Final Report Draft
Final Report Draft
SCHOOL OF ENGINEERING
DEPARTMENT OF CHEMICAL AND PROCESS
Alvine Ayieta
CPE/2569/21
CHP390
This attachment report has been submitted for examination with my approval as the Industrial
Supervisor.
i
DEDICATION
I dedicate this attachment report to God Almighty my creator, my strong pillar, my source of
inspiration, wisdom, knowledge and understanding. He has been the source of my strength
throughout the session and on His wings only have I soared. I also dedicate this work to my
parents and the supervisor Mr. Boniface who has been a mentor all through.
ii
ACKNOWLEDGEMENTS
I would like to extend my sincere gratitude to everyone who supported my twelve-week
industrial attachment at Sony Sugar in the Processing Department. My deepest thanks go to
the management of Sony Sugar for this valuable opportunity and to my supervisor, Mr
Bonface, for their guidance and expertise, which greatly enhanced my practical learning
experience.
I am grateful to the technical and support staff at Sony Sugar for their cooperation,
knowledge-sharing, and warm welcome. Additionally, I thank my lecturers and the
administration at Moi University for facilitating this program, and my family and friends for
their constant encouragement throughout this period.
iii
ABSTRACT
This report documents my completion of a twelve-week industrial attachment at Sony Sugar
Company Limited within the Processing Department, a requirement of my Chemical Engineering
degree program. The attachment provided a foundation for practical skills development and
professional growth. Through interactions with staff across various levels, from subordinates to
senior management, I gained valuable insights into industrial operations, workplace dynamics, and
potential career pathways.
The report outlines the role of field attachments in bridging academic learning with industrial
experience for engineering students, emphasizing the alignment of theoretical knowledge with real-
world applications. It provides an overview of Sony Sugar’s organizational structure and highlights
the knowledge, technical skills, and hands-on experience I acquired during this period. Key areas
discussed include the company’s sugar processing workflow, quality control, and production analysis
techniques that support high-quality output, in line with the company’s mission.
My activities involved machine operation, sampling, analysis, and direct participation in all stages of
sugar processing, covering processes from cane inspection and milling to juice treatment and final
sugar crystallization. Additionally, the report addresses energy generation via cane by-products and
outlines environmental pollution control practices, which reflect the company’s commitment to
sustainable operations. The report concludes with an examination of raw water treatment methods
used to supply safe water for both human consumption and boiler feed, and it acknowledges those
who contributed to a successful attachment experience.
iv
Contents
DECLARATION....................................................................................................................................i
DEDICATION......................................................................................................................................ii
ACKNOWLEDGEMENTS....................................................................................................................iii
ABSTRACT.........................................................................................................................................iv
CHAPTER ONE...................................................................................................................................1
1.0 INTRODUCTION...........................................................................................................................1
1.1 ORGANIZATIONAL STRUCTURE...................................................................................................4
CHAPTER TWO..................................................................................................................................5
2.0 SUGAR PROCESSING FLOW DIAGRAM........................................................................................5
2.1 CANE INSPECTION AND WEIGHMENT........................................................................................7
2.1.1 Cane Inspection........................................................................................................................7
2.1.2 Weighment..............................................................................................................................8
2.2.1 Pre- milling.............................................................................................................................10
2.2.1.1 Cane yard............................................................................................................................10
2.2.1.2 Chopper...............................................................................................................................11
2.2.1.3 Heavy Duty Cutter...............................................................................................................11
2.2.1.4 Shredder..............................................................................................................................11
Activity at the shredder.............................................................................................................11
2.2.2 Milling Section.......................................................................................................................12
2.2.2.1 Hydraulic pressure system..................................................................................................12
2.2.2.2 Cooling and Lubrication System.........................................................................................13
2.2.2.3 Mill 1...................................................................................................................................13
2.2.2.4 Mill 2...................................................................................................................................14
2.2.2.5 Rotary screen......................................................................................................................14
2.2.2.6 Sand catcher tank...............................................................................................................14
2.2.2.7 Mill 3...................................................................................................................................14
2.2.2.8 Mill 4...................................................................................................................................14
2.3 BOILER.......................................................................................................................................16
2.3.1 Furnace...................................................................................................................................16
2.3.2 Air System..............................................................................................................................16
2.3.2.1 ID fan...................................................................................................................................17
2.3.2.2 Forced Draft (FD) fan...........................................................................................................17
2.3.2.3 SA fan..................................................................................................................................17
2.3.3 Fuel System............................................................................................................................17
2.3.3.1 Flue flow..............................................................................................................................18
2.3.3.2 Flue gas flow.......................................................................................................................19
2.3.4 Water System.........................................................................................................................20
2.3.4.1 Water System Flow Diagram..............................................................................................20
2.3.4.2 Feed drum...........................................................................................................................20
2.3.4.3 Economizer..........................................................................................................................21
2.3.4.4 Steam drum.........................................................................................................................21
2.3.4.5 Mud drum...........................................................................................................................21
2.3.5 Boiler Stoppage Process.........................................................................................................21
2.3.6 Boiler Maintenance................................................................................................................21
2.3.6.1 Mud drum maintenance.....................................................................................................21
2.3.6.2 Steam drum.........................................................................................................................22
2.3.7 Boiler Start Up........................................................................................................................22
2.3.8 Boiler Box Up.........................................................................................................................22
2.4.0 WATER TREATMENT PLANT...................................................................................................23
2.4.1 Water treatment flow chat....................................................................................................23
2.4.1.0 Cascade aerator..................................................................................................................23
2.4.1.1 Clarifier................................................................................................................................23
2.4.1.2 Clarified water tank (CWT).................................................................................................24
2.4.1.3 Multi Grade Filter (MGF) unit.............................................................................................24
2.4.1.4 Activated Carbon Filter (ACF).............................................................................................24
2.4.2 DEMINERALIZATION..............................................................................................................24
2.4.2.1 Strong Acid Cat ion (SAC) unit............................................................................................24
2.4.2.2 Degasser tank......................................................................................................................24
2.4.2.3 Strong Base Anion (SBA I) unit............................................................................................25
2.4.2.4 Strong Base Anionic (SBA II) unit........................................................................................25
2.4.2.5 Mixed Bed...........................................................................................................................25
2.4.3 Regeneration and Recharging................................................................................................25
2.4.4 Backwashing..........................................................................................................................26
2.4.5 Water analysis........................................................................................................................26
2.5 EFFLUENT TREATMENT PLANT..................................................................................................29
2.5.1 Effluent Treatment Flow Chart..............................................................................................29
2.5.2 Screen Chamber.....................................................................................................................30
2.5.3 Oil Schemer............................................................................................................................30
2.5.5 Equalization Tank...................................................................................................................30
2.5.6 Primary Aeration and Clarification........................................................................................30
2.6 LEACHET WASTE WATER TREATMENT PLANT..........................................................................33
2.6.1 LTP Flow Diagram...................................................................................................................33
2.6.2 Convectional Aerator Tank (CAT) Chamber...........................................................................34
2.6.3 Flash Mixer.............................................................................................................................34
2.6.4 Equalization Tank...................................................................................................................34
2.6.5 Primary Clarifier.....................................................................................................................34
2.6.6 Heat Exchanger......................................................................................................................34
2.6.7 Buffer tank.............................................................................................................................34
2.6.8 Anaerobic Blanket Sludge Reactor Tank (UNBSR).................................................................34
2.6.9 Convectional Aeration Tank (CAT).........................................................................................35
2.6.10 Secondary Clarifier...............................................................................................................35
2.6.11 Moving Bed Bio Reactor......................................................................................................35
2.6.12 Chlorine Contact Tank..........................................................................................................35
2.6.13 Accelerated Gravity Separator (AGS)..................................................................................35
2.6.14 Activated Carbon Filters.......................................................................................................35
2.6.15 Multi Grade Filters...............................................................................................................35
2.6.16 Treated Water Tank.............................................................................................................35
2.6.2 Sludge Disposal......................................................................................................................35
2.6.2.1 Mud Sump...........................................................................................................................35
2.6.2.2 Continuous Centrifugal Machine........................................................................................35
2.7 PROCESS HOUSE........................................................................................................................37
2.7.1 Process Control Room............................................................................................................37
2.7.2 Juice Treatment.....................................................................................................................37
2.7.2.0 Juice Treatment Flow Diagram...........................................................................................38
2.7.2.1 Weighment Tank.................................................................................................................39
2.7.2.2 Heaters................................................................................................................................39
2.7.2.2.1 Raw Juice Heaters............................................................................................................39
2.7.2.2.2 Secondary Juice Heaters..................................................................................................39
2.7.2.2.3Tertiary Heaters................................................................................................................39
2.7.2.3 Liming Tank.........................................................................................................................40
2.7.2.4 Limed Juice Tank.................................................................................................................40
2.7.2.5 Flash Tank...........................................................................................................................40
2.7.2.6 Clarifier................................................................................................................................41
Juice clarification at clarifier........................................................................................................41
2.7.2.7 Evaporators.........................................................................................................................42
Evaporators diagram dome.......................................................................................................42
2.7.3 Juice Recovery........................................................................................................................45
2.7.3.1 Rotary Vacuum Filter (RVF)................................................................................................45
2.7.4 SUGAR HOUSE........................................................................................................................47
2.7.4.0 Sugar House Flow Diagram.................................................................................................47
.........................................................................................................................................
