Mechatronics Module 2-Mems
Mechatronics Module 2-Mems
ME 407 – MECHATRONICS
MODULE III
Micro Electro Mechanical Systems (MEMS): Fabrication: Deposition, Lithography
Micromachining methods for MEMS, Deep Reactive Ion Etching (DRIE) and LIGA
processes.
Principle, fabrication and working of MEMS based pressure sensor, accelerometer and
gyroscope.
Although MEMS is also referred to as Micro Systems Technology (MST), strictly speaking,
MEMS is a process technology used to create these tiny mechanical devices or systems, and
as a result, it is a subset of MST.
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Transducer:- A transducer is a device that transforms one form of signal or energy into another
form. The term transducer can therefore be used to include both sensors and actuators and is the
most generic and widely used term in MEMS.
Sensor:- A sensor is a device that measures information from a surrounding environment and
provides an electrical output signal in response to the parameter it measured. The major energy
domains include:
Actuator:- An actuator is a device that converts an electrical signal into an action. It can create a
force to manipulate itself, other mechanical devices, or the surrounding environment to perform
some useful function.
APPLICATIONS OF MEMS
Automotive:- Automotive airbag sensor, Internal navigation sensors, Brake force sensor and
suspension control accelerometers, Fuel level and vapour pressure sensor.
Electronics:- Disk drive heads, Earthquake sensors, Inkjet printer head, Overhead projection
display.
Medical:- Medical pressure sensor, Implanted pressure sensor, Pacemakers
Communications:- Fibre – optic network components, RF relay switches and filters, Splitters
and couplers, Voltage controlled oscillators
Defence:- Aircraft control, Embedded sensors, Data storage, Arming systems, Surveillance
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MEMS FABRICATION
MATERIALS USED IN MEMS FABRICATION
SILICON
Silicon is the material used to create most integrated circuits used in consumer electronics in
the modern world. It is also an attractive material for the production of MEMS, as it displays
many advantageous mechanical and chemical properties.
Single crystalline silicon is an almost perfect Hookean material. This means that when
silicon is bent there is virtually no hysteresis and hence almost no energy loss.
This property makes it to the ideal material, where many small motions and high reliability
are demanded, as silicon displays very little fatigue and can achieve service lifetimes in the
range of billions to trillions of cycles.
POLYMERS
Even though the electronics industry provides an economy of scale for the silicon industry,
crystalline silicon is still a complex and relatively expensive material to be produced.
Polymers on the other hand can be produced in huge volumes, with a great variety of
material characteristics.
MEMS devices can be made from polymers by processes such as injection moulding,
embossing or stereolithography and are especially well suited to micro fluidic applications
such as disposable blood testing cartridges.
METALS
Metals can also be used to create MEMS elements. While metals do not have some of the
advantages displayed by silicon in terms of mechanical properties, when used within their
limitations, metals can exhibit very high degrees of reliability.
Metals can be deposited by electroplating, evaporation, and sputtering processes. Commonly
used metals include gold, nickel, aluminium, copper, chromium, titanium, tungsten,
platinum, and silver.
CERAMICS
The nitrides of silicon, aluminium and titanium as well as silicon carbide and other ceramics
are increasingly applied in MEMS fabrication due to advantageous combinations of material
properties.
OTHER MATERIALS
Besides silicon also some metals and polymers can be used to form MEMS elements or
functional layers.
The common fabrication processes for metals such as gold, nickel, copper, titanium, silver
and several more are electroplating, evaporation and sputter deposition.
Polymeric MEMS can be produced by using injection moulding, embossing or stereo
lithography. These MEMS devices are especially well suited to micro fluidic applications
such as disposable blood testing cartridge.
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2. Patterning
Lithography
Photolithography
3. Ion implantation
4. Diffusion
5. Oxidation
Wet
Dry
LITHOGRAPHY
produces a thin layer of photoresist on the wafer surface. Chemicals commonly used as
photoresists are; poly methyl methacrylate (PMMA), polymethyl glutarimide (PMGI) etc.
o Prebaking/ Softbaking – After applying the photoresist to the desired thickness, a softbake
is used to remove the residual solvents of the photoresist. Photoresist is prebaked at 900C to
1000C for 5 – 30 minutes. After the softbaking, the wafer is cooled to room temperature.
o Mask alignment - A photomask, consisting of a glass plate (transparent) coated with a
chromium pattern (opaque), is then placed in contact with the photoresist coated surface.
