade Method wa not speed the Quamtve Mette no ne specy an inert, Remy: ooo se the tera and a Compound Table Type Peas set onsen, ‘Cau: Wihoa a specie concent, he cllation curve cenet be gente ere: Each vin the Compouné Table requires a concentaion. Except fr Level evalu of 0 aan be st. Peas et nd range nthe Qunitation TB. Case: Henteuon pocesing cmt te petfoned because uband tine with wasnt pei Rema: When Hens eat fete Heian Method a Band Te aie Spey he Han ein the ‘Compo Table Pols witha ecmlon une wit te band wl be ate, rte Compound Table Banca shin, let fo espa em th Table Sgt Colum Order ta Pease st 18 grup number. Cause: No1S group umber as bon specified ine Compound Tae Remedy: The ISTD Group number specif in the Compound Table groups ompounds by IST group. Spit ery one nl standard per hou. Quan is pefonned ih he ines stdad o ago4p. Copy Time Program alo? ‘Case: Coie wheter oop te Tame Prog aloft tants omg wit the Pe nteration Parameters o he caren ehana 12 Remedy This ist carrey played, Renee fr ft we, “The Reteton Time a coca inthe Compound Table ‘Coun: Boas erifeation was cco pefomed, the tet in othe star wan pete the Compound Table ems: Nene Exceds umber faa cave levels sein Meta. ‘Cause: Wher the cation cue was appli was nt cnet With he miu aber felaton pln se ine Mstod. ere Crete ew cliraton cre with Hash proces, Lab Solutions/GCsolution Operation HNN 162Case: Who the quntative pramstr and Compound Table te etd th clan curve ay be they al corspond Remedy: This i cnfrmation mesa. A24 Some IDs have wo compound name. These IDs willbe deleted. Do you want comin? ‘Cause: Mer tbe Compound Table was ee aso TD was ud without compoure me Remey: compound names eqited fo the compound o be recognize inthe ble. Er he compound ame, ows ‘without compound mew be deleted 0428 Quantitative Parameter andr Compound Tale n Dat ae dre rm ths ie Mesh Compound Table Rema: For allt oregon, he quantitative params infrmation re oped tothe ds fe, 9426 No nfonmation nthe Compound Tabs, ‘Cause: Procesing cannot cominuc because th Compound Tal information has et been eee Remedy: Ener the wet compound intsmation i the Compound Table. PART The Compound Table iinet mode ‘Case: Inthe Data Anas an Calton Curve windows whe he Compound Tele sin Et Mode, the window Remy: Choose wht to sve the crn cones fhe dtd Compo Table, ro delat any changes that were the Metbed the Compound Table ad the clan ure DA29 Plast RF ‘Case: RF(-Response Fst) mist not be on [RF] column of Compound Tbk, whe the Cllvation Curve Fite ‘eset "Manul RP Remedy: Setcoret RF vale AS® tase Reference Compouis inane of Relative Rotaton Tie nication Maha. Cause: tent one reference compound is ses in [yp] cain of compound ble for "Relative Ras Peak eenicaton Metoe Remy: Set Referens” or ISTDAReferese” to [yp cl compo be, OAS1 Some Cabbraton Cures ae deleted. Do you wana continue? Cause: Nomally cain curve i clelted wt pl dtu. Changing pramet roundealbation uve singe at mas rest nen clbaon core Remedy: Conia “Yes of No", ASD Group Calbaon is upper For oka Stra’ Method ‘Cau: This combanton of eting nt supported Remey: None AR. Group Calibration i suppor Man RE ‘Cru: This combination of tin Remedy: Nene ASS “Force Through can't bested for exponen cure Rema: Make another skin. ARG Pleasset more hin 2 at of Ca. Levee or expone ce Case: ThisieMatematil resto, Rema: Set 2 or ioteCliraton Level amber not suppor 163 (HN LabSolutions/GCsotution Operation Siecor can, as oe Case: 4 noreistent comand as specified within a GC Time Progam Reidy Enter command fom he dopo i, gal prose ‘Cruse: Ther sa rae vale emo in the Tne Program or Flaw Program. Remedy: Cheek values corm thecror Fr example fa postive ae vale the ven temperate is twalover vale that the carrentals the tempernare ate cannot be positNe, GC temperature program enced Ma. ime ‘Case: The program ime pein the GC program excel the maximum allowable dns int Remo Change the sting tha it donot ese the maximum in Sutin et tr than Ed tine Case: The staring