.............................................................................................................................................................47
2.7.4.1 PANS....................................................................................................................................48
2.7.4.1.1 A- Pan Boiling...................................................................................................................50
2.7.4.1.2 B-pan boiling....................................................................................................................51
2.7.4.1.3 C-Boiling...........................................................................................................................52
2.7.4.2 Operations in Pans..............................................................................................................52
2.7.4.2.1 Wash Out.........................................................................................................................52
2.7.4.2.2 Striking.............................................................................................................................52
2.7.4.2 CRYSTALLIZERS....................................................................................................................53
2.7.4.3 CENTRIFUGAL......................................................................................................................53
2.7.4.3.1Batch Centrifugal..............................................................................................................54
2.7.4.3.2 Continuous Centrifugal....................................................................................................55
2.7.4.4.1 Grass hooper....................................................................................................................56
27.4.4.2 Rotary Sugar Dryer (FBD)..................................................................................................56
2.7.4.5 GRADER...............................................................................................................................56
2.8 PROCESS LABORATORY.............................................................................................................58
2.8.1 Sugar moisture test................................................................................................................58
2.8.2 Sugar colour test....................................................................................................................58
2.8.3 pH determination...................................................................................................................58
2.8.4 Determination of water insoluble matter in sugar................................................................59
2.8.5 Determination of moisture in bagasse..................................................................................59
2.8.6 Determination of sugar trace................................................................................................60
2.8.7 Determination of sugar ash...................................................................................................60
2.8.8 Determination of brix............................................................................................................60
2.8.9 Determination of pol/sucrose content..................................................................................61
2.8.10 Laboratory terminologies....................................................................................................61
2.8.11 Procedure for slurry preparation.........................................................................................62
CHAPTER THREE..............................................................................................................................63
3.1 CHALLENGES..............................................................................................................................63
3.2 RECOMMENDATIONS...............................................................................................................63
3.3 CONCLUSION.............................................................................................................................63
3.4 REFERENCE................................................................................................................................64
CHAPTER ONE
1.0 INTRODUCTION
Sony sugar Company was established in 1976 under the companies Act Cap 486 of the
laws of Kenya and commissioned in 1979. The company premise and sugarcane nucleus
estate sit on an area covering 2492 hectares without-growers cane area of 15500 hectares.
The company serves over 25,000 cane farmers in ten districts within the cane growing zone
at Homabay, Gucha, Trans Mara, Kuria Migori, Uriri, Rongo, Kisii south Ndhiwa and
through sugar production whose current capacity stands at 2500 TCD. Government is the
main stakeholder of the company owing 98.8%, centum investment co. (ICDC) 0.717%,
industrial development bank (IDB) 0.28% and Mehta group 0.21%.The company is
agriculture manager, human resource manager ,finance manager and marketing manager.
Vision
Mission
Core values
Customer first
Integrity
Sustainability
Professionalism
Entrepreneurship
Safety
1
Timeliness
Sony is committed to provide a work environment devoid at risk to health and safety of its
employees, contractor, visitors and other personnel within its premises in all aspects of our
Ensuring compliance with all applicable loss, regulation and any other statutory
Identify and prevent any potential risk to health and safety at the workplace and
Create awareness on individual obligation to all persons working under the control
place engineering control to prevent injury and ill health at the place of work.
Ensure that health and safety rules and procedures are in place implemented and
Establish mechanism for investigation and follow up all health and safety incidents
to avoid recurrence.
Periodically reviews the occupation health and safety policy to ensure that it
The audits carried out include: environmental audit, safety and health audit, noise level.
thermal, air quality, waste water, hazardous substance, fire safety, risk assessment, plant
inspection, and medical examination among others. The environmental, health and safety
aspects identified forms the basis for the development of environmental health and safety
2
management plan for implementation and continual review. It also forms part of the
To this end the company has successfully implemented and reserved substantial number of
aspects and significant impacts as identified in the audits. These include; establishment of
oxidation ponds to improve on waste water quality, safe handling of used oil, reduction in
accidents and incidents, procurement of new and modern fire engine, creating awareness
on environment health and safety, adequate ablution blocs and provision of wholesome
water.
v. Enough capital
3
ORGANIZATIONAL STRUCTURE
Managing
director
Board of
General Manager
directors
Agriculture Cane
service manager development
manager
4
CHAPTER TWO
Milk of lime
preparation
If Ok sent to weigh Bridge Juice liming tank 10 Bx.
PH 7.20 +/- 0.3
Evaporation (Raw syrup)
Filtrate Juice
5
Brown
Sugar Boiling
Treated B A Light A H- C- BH - Seed
syrup Magma molasses molasses Magma molasses slurry
A B C
Crystallizer
Crystallizer Crystallizer
A AL
Centrifuge B BH C
AH Centrifuge Centrifuge
A - Sugar
B- Sugar / C- Sugar /
magma magma
Final
molasses
Hopper – grader - Bin
Store
6
2.1 CANE INSPECTION AND WEIGHMENT
Here the canes are received, inspected of their quality, weighed then the farmers’ slips
verified for payment processing as well as transporters payment as it depends on the number
of tonnes received. The slips are recorded on a slip delivery record sheet for future reference
purposes. A summary is done on a daily basis on the ages of the canes according to the
farmer’s slip and the assessed age by the analyst, the crop rotation as either ratoon or first
planting, ratoons have high sucrose content than first plants, the level of trash on the canes
and the tonnes for every age blanket.
2.1.1 Cane Inspection
Inspection is done mainly to determine the quality of cane received at the company. This is
done by checking on;
Levels of trash, tops, mud and roots on the canes – the weight of extraneous matters
should be below 8%.