"Align" is one of the most critical steps in the entire microsystems fabrication process. A
misalignment of one micron or smaller can destroy the device and all the devices on the
wafer. Each layer must be aligned properly and within specifications to the previous layers
and subsequent layers
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o Exposure - The wafer is exposed to the ultraviolet radiation transferring the pattern on the
mask to the photoresist. The wafer is exposed by UV (ultraviolet) from a light source
traveling through the mask to the resist. A chemical reaction occurs between the resist and
the light. Only those areas not protected by the mask undergo a chemical reaction.
o Development - Portions of the photoresist are dissolved by a chemical developer. With
positive resist, the exposed resist is dissolved while the unexposed resist remains on the
wafer. With negative resist, the unexposed resist is dissolved while the exposed resist
remains. Most commonly used developer is tetra methyl ammonium hydroxide.
o Hard Baking – It hardens the photoresist for the next process. The temperature of the
hardbaking is higher than that of the softbaking after coat (1200C – 1500C). After the
hardbaking the wafer is cooled to room temperature.
o Etching – It is performed either using wet chemicals such as acids or using dry etching. The
photoresist wall resists the etching and protects the material covered by the resist.
o Stripping – After etching the remaining photoresist is removed by wet or dry stripping.
Commonly used stripping medium are phenol based organic compounds like acetone.
DEPOSITION
CHEMICAL VAPOUR DEPOSITION
(b) Organic materials: Al2O3, polysilicon, SiO2, Si3N4, piezoelectric ZnO, SMA TiNi
CVD involves the flow of a gas containing diffused reactants (normally in vapor form) over
the hot substrate surface.
The gas that carries the reactants is called “carrier gas”.
The “diffused” reactants are foreign material that needed to be deposited on the substrate
surface.
The carrier gas and the reactant flow over the hot substrate surface, the energy supplied by
the surface temperature provoke chemical reactions of the reactants that form films during
and after the reactions.
The by-products of the chemical reactions are then let to the vent.
Various types of CVD reactors are built to perform the CVD processes (horizontal and
vertical).
EVAPORATION
Evaporation involves two basic processes: a hot source material evaporates and condenses
on the substrate. It resembles the familiar process by which liquid water appears on the lid of
a boiling pot.
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Evaporation takes place in a vacuum, i.e. vapours other than the source material are almost
entirely removed before the process begins. In high vacuum (with a long mean free path),
evaporated particles can travel directly to the deposition target without colliding with the
background gas.
Resistive heating method is used for heating the target material. Voltage and current is
manually controlled.
Electron beam can also be used for heating the target material.
SPUTTERING
PVD is used to deposit titanium, titanium nitrate, tantalum, tantalum nitrate, aluminum and a
very thin film of copper called seed layer.
The PVD equipment will be about 4 ft in height and 4 ft in diameter. The material to be
deposited (e.g. titanium) will be at the top, as shown in schematic Fig 3.6.
The tungsten will be in the form of a disc of 1 inch thickness and 5 or 6 inches diameter. At
the bottom, silicon wafer will be kept.
Apart from these, there will be facilities to allow gases into the chamber and to evacuate the
chamber with vacuum pump and electrical connections to apply very high voltage (of the
order of 10000 V).
The negative plate will be near the tungsten and the positive plate will be near the wafer.
Tungsten (or any other material in its place) is called target.
First the air in the chamber must be removed and vacuum must be created. Then argon gas
sent inside and a low pressure will be maintained.
If high voltage is applied to the plates, a plasma will be generated. The plasma will have
electrons and positive argon ions. The plasma cannot be generated by normal 230 volts.
The positive argon ions will be attracted towards the negative plate. They will move towards
the negative plates and hit the tungsten with high force. That is why tungsten is called target
in this process.
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Since the argon ions impinge on the target with large force, some of the target atoms will
break and come out, as shown in Fig 3.7.
The number of tungsten atoms bounce back for each argon ion hitting the target is
called sputtering yield. It depends on the speed of the argon ions, the angle of the impact and
also on the bond strength of the target.
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The atoms from the target will come towards the wafer with some force. Not all of them will
deposit on the wafer. Some will be deposited, while some will bounce back. Some may even
bounce back and remove some of the materials already deposited on the wafer.
Among the tungsten atoms that fall on the wafer, the fraction that stick to the wafer is called
sticking coefficient. If all the atoms that fall on the wafer stick to it, then the sticking
coefficient is one. If none of them stick, then the sticking coefficient is zero. Typically, the
sticking coefficient is about 0.7 to 0.8.
DEPOSITION BY EXPITAXY
Both CVD and PVD processes are used to deposit dissimilar materials on the silicon
substrate surfaces. Epitaxy deposition process is used to deposit polysilicon films on silicon
substrate surfaces.
Most polisilicons are doped pure silicon crystals randomly oriented. They are used to
conduct electricity at desired locations on silicon substrates.
This process is similar to CVD with carrier gas with reactants that release the same material
as the substrates.