ie value is rete than beeing ime value Remedy: Change the suring ins 5 that oceus ear the ead ine ‘The vate of instrament parame n method ut of range. ‘Cause: There isany exceed vals for its sing ange of inset preter. Rema: Chk the ranges and st comet sales (90 Corman Hadar i ot count ‘Case: A communications fire prevented comnicaton wih the GC. Rema: Check thecal, canocons, an th ponerse td sup. AOC Cammanicton Hardware snot connec. ‘Cause: A comemnicaons fire prevented eommeaticn withthe AOC ern: Check thecal, snnsstions, nthe power swith nd AOC Astosaplr is ot orm ‘Case: The Sysco Configuration sctiags pci tht wn AOC autosampler acu i connected tothe AOC ato intr, bt the arouse may nt actly be eoancied Reme: Vety adhe ADC autosampler crests acm connectd the suum and He eco he ‘canna, vai parame en ‘Caos: There wns anton see armors whic cannot us has on the ADC stings inthe Systm Coatigurtin. Remedy Verify thatthe ADC Method arms ae st within eco get. Also wet the i nets ‘Volume, Numer of Maint, paramctens hve been et corel he singe sample rn Rach Tae Invi Line ‘Cec: rocening nat tempting a dl in the Aral Lin wick dacs nat upon hist of proces Remedy: Verify thatthe Analyte ova Ijeston Vlene ine stings in System Coniguation ae set conse ‘Case: The ston vole valu inthe Bach is out he sting ngs Remedy: Set an appropriate vale “The hardware conigato i diferent om the curt nar! sontiguaben ‘Coun: The System Configuration pci i ileet om he acl instrument coafguation Remedy Revise the Sytem Configuration stings tomate he seal entation. Le LapsotutionsGCsolution Operation (N61Case: Ths messages great posure does rie wha a eri ine eid. The lowing are posible eae, “The aye ears as leak ihre clung ot eammetd, t's broken, ‘Carer gsis ot own. Bter he as ylndr smyth eid mun ale is esd "When this message i splayed the soln oven hes i attomaly switched of hoy tears, the flow enrol is iced off Remedy Mie limiting the cause of he xo, es the CLEAR Ke e he GC Keypad. The ow contol estes ‘pcan andthe ove eae tsa, 95 Dect ore. Tam fT GC poner ‘Cause: The hemocouple as acted he overeating Fotction cuit. Al ofthe heated zones are turned somatic This menage a dpe the herman bis Oa Remedy: Tum of the GC an contact your Shimada Service Represetive D8 GC Inet i ot sonnet ‘Case: This means connctn file bersen GC 9 PC Remedy: Aint hk he GC power sappy heal omecton of ansmison cable, device ting i Window side ‘Tn checthewansmssion or sting a [estrmet] en of [83stem Congnreton}- [Walle Ui) Remedy: Ibis doesnt solve this problem, cont your Shimadzu Service Repesetatv. 0A Communication ts wens ‘Cause: Communication por swt eee Remedy Set the proper cmmaniaon pot is [Sytem Conigration [velbe Uni] Te. Israme ico HC AOC ostunents not comet Conf a conection been CBM and AOC, and rest the CBM and GC. ‘Cre: Sytem Contguation sting arsed AOC comet nat match fr etal configuration Remy: Cesk te camsctonofrananision cele tween CBM and AOC, or seth raper valu to AOC soarecten| ‘heck box on under he Insane Propet window 81 Cannot dnd system pogans. ‘Cause: The system program les necessary or software operation could nat oun Remedy Reis the GCsoation 82. Senna yormters ‘Cone: Thin rite ney ndct tht th tem unstable Remedy: Rebot he PC and esa the star 85. Soe ad rameter ‘Cause: Thisenoris rare. lay indict that he sytem unstable Remedy Reboot he PC ar restate star 84 Recs aboxmaly-frmated ow data ‘Crue: Ancor ecu rng data anemic, ethers may bea problem withthe GC tem, Remedy: Hibs mess occrs in dig ta sequin, rest the GC DAF Cart comes th OC. “Case: The conneton was broken when the PC ed somes he nsranent.