The age of cane is calculated to estimate the age of the cane since they sometimes
vary with the slip age.
Cane varieties- specific varieties are recommended by the department of agriculture to
farms. These are canes with high sucrose content and other species that take short
time to mature. Hybrid canes take even 14 months to mature.
They include;
Co 421
Co 420
Co 945
EAK
D8484
A random sampling is done for the canes in the tractor, from them an average of their ages
recorded. After verification, canes proceed to weighment.
To calculate the age of sugarcane, formula used was;
( X + 6)2
3
Where;
X is the total number of internodes present
6 represent three internodes assumed to be present at the top and bottom (left on the ground
after cutting the sugarcane).
2/3 means it takes one and half months for an internode to grow.
For example, if sugarcane brought has a total of 30 internodes;
7
(30+6)2
3
=36×2/3
=24 months
The recommended age of canes is 18 months because at this time they have high levels of
sucrose.
Canes are received from different stations. Tractor canes are from local farms whereas trucks
transport canes from out stations, which includes, Makuti Misikhu, Busia, Chemilil, Miwani,
Kericho and Naitiri.
Sampling is done for all the station, where six canes are taken from every station in a day.
Composite sampling; a sample is obtained at different points of the same source about three
or four times or any other specific time. Spot/systematic sampling; sample is taken once from
the source. A full unbroken cane is picked from every compartment of a truck. They are
labeled then taken to the laboratory for analysis.
Quality of canes
Fresh- transported same day of harvesting
Burnt canes- burning was done before harvesting. They affect boiling as they stick on
the walls of the boiling surfaces
Stale canes- have stayed for more than one day before being delivered to the
company. They have low contents of sucrose since inversion (conversion of sucrose
to reducing sugars) has taken place.
pol
Purity= × 100 %
brix
8
Importance of Weigh Bridge in SONY SUGAR CO LTD
Weighbridge truck scales accomplish one main task: They allow truck owners to sell
or charge by weight over the bridge and they effectively help prevent heavy fines or
axle overloading by checking on the weight of both axles and taking the gross vehicle
weight. The load is measured by weighing the vehicle when it is first empty and then
loaded, and taking the difference.
To preserve record for all products and materials entering and exiting the company.
Aid in farmer’s payment
Aid in payment of drivers and loaders (for tractors)
9
2.2 MILLING SECTION
WESKOL is in possession of two mills. The old FS mill which was acquired from Mumias
Sugar Company in 2007 (mills 180- 200 tonnes of canes per hour) and a new mill which is
capable of milling 300 tonnes in an hour. The old mill is only used if the new mill has a break
down or during maintenance. Both of them cannot work simultaneously due to lack of
enough volume in the process house, wince it can currently accommodate 300 tonnes of raw
juice per house.
2.2.1 Pre- milling
This process involves; offloading of canes from tractors and trucks, conveying and cane
preparation before milling.
10
Materials in the mills are transferred to the next stage by the use of conveyers. The conveyers
are interlock in that when a specific point breakdown, the other parts behind stop instantly but
the front sections continuous. The conveyer is connected all through with an emergency line
which when pressed stops the whole process. It is only applicable in case of a danger or an
occurrence of an accident. All the conveyers are monitored at the console room. They
include; cane carrier, rake conveyer, belt conveyer, intercarrier and bagasse carrier.
Fibre preparation
The cane is prepared by cutting it into small pieces this increases surface area for juice
extraction by exposing juice out of cane.
2.2.1.2 Chopper
This is a leveller device. It has first moving knives suspended on the upper part of the cane
carrier. It cuts through the top regions of the conveyed canes to level them so that the HD
does not become chocked. The knives are attached to a motor on a coupling and a gear box.
Lubrication is done on the gear box to prevent wear and tear. The knives are frequently check
and changed in case of any brokage.
2.2.1.3 Heavy Duty Cutter
This is a device with incorporated knives. They cut through the cane carrier. This ensures that
all the cane passing through its cut into small segments. The heavy knives are arranged in
such a way that, there are moving and stationary knives. This ensures maximum breakage of
large cane sizes. It is also connected to a motor and a gear box on a coupling. It has fan that
cools the motor to avoid overheating.
2.2.1.4 Shredder
Activity at the shredder
On arrival of the cane fibre at the shredder, the cane fibre is crushed into very fine cane
fibres. The shredder revolves at 1000 rpm. It has about 200 hammers and eight shafts on to
which hammers of 8-10 kgs each are mounted. Its chute has two connected feeder rollers that
oscillates in opposite direction as a result they regulate and align the entering canes to enter
the shredder in a blanket- like form. It also has stationary anvils connected after every line of
hammers. Upon sticking against the hammers, they leave a gap of 75mm thus break canes
into fine fibres. This exposes the juice cells in fibres. The juice cells are the one that stores
juice. The fine cane fibres are generated at very high rate; hence they are carried away by the
rake conveyor into a rubber conveyor belt which leads to the mills.
They shredder has a lubricating oil pump which ensures continuous lubrication and cooling
effects on the gear box. The oil levels are frequently checked and the oil changed upon
exhaustion. It has air conditioner fan which cools the motor throughout when running. The
procedure of starting remains putting oil pump on then the fan before running the shredder.
After which it is allowed to running for 10 minutes before milling begins. At this point its
conditions are checked. Also, for every stoppage, it is inspected of its condition in case of
broken hammers they are changed. Vibrations are detected when hammers break. Then
calibrated depending on the extend of vibrating to know the level of breakage as they cause
weight imbalance that brings about vibrations.
11
Along way, there is a kicker that regulates the amount of fibre passing the magnet (traps any
magnetic material and drops it down after some time) on a conveyer. The fibre is now ready
for milling.
Preparation Index (PI)
This is a percentage taken as the ration of the prepared sample. Example, a sample
of 5 kg is taken, its pol analyzed for 2kg and the other 3kg is further processed and
its pol also taken.
PI = pol for 2 kg: 3 kg
Sugar – 18%
Non-sugars and salts – 22%
Water – 60%
12
The pump creates pressure by pumping oil to the accumulators. The funnel regulates the
accumulators which are connected to tubing to the top cups. When the top roller is at the
bottom, the accumulators supply oil to top cups. This intern compels the top piston connected
to the roller to move upward. As the top piston reaches its highest point, oils is withdrawn
continuously to the accumulators. This causes downward motion of the top roller. This action
is simultaneous for all pressure top cups as they are all connected to same pressure by help of
equalizers. Repeatedly, this enhances up and downward movement of top roller thus
squeezing juice out of the fibres.
The hydraulic oil is added daily to the pump tank.
2.2.2.2 Cooling and Lubrication System
Every mill has its own lubrication pump, which supplies oil to the gear box of the rollers and
motors to avoid wear and tear. The oil is replaced when it is exhausted.
The fibre is lubricated from one mill to another by use of imbibition juice or imbibition
water. This helps avoid rollers choking effects.
Cold water is continuously pass-through gear box systems of rollers, as a result causing
cooling effect. The water is collected by a common header into a cooling tower then pumped
back to the cooling lines. In case of detectable overheating of cooling water, oil is manually
pumped to the roller’s gears by the help of tubes connected directly.
2.2.2.3 Mill 1
It constitutes of three pressure feeder and four rollers.
Pressure feeders
Top
Bottom
Drum
The top and bottom feeders are connected to a motor and drives the drum (conveys cane
fibres to feed roller).
Rollers
Feed roller- receives fibre from pressure feeders and is in possession of trash
blade for scrapping off fibers from the rollers.