Reactor is very similar to those used in CVD, except that many of the carrier gas used is H2.
For safety reason, N2 gas is used to drive out any O2 gas in the system before the process
begins.
ETCHING
Bulk micromachining involves the removal of part of the bulk substrate. It is a subtractive
process that uses wet anisotropic etching or a dry etching method such as reactive ion
etching (RIE), to create large pits, grooves and channels.
Materials typically used for wet etching include silicon and quartz, while dry etching is
typically used with silicon, metals, plastics and ceramics.
WET ETCHING
Wet Etching is an etching process that utilizes liquid chemicals or etchants to remove
materials from the wafer, usually in specific patterns defined by photoresist masks on the
wafer.
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In wet etching, the wafers are immersed in a tank of the etchant (mix of chemicals. There is
a chemical reaction between the wafer surface and the etchants that helps in material
removal.
Either a photoresist layer or a hard mask like oxide or nitride layer is used to protect the rest
of the wafer.
The time for etching depends on the amount and type of material that needs to be removed.
KOH (potassium hydroxide) is a common etchant used to remove Si. Usually, 30% KOH
solution is used, which has a etch rate of ∼ 100 µm/hr at 90 ◦C.
After etching, the wafers are rinsed, usually in DI water, for removal of etchant and then
finally dried.
DRY ETCHING
Dry etching refers to the removal of material, typically a masked pattern of semiconductor
material, by exposing the material to a bombardment of ions (usually a plasma of reactive
gases such as fluorocarbons, oxygen, chlorine, boron trichloride; sometimes with addition of
nitrogen, argon, helium and other gases) that dislodge portions of the material from the
exposed surface.
Dry etching relies on vapour phase or plasma-based methods of etching using suitably
reactive gases or vapours usually at high temperatures.
The most common form for MEMS is reactive ion etching (RIE) which utilizes additional
energy in the form of radio frequency (RF) power to drive the chemical reaction.
Energetic ions are accelerated towards the material to be etched within a plasma phase
supplying the additional energy needed for the reaction.
As a result the etching can occur at much lower temperatures (typically 150º - 250ºC,
sometimes room temperature) than those usually needed (above 1000ºC).
RIE is not limited by the crystal planes in the silicon, and as a result, deep trenches and pits,
or arbitrary shapes with vertical walls can be etched.
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Deep Reactive Ion Etching (DRIE) is a much higher-aspect-ratio etching method that
involves an alternating process of high-density plasma etching (as in RIE) and protective
polymer deposition to achieve greater aspect ratios.
Etch rates depend on time, concentration, temperature and material to be etched. To date
there are no universally accepted master equations to predict etch performance and
behaviour.
Advantages of DRIE
Fine resolution
High aspect ratio
High etch rate
High sensitivity and precision
Disadvantages of DRIE
Applications of DRIE
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ION IMPLANTATION
It is physical process used to dope silicon substrates.
It involves “forcing” free charge-carrying ionized atoms of boron, Phosphorous or Arsenic
into silicon crystals.
These ions associated with sufficiently high kinetic energy will be penetrated into the silicon
substrate. Physical process is illustrated as follows:
DIFFUSION
Diffusion is another common technique for doping silicon substrates. Unlike ion
implantation, diffusion takes place at high temperature.
Diffusion is a chemical process. The profile of the spread of dopant in silicon by diffusion is
different from that by ion implantation:
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OXIDATION
SiO2 is an important element in MEMS and microsystems. Major application of SiO2 layers
or films are:
o To be used as thermal insulation media
o To be used as dielectric layers for electrical insulation
SiO2 can be produced over the surface of silicon substrates either by:
o Chemical vapor deposition (CVD)
o Growing SiO2 with dry O2 in the air, or wet steam by the following two
chemical reactions at high temperature:
Si (solid) + O2 (gas) → SiO2 (solid)
Si (solid) + 2H2O (steam) → SiO2 (solid) + 2H2 (gas)
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SURFACE MICROMACHINING
Surface micromachining is a process that uses thin film layers deposited on the surface of a
substrate to construct structural components for MEMS. Unlike bulk micromachining that
builds components within a substrate, surface micromachining builds on top of the substrate.
Most commonly used materials for surface micromachining:
Substrate: silicon
Sacrificial material: SiO2 or phosphosilicate glass (PSG) s
Structural material: polysilicon
The dimensions of these surface micromachined structures can be several orders of
magnitude smaller than bulk-micromachined structures.
The prime advantage of surface-micromachined structures is their easy integration with IC
components, because the wafer is also the working area for IC elements.
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LIGA PROCESS
Step-1
Coat thick photoresist (300 m to > 500 m) on a substrate with an electrically conductive
surface.