| Remedy: Reboot the PC. De3 Fido crete ts sequstion had ‘Cae: Due inset memo he program cael anton pop Remedy: Clonal unnecessary appicaions oe up a uch avilable rorya possible, 0F¥0 Filedto cones the nar ‘Case: The connection sale Beas communication can be sled with the samen, ere: Cheek the cable an power sare 165 lll LabSolutions/GCsolution Opera1001 ss Act ln ontiguntos i liiren fm the ein sytem cofiaton i (Case: The ine cofguration change on OC sie om st sting ia tem configuration ile Remedy: Aesth mesg, he confirming wil ome up toss one of them. No ID hasbeen eect ‘Case: For the information tobe displayed compexnd must esl rom the Compound Tobe Remedy: Select te componne ody cr pees No dat ile has hen slestd ‘Cause: Ada fleas not een let for dil processing Rema Solos dati rom the dase. Compo able is mp: ‘Case: Processing cannot be conned because he compound wb Fumes have not ee pie, ere: Faith compoana able No dt ile has eon incl the easton imation, Crue: Tere inn dt lectin the caliton cu information, Remedy Te cainatin curve was ot rated prope Re-reae the elibaton curse sr in the Bath Tale ot Callration Care wind “This tie rangetsshonter than dat collection interval ‘Case: The spect aa collection ners es an the ang tin te mana peak ine ration stings tener Remedy: Selesta wider ange ‘Case: Confirm wheter fo emave the dt ile fom he ealation ont inthe sivation cue. ems: Upon confiemation, th in ile rove, Allain pons ram ha aa ie ae removed hen he ‘ibation curve fesse ‘Canta the slot files. Adding ies would xcced maximum numberof reins (Cate: The mina rer of lian ave pins por ee i 1. Remedy, When using teh, set tad hte Carton Cure) asthe Type to ler he revios clan ‘ave Oikerws, now sans wlleonbeucts be averaged Neral the Bastard nthe Batch Tale should ivealie the albation cave. Calation Cure ntoemation (Quant Paramcs Cmmpoun Tab) of as Heder en inrmation neta ‘le. Copy the information ofthe method feo he dat ie wo make them mae? ‘Cane: The Caliaton Cave tnormatin[Ouamaiative Parte, Compan Tole doesn mach he orrtion the dale. procesing cant be perro. ere: Cay he information om te metho ile tthe data es hat all he information corresponds corey "Wh nbd svete thd ie sng with hed le, ‘Cae: Because the compound lei in Et Mode, les cannot be saved x ese Rema Sith th Compound Taleo View Moss thn rf he operation gin. Setet new bu sage. Case: Inappropriate sete. Rema Use the mouse ag om the tain same tothe basic cad ine ‘Carot execute his process ects ile) ar rea ony ‘Cane: The sme ile maybe open in ancter window, oth ile nib i edly. Saving or processing cannot be permed Rema Clos the ile tat nope inthe thr wind, or amove th ea aly tats ee LapsotutionsGCsotution Operation (NN 165008 ima ms 040 wat Cun: Ta change no parameter ei eof Mad view in GC Res Time Anyi cen, dt mst be onde Remedy: Lond da let srcn and eset the power of PC. Thencheck he program wih using (Tol) - [Program Check enti Failed upload he Ge parame ‘Crus: At the Angst] Upload GC parometers in GC Real Te Analyse sree, he GC pamela oes nt performed Remedy: Close sercen nd rest he power PC. Then check he program with wing [Tol] [Program Chest into, GC Ere, Remedy: The message, posted by GC. sallowing this message, Check te dseriion wound “Cause” or “Reme" a Instron Mana for GC isl all stb sample intoration. ‘Cause: Seng sample inormation to GC seminned with ro. ered Tam of theater and coat the computer te prblen sl ess co! ye Shima Sere Representative Conan Ee. Cue: Communistion Emor osu in tensiston poole Remedy: Tum of the antramci and chou the cout the prblen sl sn coat your Shia Service Represent Doveod the Tsranent Parameters? (OK: Dowlad and System On, Canc System On ol) ‘Cause: Isrumsnt Params dawnload his rot dane or Some params have changed af st dowloaing. ere: Conim “OK or Canc” De you want stp GC Program sinutansousy? ‘Cru: uring ttchorsngle dt scion, shor proce perform. Rema Click "Yes" normaly oF “Cancel to continue GC pow oly ‘GC Program sated when dt equsion dd sandy ‘Case: GC has posted “Uaknown enor Remedy: Tam of the astrumert and reboot the computer, the prblen sil pests cot your Shima Service Repeseave Do you save the charge stop time in Method ile? Case: Forse dts segustion lial Stop Tae ar stat data acquis ieee etl Stop Tie at suspension Rema Conia aput ew Sap Tine it mato file ee LapsotutionsGCsolution Operation lm 70