Top roller- it is connected to a motor. It drives the other three rollers in
varying direction depending on their position as well as extracts juice from
fibres and pushes the fiber to discharge roller.
Discharge roller- conveys the bagasse to the intercarrier for second milling.
Underfeed roller- receives fiber from bottom side and conveys it to the top
roller.
The rollers are corrugated to prevent the sugar fibres from sticking onto their
surface.
13
Top roller motion of sugar fibres
Feeder roller
The juice from mill 3 lubricate bagasse from mill 1 before proceeding to mill 2. The juice
from mill one is collected by a collector plate and stored in a small tank in possession of a
pump which pumps the juice to rotary screen.
2.2.2.4 Mill 2
It has four rollers. Its bagasse is lubricated by imbibition juice from mill four. Harvested juice
from mill 2 is pumped to the rotary screen.
14
to the atmosphere. They are used for binding the mud together in rotary vacuum filter. They
are therefore collected and conveyed by pipes to bagacillo feeders in process house.
15
2.3 BOILER
This is the section where steam is generated from boiler water to run the turbine (Mechanical
energy) to produce electrical energy as well as used in heating purposes. WESKOL has two
boilers put in place which run simultaneously.
NHEC boiler- Produces 100 tons of steam in an hour and 12-megawatt power
production to run machines and supply electrical power demand.
ISGEC- produces up to 80 tons of steam and at most 9-megawatt power.
The steam generated should have a pressure of 42-45kg/cm2 and at 400-450 0C.
2.3.1 Furnace
It is hollow from bottom to the top and works under negative pressure. This ensures water
vapour is not formed and steam is generated at elevated temperatures.
There are two types of furnace, Spreader stopper (It has stationary fire bar grates which are
connected to a man handle which are adjusted after sometime to release the ash to hoopers
which have rotary ash machines that combines the ash with cold water) and travelling
furnace- this type of a furnace is in ISGEC boiler. The grates oscillate slowly into a hopper
line where the ash is damped and carried to a water mixing head. This prevents dust from
escaping to the atmosphere and are also a source of manure. The furnace has a temperature
of about 700- 900 0C. On its walls are vertical connected tubes coming from a common a
horizontal common header from the mud drum and also downcomers carrying water from
steam drum to the mud drum. The risers are thin numerous tubes connected from the bottom
of the furnace to the steam drum. As the water moves downwardly and upwardly, they get
heated and turns into steam which is harvested in the steam drum. The steam is conveyed
through risers to the primary superheaters which are coiled tubes at the top most of the
furnace. The PSH are heated by the flue gases to elevated temperatures. They heat the steam
to 350 0C. The steam at high pressure escapes to Secondary Superheaters (SSH). The steam is
further heated on the tubes to a temperature above 400 0C. both SSH and PSH are connected
to attemperator that cools he coils in case of over heats to avoid melting of the tubes.
2.3.2 Air System
Flow diagram
Mill 4 bagasse
Conveyer belts
TO NHEC FURNACE
18
2.3.3.2 Flue gas flow
Hot gases move up the furnace to the preheaters where they heat steam and elevate Air
temperature. Due to the draft in the furnace, they are trapped towards the economizer. Here
they travel outside water tubes as a result heat exchange takes place. They flow to the APH
system preheating the atmospheric air in. The gases pass the Main Dust Controller (MDC).
The particles within the flue gases are charged by ionised environment in their way through
the MD. The charged particles are trapped by positively charged plates which after
accumulation, they are scrapped off then cooled using cooled water and transported to farms
as manure. Throughout, the temperature of the flue gases goes decreasing to 150 0C as it exits
the chimney.
Flue gases to
Economizer and Bagasse
air heaters feeder
Downcomers
Mud drum
Common header
Grate
19
2.3.4 Water System
The water used in the boiler is supplied from river Isikhu to the DM (Demineralisation)
plant in order to achieve the boiler water parameters. i.e.
Ph- 9-10
Hardness- nil
Sugar trace- nil
TDS- <400
Dissolved salts- nil
The water is the pumped to DM tanks which supply the water to surface tank. Here the DM
water is heated by condensate from evaporator body one to a temperature above 90 0C. This
tank supplies its water to feed tank for ISGEC and NHEC boiler.
DRTR
Storage Economizer Steam Drum downcomer
Tank Feed tank
s
(Demineraliz
ed water)
20
2.3.4.4 Steam drum
The water from economizer second chamber proceeds to the steam drum. It is divided into
two, a steam chamber and water chamber. It has a gauge glass that shows the level of water to
steam. It should not exceed 50 percent and the boiler should not start if its below 30%. The
water is conveyed to the mud drum through downcomers. While steam passes through a
separator (to separate water from steam) to the primary super heaters the steam is further
heated to 350 0C. It is further conveyed to a secondary superheater that rises the temperature
to 450 0C. The steam escapes through a main stock valve to the steam line and heads to
turbines at 45 bars.
2.3.4.5 Mud drum
It is at the bottom of the furnace and connects tubes to the furnace through a common header
line. The vertical tubes (risers) carry away wet steam to the steam drum. It is connected to a
high dosing pump which adds sodium thiosulphate to the water. This aids in coagulation of
total suspended and dissolved solids, which are blown out through the mud drum blower line.
21
2.3.7 Boiler Start Up
Open water supply valve to feed tank up to 85%water. Make sure the steam drum is at
least 30% water.
Put logs and small bagasse then lit a fire inside.
Put ID fan at low RPM.
NOTE: if you are not going to use the boiler for some time, consider opening the air vent and
filling the boiler (again dosing with sodium sulphide) until water issues from the vent, then
dose it. This will cover all the internal surfaces with treated water to avoid corrosion. The
water drum steam coil should be left on (the pressure will not rise over much, but keep an eye
on it to avoid an unplanned hydraulic pressure test). Before use, blow the boiler down to just
show in the glass before firing.
22
2.4.1 Water treatment flow chat
Cascade clarifier
Power tank
aerator
Flash mixer
Clear water
Domestic
ACF MGF tank
water SAC
degasse
r
NAOH HCL Morpholine
MBF DM H2O
SBA1 SBA2
2.4.2 DEMINERALIZATION
This involves removal of all sort of minerals present in water i.e., all the cations, anions and
foreign gases present in water.
2.4.2.1 Strong Acid Cat ion (SAC) unit
It receives water from ACF. All cations present in water are removed here. Therefore,
cationic resins are used here, always of the sulphuric group. Equation of the reaction taking
place is attached. Resins react with the salts in water to remove the cations and forming weak
acids such as carbonic acid. This is when in service. During regeneration of resins in the
SAC, Hydrochloric Acid is used to regain the resins in their service state. Further explained
in the reaction equation. The water from here as a pH of 3.5.
2.4.2.2 Degasser tank.
Water from the SAC has weak acids such as carbonic acid. This gas is unstable hence it can
dissociate further in presence of air. Therefore, a blower is connected from the side and water
dropping from the topmost of the tank. This allows for counter current reaction to take place.
It leads to formation of carbon dioxide, for instance, when carbonic acid dissociates. CO2
together with other gases such as hydrogen sulphide and carbon monoxide are expelled out
from the tank through an outlet. There are pumps connected to this tank that facilitate
pumping of air. The water from the Degasser tank is then pumped to SBAI for removal of
anions from water.
2.4.2.3 Strong Base Anion (SBA I) unit
Consists of anionic resins that remove strong anions from water. The resins used here are
carboxylic group (R–OH). The hydroxide ion present in resins is replaced by an anion.