Step-2 Irradiation
X-ray lithography with extended exposure from highly collimated X-radiation to penetrate
thick Resist with well- defined sidewalls.
Irradiation involves exposing a thick layer of resist to high-energy beam of x-rays from a
synchrotron.
The mask membrane is normally a low atomic number material such as diamond, beryllium,
or a thin membrane of a higher atomic number material such as silicon or silicon carbide.
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Step-3: Development
In this step the pattern is etched into the resist substrate by the use of x- rays and desired
structure are formed.
Step-4: Electroforming
Metal electroplated on the exposed conductive substrate surface. Electroforming is the same
as electroplating.
Electroforming suggests that the plating is used to create an actual metal component
Step-5
Advantages of LIGA
No diffraction effect
Simple to use
Uniform refraction pattern
High resolution for small feature size
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Disadvantages of LIGA
Distortion in absorber
Mask is expensive to produce
Slow and complicated process
Applications of LIGA
Two elements have their primary axes parallel to the membrane edge, resulting in a decrease
in resistance with membrane bending. The other two resistors have their axes perpendicular
to the edge, which causes the resistance to increase with the pressure load.
It is necessary that the four piezoresistors have identical resistances in the absence of applied
pressure. Any mismatch in resistance, even one caused by temperature, causes an imbalance
in the Wheatstone bridge. The resulting output reading is known as zero offset, and is
undesirable.
After completing front surface, we need to rotate the wafer and the same process is repeated
to the other side also. Lift off resist coat is poured and by rotating the surface, it allows to
spread all along the surface.
Photo resist coating is done by the same as above and then it is undergone in to a LOR and
PR exposure by UV light through a mask and then rinsed in the developer solution (LOR
and PR develop.).
Then, deposition process takes place by chrome and gold disposition. It is a physical vapour
deposition method. Then PR strip lift of by acetone solution is done and then LOR strip off
is done finally through KOH anisotropic etching method.
MEMS pressure sensor is created/ fabricated by placing a pyrex 7740 glass anodic bonding
on the surface.
The mass develops a force which is given by the D‟Alembert‟s inertial force equation
F= m*a.
This force displaces the spring by a distance x. Hence the total force externally is balanced
by the sum of internal forces given by,
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Stress is the defined as the force per unit area acting on the surface of a differential volume
element of a solid body.
Spring Constant (proportionality constant) that relates the force and the displacement in
Hooke‟s law. By increasing or decreasing the spring constant we can alter the movement of
the proof mass in the corresponding direction
CAPACITANCE ACCELEROMETER
One of the most commonly used MEMS accelerometer is the capacitive type. The capacitive
MEMS accelerometer is famous for its high sensitivity and its accuracy at high
temperatures.
The device does not change values depending on the base materials used and depends only
on the capacitive value that occurs due to the change in distance between the plates.
If two plates are kept parallel to each other and are separated by a distance„d‟, and if „E‟ is
the permitivity of the separating material, then capacitance produced can be written as;
EA = E0EA
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High sensitivity.
Easy readout circuitry.
Independent of temperature variation.
Easy fabrication (two level mask).
Large noise margin.
Fabrication on silicon.
Compatible with CMOS technology.
Automotive
o Crash detection & Air bag deployment.
Consumer Electronics
o hard disk protection(laptops)
o screen rotation (mobile)
o Image stabilization (camera)
Industrial
o Vibration detection (machine)
o crack detection (pulley)
Aerospace & Defence
o Navigation
o Missile guidance
o Thrust detection
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Working Principle
All MEMS gyroscopes with vibrating element are based on the transfer of energy between
two vibration modes caused by the acceleration of Coriolis.
Corioli’s effect – an effect where by a mass moving in a rotating system experiences a force
(Corioli‟s force) acting perpendicular to the direction of motion and to the axis of rotation.
Silicon wafer is taken with implanted etch to stop on the bottom surface. Processing takes
place only on the top surface of the wafer. Anisotropic KOH etching is taken place on the
wafer surface and sacrificial layer is added on to it. An oxide layer is added on top. Through
etching process, the sacrificial layer is etched out.
Sputter thin aluminium layer, pattern with PR mask. Then etch away aluminium from the
substrate to create leads.
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Use sol – gel method to add 2 micron layer of PZT and use another mask PR and etchant to
create piezo electric sheet. Sputter more aluminium leads and pattern with a third mask,
photoresist and etchant.
DC source creates an electrostatic force that moves the disc. Proper control of these
electrodes can put the system into resonance. Similarly, the sensing electrodes change to
gauge system change.
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Improved sensitivity
Improved accuracy and reliability
Easier to alter the parts of device as compared to its macro counter part
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