Consider for instance, a strong acid, sulphuric present in water. When in service, the
hydroxide ion will be replaced by the sulphate ions. During regeneration, caustic solution
(sodium hydroxide) is used both in SBA I and SBA II. For SBA I, sodium hydroxide reacts
with the loaded resins renewing them. Below are the reactions taking place at the SBA i.
24
(a)R-OH +H2SO4 R-SO4²- +H2O
2.4.4 Backwashing
Important valves used in backwashing are:
Air inlet valve
Air vent valve
Backwash inlet valve
Backwash outlet valve.
Backwashing in MGF helps to expel all the suspended solids. In SAC, WBA, SBA and MB
backwashing aids in separation of resins.
2.4.5 Water analysis
At every step of water treatment, a sample is taken for laboratory analysis. Which includes;
Old and new boiler water
SK condensate water
Super saturated steam
Feed water
Saturated steam
ACF H2O
SAC H2O
Degasser water
SBA water
Mixed bed water
DM water.
pH of water
Conductivity
Total dissolved substances (TDS)
Total suspended solids TSS (880nm)
Phosphates (phosver 4)
Silica: Low Range and High Range
Nitrates
P– alkalinity (phenolphthalein)
26
T–alkalinity (total) methyl
Total hardness (TH)
Sulphates
Iron– furrower hatch
Copper – curve.
Procedure for silica test for Low Range
•Into 2 empty cuvettes, measure 10ml of the sample.
•Add 14drops of Molybdate 3 Reagent to each sample.
•Swirl to mix and start the timer- A 4 minute’s reaction will begin.
•Add citric reagent and swirl to mix, A 1min reaction will begin.
-the destruction of possible phosphate interference occurs.
•Add contents of one amino acid F reagent to one sample, swirl to mix
•Blank preparation
-the sample without amino reagent is the blank
•Start the timer
A two minutes reaction will begin. Blue color will develop if silica is present
•Wipe the blank and insert it into cell holder in spectrophotometer. This will enhance Zero
the machine, it will display 0.000mg/LSio2
•Wipe the prepared sample and insert and read the results in mg/LSio2
Procedure for silica test in water (High Range)
•Reagents: citric acid, Acid (RGT) and Molybdate
•Take two cuvettes, one for standard (A) and for Blank (B)
•To cuvette (A), measure 10ml of the sample also 10ml to (B)
•To (A) add molybdate
•Add Acid RGT to (A) and set spectrophotometer and wait for 10mins
•Immediately the spectrophotometer alarms you that the set time 10mins set earlier have
elapsed add citric acid and wait for 2mins
•There after zero the spectrometer by use of a blank sample
•Place the standard sample, the resulting reading reflects silica content in the tested water.
Principle Of spectrophotometer performance, light absorbance and penetration
NOTE: high range silica test is done for boiler water only.
27
: low range silica test is done for the other samples.
: sugar trace is done for SK water only.
: analysis is done after every three hours.
28
2.5.1 Effluent Treatment Flow Chart
screen
shock load
chamber oil skimmer
raw effluent
(1) lime,urea,
DAP,
Phosphoric
addition
from process,
boiler and mills
equalization screen
tank chamber (2)
treated water
to River/ wetlands pond
stream
29
There are also organic load present in raw effluent. Sugar in raw effluent also constitutes the
organic load. The lower the pH. The higher the organic load the higher the Chemical Oxygen
Demand, COD hence the higher the Biological Oxygen Demand, BOD. This makes the
effluent water acidic.
2.5.2 Screen Chamber.
The raw effluent first flows through the screen chamber. This is the initial stage of effluent
treatment. Here large insoluble substances in water are by means of a screener.
2.5.3 Oil Schemer
The screened water flows through the oil chamber. It has an oil schemer/separator which
removes oil from water. When the COD of the screened water is found to be high or its
temperature high, it is channelled to the shock loading pond.
2.5.4 Shock Load
This is a large tank that holds the screened effluent water. In case the organic load is high, the
water is not allowed to proceed to equity tank. It is first stored in shock tank for dilution to
lower its COD.
2.5.5 Equalization Tank
The screened water with the low or normal COD is directly allowed to flow into the
Equalization Tank [EQT]. After the shock loading tank, there is dosing of lime to the effluent
water before it drains into the Equity Tank. This chemical raises the pH of the water to
neutral. The pH of water is maintained at neutral since it is conducive for sludge formation.
Urea and DAP is fed into the water entering the equity tank through a drainage line. The
fertilizers provide food for aerobic microorganism for growth and reproduction. This effluent
is then pumped to the DSM tank; where it is screened to eliminate some fine insoluble
particles. The screened effluent then flows into the tube settler through a base inlet. Here the
mud and insoluble particles settles at the bottom while water raises through over flowing
from the top. The organic load is also reduced here. Therefore, as water gets into aeration
points, it is less of insoluble particles.
2.5.6 Primary Aeration and Clarification.
There are two consecutive aeration ponds, the first and second primary aeration ponds. There
are acetogenic and methanogenic bacteria, at these ponds which feed on the organic matter
such as sugar in water. The feeding action is simply aerobic which require oxygen. Therefore,
there are two motors at each aeration pond which expose water which expose water into air
for maintained oxygen supply. Dosing of dissolved DAP increases the phosphates while
urea/CAN increase nitrate in water. These two chemicals are economical for the growth of
bacteria and activate their functioning. The breakdown of the organic components leads to
formation of sludge thus making the water browner in colour.
The role of bacteria at the second aeration pond is less compared to the first aeration pond.
This is because more organic compounds have been fed by the bacteria at the first aeration
pond. By taking a sample of water at these ponds, when the sludge is present and settles fast,
simply shows the bacteria present. Thus, the lower the sludge content the lower the bacteria
load and vice versa. Sludge range is usually 600. It should not exceed this value. If it does,
30
desludging action is taken This biological action makes the effluent at the primary aeration
ponds to ferment and produce bad odour.
Characteristics of water with sludge are; Very brown in color and settles fast.
The effluent, now less of organic matter drains into the primary clarifier. Sludge is separated
from water. The sludge being denser than water settles at the bottom of the clarifier as clear
water overflow at the top and channelled into the secondary aeration ponds.
2.5.7 Secondary Aeration and Clarification.
Secondary aeration ponds constitute of 3 consecutive ponds; 3 up to 5. Each pond has two
motors and their operation is just similar to the working principle of the primary aeration
ponds. At these ponds there is less bacterial action compared to the first two aeration ponds.
The role of bacteria reduces from pond 1 to 5. This is simply due to decrease in organic load
in water which has been eliminated in the previous aeration ponds.
This effluent water from secondary aeration pond 5 drains to the secondary clarifier. It can
either pour to secondary clarifier A or both A and B depending on water capacity. These
clarifiers enable settling of sludge at the bottom and clear water floating at the top. The
sludge of the secondary clarifiers may be discharged at either primary or secondary aeration
ponds. The partially clear water from the clarifier flows into the chlorination chamber.
Addition of chlorine [sodium hypo chloride] in this water helps to bleach, sterilize and
remove odour in water. It is then pumped into two multi grade filter [MGF] unit tanks. Here
it is filtered to remove dusts and some impurities in water. MGFs have sectional media of 5
different sizes that performed filtration.
The filtered water is released to the pond water treated tank. This holds the treated water
before it gets into the wetlands. The plant simply has a constructed wetland made of a series
of 6 ponds. There is meandering of the channels leading into the pons from one to another.
The meandering allows aeration and removal of bad odour. The ponds have some plant
species and fish to absorb nutrients, mud/dust and colours. They are shallow to allow sunlight
penetration for photosynthesis of the plant species. The final water from the sixth pond is the
treated effluent which is released to the river. It is free from toxic substances, nutrients and
other harmful substances. Therefore, it is safe with no adverse effects with river water.
31
N/B
There are two types of wetlands
(a)Constructed wetland
(b) Natural wetland
32
2.6 LEACHET WASTE WATER TREATMENT PLANT
This plant deals with leached acidic water from packed bagasse. When it rains, a lot of water
seeps from the bagasse. It is collected into a dam through gravity. It is then pump to LTP
plant for treatment. The treatment here is mostly pH boosting.
CAT screening
chamber
Heat exchanger
CAT tank
UNBSRT Secondary clarifier MBBR
CCT AGS
ACF MGF
TREATED WATER
33
ETP SECONDARY TANK
AERATOR TANKS
2.6.2 Convectional Aerator Tank (CAT) Chamber
Leached water from bagasse water dam is pump to a screening chamber to eliminate any
solid materials carried along. This water is black in colour free from bagasse and other
contaminants. It has a high COD of about 4000 as well as high BOD due to high organic load
in it. Its pH averages 3.3.
2.6.3 Flash Mixer
It is a small chamber where heavy polymer and coagulant are added to aid in flocculation and
coagulation. It has a stirrer that mixes water with the polymer, coagulant and a flocculant.
These chemicals are prepared in small tanks then drained off slowly into the inlet water line.
They are prepared depending on the level of contamination. Usually done by performing a jar
test and analysing the concentrations with best settling activity. It is usually done in a 1000ml
beaker. Scaling up is then done for the volume of the tank and the volume of water treated in
a day.
2.6.4 Equalization Tank
It is a tank responsible for pH conditioning. Rock Alum is added into the tank depending on
the volume of water and its Ph. It raises the pH to neutral. Agitator are connected to the tank
that ensures homogenous mixing.
2.6.5 Primary Clarifier
This aids in coagulation and settling of the formed flocs which are desludged after sometime.
It is connected to a stirrer that enhances circular uniform flow of water which aids in
agglomeration of flocs to form big particles which settle at the bottom of the clarifier.
Clarified water is collected through overflow collector line and directed to heat exchanger.
2.6.6 Heat Exchanger
The water from the dam has a temperature of about 30 0C depending on the room temperature
of that day. The temperature is boosted to about 40 0C by passing it through a heat exchanger.
The heat exchanger operates by taking in air, then heating it via coils then using the hot air to
raise the water temperatures.
2.6.7 Buffer tank
It boosts the working environment of the bacteria. Urea and DAP is added as food for
microorganisms. Hot water is also added to maintain the temperature of water at the buffer
tank. The tank is under disturbance to mix the content thoroughly with water.
2.6.8 Anaerobic Blanket Sludge Reactor Tank (UNBSR)
This tank contains high levels of sludge at the bottom habited by anaerobic microorganisms.
Waste water flows from the lower end. The outlets are connected at the uppermost end.
Desludging tubes are connected to the top in case high levels of sludge are noticed. The
bacteria feed on the organic matter through anaerobic respiration yielding pyruvic acid. The
acid is further converted to lactic acid. The bacteria use oxygen that is found in the organic
materials within the water. This process is important as it is able to stabilise water with little
biomass production. They key microorganisms are methane formers and acid formers. The
acid formers are microorganisms that create various acids from the sludge. Methane formers
convert the acids into methane. The continuous system continuously produces biogas as the
micro-organisms feed on the biodegradable materials. The methane gas produced is burnt in
free air to Carbon (IV) Oxide and water. This reduces the levels of COD to <1000.
34
2.6.9 Convectional Aeration Tank (CAT)
This tank contains inoculated aerobic bacteria that break down organic matter to carbon IV
Oxide and water. They are attached to media (cock-like floating material) that increase the
surface area for their action. The equation below explains aerobic respiration process.
C6H12O6 + O2 CO2 + H2O.
Oxygen is provided by use of compressors with tubing connected down the tank. They induce
bubbling effect. The tank is also sliding from the inlet end to enhance maximum aeration.
2.6.10 Secondary Clarifier
Used for sludge settling and recovery for recirculation by the use of pumps or damping the
sludge away if it becomes voluminous.
2.6.11 Moving Bed Bio Reactor
The water with sludge is kept on disturbance. The tank containing microorganisms that feed
on the remaining contents of organic matter. Here there are less volumes of sludge and
microorganisms due to low levels of COD and BOD. More aeration is achieved in this stage.
2.6.12 Chlorine Contact Tank
Chlorine in the form of Calcium hypochlorite is added to the tank. It is responsible for odour
removal, disinfection and bleaching. Light polymer and coagulant are added here
2.6.13 Accelerated Gravity Separator (AGS)
It has same operation as a clarifier with a stirrer in it. It helps in sludge recovery from MBBR
tank. and in water clarity as flocs are withdrawn from the bottom.
2.6.14 Activated Carbon Filters
Acts as adsorbent for removal of colour, odour and chlorine.
2.6.15 Multi Grade Filters
Filters off suspended particles and mud from water. It is backwashed in case of a difference
in OBR.
2.6.16 Treated Water Tank
Stored treated LTP water. When the volume increases the treated water is pumped to ETP
secondary Aerator tank 5. The water from here as a pH of 7.5-8, COD-150 and BOD- 30.
2.6.2 Sludge Disposal
2.6.2.1 Mud Sump
It is a tank that contains agitators. Excess sludge is pumped here then thoroughly mixed with
water before being separated by a centrifugal machine.
2.6.2.2 Continuous Centrifugal Machine.
It separates sludge from treated water. The water is conveyed in pipes to drying pond, which
have algae in them. The algae feed on nutrients in water and add dissolved oxygen to the
water. After some days of dilution, the water from ponds is pumped back to secondary
aerator tank.
35
36
2.7 PROCESS HOUSE
2.7.1 Process Control Room
It is a room with computers that have application which monitors all the processes in the
process house. The computers are controlled by a specialised who adjusts the inlet juice
valves, steam flow from the turbine, sweet water flow, steam flow rate to the centrifugal,
crystallizers, monitors brix of the syrup, detects temperatures and pH of the juices and also
monitors continuous pan.
2.7.2 Juice Treatment
Juice treatment involves juice clarification and separation methods. Mixed juice is made up
of the following composition:
Sucrose
Mud
bagacillo,
organic coloring matter
water
reducing sugars
wax
microorganisms.
37
2.7.2.0 Juice Treatment Flow Diagram
Secondary heaters primary heaters
Weighment
tank
Flash
Liming
tank
tank Limed juice
clarifier
tank
Telescopic valves
Syrup
tank
38
2.7.2.1 Weighment Tank
The tank is incorporated with flowmeter sensors that detects the volume of juice in the tank
and sense the signal to computers in the process control room. at any time. The juice enters
mixed juice tank with a pH of 5.4 and at 30- 35 0C. Phosphoric acid is added to the juice to
boost its concentration to 350 ppm. The Phosphates concentration in sugarcane varies
depending on the kind of soil grown on. Biocide is also added to kill the microorganisms
causing sucrose inversion to glucose and fructose. The leuconostic spp bacteria activity on
sucrose inversion are favoured by low temperature and low pH environment. Biocide is made
of chlorine compounds. When mixed with water, it forms hypochlorous acid which eats away
the cell walls of the bacteria, causing membrane permeability. Water flows into the cells of
the bacteria through osmosis, thus, the cells burst and the microbes die.
2.7.2.2 Heaters
Heaters functions to raise the temperatures of the juice. They are made up of a calandria body
filled with vertical tubes in 2 compartments and 6 chambers in each. Juice flows through the
first compartment with 6 chambers in the first chamber. At the 6th chamber, the juice
overflows to the second compartment first chamber and leaves at the sixth chamber.
Throughout heat is exchanged from a hotter media to a cold media. They are connected by a
double bit valve and a temperature gauge is connected on the outlet line. They have air vents
to allow hot noncompressible gases escape.
2.7.2.2.1 Raw Juice Heaters
Juice is pumped from the weighment tank to primary juice heaters. It is made up of 4 heaters,
where only two operate and the other two are standby heaters. In the 1st stage heating, the
juice temperature is raised from its room temperature to 450C by application of pan
condensates. In the second stage heating, the juice temperature is raised to 720C by the use of
3rd body vapours. The temperature is rise to increase the reaction rate of calcium ions with
phosphate ions in the liming tank. The condensate is connected directly to the sweet water
tank.
NOTE: Higher temperatures that this would result to sucrose inversion without the action of
microorganisms.
2.7.2.2.2 Secondary Juice Heaters
They are five heaters. It aids in clarification through heating and evaporation. Two are
functional at any time and the others are stand by. In the first stage heating, limed juice is
heated to 960C by application of 2rd body vapours. In the second stage heaters the
temperatures are raised to 1050C, and uses 1st body vapours. The juice flows to the flash tank.
2.7.2.2.3Tertiary Heaters
They are three heaters operating in parallel. As the juice leaves clarifiers, its temperatures
drop, due to high retention time at the clarifier and in clear juice tanks enhancing heat loss
and also heat loss in pipes. The clear juice leaves clear juice tank at a temperature below
1000C. Heater is used to raise the juice temperature to 1020C by the use of exhaust steam.
Clear juice should not enter the evaporators with a lower temperature, if this happens the
39
temperatures at the calandria will drop causing inefficiency in boiling and also contraction in
pipes which will cause high velocities in juice flow.
2.7.2.3 Liming Tank
It is a cylindrical tank with a low juice retention time. It is used to enhance maximum lime
conditioning of raw juice. Milk of lime is added on the top of the tank by the use of pumps in
the lime tanks. The lime is continuously agitated to ensure it maximumly dissolves in water.
It is added to raw juice flowing through gravity by junction pipe connecting pipe coming
from raw juice heaters. The pH of the juice from this tank is at 7.4. The reaction here
proceeds as follows;
2.7.2.4 Limed Juice Tank
This is an open tank that allows escape of vapours and gases. It also gives more room for
liming reaction.
2.7.2.5 Flash Tank
Juice enters tangentially to this tank. this reduces the flow rate of the raw juice, which may
cause disturbance on the clarifier. It has air vent to allow vapours escape through the top. It is
conical at the bottom end. This enhances large particles to agglomerate and flocs formation.
If vapours are not effectively eliminated, they cause buoyance effect at the clarifier. This
results to floating of the flocs at the clarifier which causes ineffective clarification. Juice
flows from the bottom of this tank through a siphon. This reduces the velocity of juice to the
clarifier. A flocculant is added from flocculation tank to the pipes. The flocculants used are of
polyacrylamide type. They include:
melfloc
kemira
R-300
Bufloc
Separan
Flopam
They function by coagulating suspended particles into flocs which bind together to form
bigger particles, by the aid of the polymer, and settle bottom of the clarifier since they have a
high density than juice.
40
2.7.2.6 Clarifier
Juice clarification at clarifier
The operation of clarifiers is to clarify juice by coagulation of flocs into larger ones that form
mud which settle at the bottom. It has a motor on the top and a shaft running to the bottom
attached to a mud booth. This causes centrifugal force and gravitational force which separates
materials depending on densities. The lighter materials settle at the top while heavy ones at
the bottom. The shaft has holes in each of the chambers which feeds juice to the four
chambers. When the juice if filled for clarifier 1 it overflows to clarifier 2. The clarifiers have
a scum chamber at the top which harvests any form in juice which may affect clarification
process. Form is due to reaction of CaO with other chemicals in the juice. The shaft is
connected to a skirt plate in each chamber. The skirt plates enhance reduce the falling force
of the juice thus reduce disturbance in the mud booth. The shaft is also connected to the
deflector plate which ensures uniform spreading of juice in a chamber. The mud booth
collects mud at the bottom of each chamber. It is connected directly to mud outlet valves in
each chamber. The outlets valves pour mud to a common header which conveys the mud to
mud-receiver tank. Each chamber has four compartments from which levels of separation are
checked. Compartment 1,2, and 3 have telescopic valve for discharging clear juice. If the
level of mud exceeds the second compartment, clarification begins failing, therefore, there is
a need for mud discharging from compartment 3 and 4 using mud discharge valves. The top
part of the clarifier has a pipe coil that collects overflow clear juice to the liquidation line.
41
pH is continuously monitored at the clear juice collector tank, connecting the common header
line, by the use of a litmus paper. The pH of juice should be neutral. Phosphoric acid is added
to the clear juice before proceeding to clear juice tank to increase the polarity of the juice.
The clear juice from the three clarifiers proceeds to clear juice tank for storage. The mud is
pump to a rotary vacuum filter for juice recovery and filter cake extraction. The clear juice is
then pumped form clear juice tank via clear juice heaters to evaporators.
It is a long retention time clarifier of Rapi Dorr 444 model. The company has three working
clarifiers and one short retention time clarifier that is yet to be commissioned. The retention
time for these clarifiers is 2-3 hours.
2.7.2.7 Evaporators
WESKOL has three sets of evaporators, A, B, C. Set B and C has 5 evaporators each while
that of A has six evaporator bodies. The evaporators bodies are those of Semi Keshner model.
The evaporator is made of;
Saucer
Calandria
Holder
Dome
Down take
Steam/vapour in
Tubes Calandria
Juice intake
Juice outlet
42
Dome
It makes up the upper part of the evaporator. Vapours from calandria move up the
evaporators to the dome. It contains brick like materials at the top. Due to variation in
temperatures below water boiling point, water vapour condenses and drops down the
calandria to preheat the juice. It is collected at the saucer by condensate tubes. Vapour
bleeding is applied by harvesting the hot vapours and directing them to the next evaporator.
This helps to conserve energy.
SK body 1,2 and 3 are used in vapour bleeding. The common header from dome has a
condenser box for harvesting condensates that escape the brick like materials, the
condensates are returned back to the evaporator. Vapours for SK 4 and 5 are conveyed in
vapour common headers to a condenser.
Condenser
It is used for vacuum creation in evaporators and pans.
Hot vapours from evaporator body 4,5 and pans flows to the condenser. The condenser is
made up of a vertical descending header carrying vapours in it. A horizontal pipe with cold
water at high velocity. The cold water meets vapours in a junction with high surface area than
the outlet. As a result, the vapours are contracted instantly and creates an empty space above
it. A vacuum line is connected at the junction to the evaporator or pan body, thus draws any
materials i.e., air to the condenser creating vacuum in the body.
Holder
It is the body of a rising film type evaporators. It is where evaporation takes place. It has
watch glasses for checking the syrup brix and the temperature of evaporators body. When
juice is heated, it boils from the calandria tubes to the holder losing vapours to the dome,
while the boiled juice is collected at the down take or in a gutter, connected on the walls of
SK body 1. The height of the holder gives room for water vapour to condense and flow back
to the saucer.
Calandria
It is occupied by vertical tubes of 4m height. Juice is fed from the bottom of the calandria
until juice occupies fully the calandria tubes. Vapour or steam flows to the tubes through
calandria. Juice boils above the calandria back and forth until the juice concentrates.
Concentration of juice to syrup is achieved by series flow of juice from the first body to the
5th body. The discharge line is connected to a discharge valve that regulates the flow of juice
from one body to another. Over brix of the syrup causes crystal formation at the syrup tank
which forms amorphous crystals and also may block pipes to the syrup feed tank.
Saucer
It is the bottom part of an evaporator. It has connected pipes that collects condensate from the
bodies and conveys condensates to a condensate Mond. A Mond is a condensate storage tank
with a pump that transfers condensates to sweet water tank.
43
Evaporator body 1 for Set A conveys its condensate to a condensate tank. The tank removes
vapours from the condensate and pumps it to boiler surface tank. This water has no sugar
traces in it.
Evaporator body 1 Set B conveys its condensate to surface tank directly.
Evaporator 1 Set C has a condensate cigar. Condensate flows through a U pipe that reached
the ground and flows back and pours condensate in the cigar just above its inner service. This
enhances maximum vapour elimination to the atmosphere. The condensate flows twice with
this mechanism and passes through a pump which supplies the condensates to surface tank.
SK body 1 evaporators use exhaust steam from turbines for boiling. The steam is at 1200C
and pressure of 1.2 bars. Their vapours are used for pan boiling in C- boiling. The bodies and
their calandria work under low pressure.
SK body 2 evaporators use vapours from body 1 and bleeds its vapours for body 3 boiling.
Part of its vapours are used for B- pan boiling. They work under low pressures.
SK body 3 evaporators boil juice from body 2. Their vapours are used for body 4 boiling and
in A-pan boiling. The holder is under pressure while calandria works under vacuum, due to
the effect of SK body four.
SK body 4 evaporators uses vacuum for boiling. Vacuum lowers boiling temperature thus, at
this point the body operates at 900C set point temperature. Excess vapours flow to the
condenser for vacuum creation.
SK body 5 evaporators applies vacuum in boiling. Juice boils here at 600C. Its vapours move
to condenser for vacuum formation.
The multi-effect evaporators work under Rillieux’s principle.
First principle
In a multi-effect evaporators of n effect, 1 kg of steam evaporates n kg of water. Thus, in a
double effect evaporator, 1 kg of steam will evaporate 2kg of water, in a triple effect
evaporator, it will evaporate 3kg of water and so on.
Second principle
If vapour is withdrawn from the ith effect of a multiple effect evaporator of N effects and used
outside the evaporator system in place of steam, the steam saving will be i/N times the
quantity of steam used in this study.
Third principle
Whenever stem or vapour is condensed, provision must be made to withdraw incompressible
gases continuously.
44
2.7.3 Juice Recovery
2.7.3.1 Rotary Vacuum Filter (RVF)
It is a cylindrical drum that oscillates along horizontal axes and uses vacuum to separate juice
from mud in a sugar factor for juice recovery.
Components of RVF
High and low vacuum vessels
Mud mixer
Bagacillo feeder
Spider tubes
Copper screen
Compressors
Mud trough
Rubber scrappers
Oscillating agitator
Hot water line
Filtrate tank
Motor
Mud from clarifiers is pumped into mud tank. the mud is filtered to separate juice from mud.
The polarity of the filter cake is expected to be below 1.5%. The reciprocating pumps draws
mud from mud tank/mud drum to the mud mixer. Bagacillo is continuously added to the mud
mixer through a chute at the rate of 7kg per tonne of cane crushed. The mixer has oscillating
stirrer that thorough mixes mud with bagacillo. This aid to increase the porosity to enhance
maximum sucrose recovery. It also prevents blockage of screen perforations by the mud.
From the mud mixer, mud flows through gravity to RVF trough. The trough has suspended
agitators connected to motor, they ensure homogenous mixing at the trough and that the mud
does not settle in the through. The RVF drum is rotated by help of motors at a revolution of
1/5 to 1/3 per minute. This gives high retention time for juice suction through screen
perforations (the screen has 625 perforations per sq. inch). The surface of the drum is
corrugated to increase mud holding ability. Hot water at 600C is sprayed on the drum to
increase juice extraction rate as low viscosity favours filtration.
The vacuum filter picks at low vacuum as it rotates and goes to high vacuum where juice is
sucked into the capillary tubes (spider pipes) as filtrate where the suction breaks and mud is
scrapped by a rubber scraper and falls to a conveyor to mud bin. Vacuum is created in the
condenser by compressing air and juice. The vacuum passes through filtrate receiver tank
which aid in sucking of juice (filtrate) from mud. The filtrate is pumped to filtrate receiver
tank, filtrate tank and pumped back to mixed juice tank.
The RVF drum is manually scrapped on parched that are seen to be wet at the rubber
scrapping head. The wetness is due to perforation blockage by the mud.
Procedure of starting RVF
i. Ensure the light (low) and heavy (high) filtrate valves at the filter drum ends are
closed for fast vacuum creation.
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ii. Fill up mud tank by opening the mud valves of the clarifier slowly.
iii. Start bagacillo mud mixer unit
iv. Start bagacillo fan and ensure that it delivers bagacillo to the mud–bagacillo mixer
trough.
v. Start rubber mud conveyor.
vi. Open vacuum filter condenser feed Valve.
vii. Start the vacuum to create vacuum in filtrate tanks
viii. Open spray hot water by opening the valve.
ix. Open the blight filtrate valve slowly to attain pick up and the heavy filtrate to attain
suction
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2.7.4 SUGAR HOUSE
2.7.4.0 Sugar House Flow Diagram
Crystallizer
Remelt tank
Pug mill
Weighing and
bagging B sugar C-massecuite
mingler crystallizer tank C-centrifugal
fore
warehouse
Pug mill
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Molasses
storage
2.7.4.1 PANS
Pans are used in sugar house for crystal formation, crystal growth and evaporation. They are
divided into three stages: A- boiling, for high grade sugar, B- boiling and C- boiling for low
grade sugar. The expected brix and purity of the massecuites must be achieved best crystal
sizes. Right working parameters must be maintained all through to avoid sugar loss
Diagram
Catcher
Heating vapor in
Condensate remover
Down take
Parts of a pan
Calandria
The calandria body is occupied by pipes shorter than those of evaporators but with larger
diameter. Heat is supplied at the calandria and boils the liquor on the tubes, the is
convectional flow of the fluids in the pan. Cold materials flow to the bottom while hotter
one’s flow to the top. This circulation helps in crystal growth. The seed for the pan is fed at
the calandria.
Body
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It is a hollow body that creates room for boiling and also for feeding of the pan with
maximum amounts of the mother liquor to enhance high rates of crystal growth. It also
provides vacuum in the pan which helps regulate the amount of heat used for boiling thus
overcome sucrose inversion and caramelization of the mother liquor/ massecuite. It also
creates a large surface area for escape of vapours from the juice.
Dome
It is the upper most part of the pan. It collects exhaust vapours from the pan and conveys
them to condenser for vacuum creation. It has a catcher that traps condensate escaping
with the vapours and drops them to the saucer for withdrawal.
Vapor line
Pans use vapours from evaporator bodies for heating. Vapour lines from evaporators are
connect to pans via vapour valve. The valves operate to close vapour flow or allow
vapour into the calandria.
Steam line
Hot water in form of condensate is used in boiler for lowering brix for massecuites,
hardening grains at intermediate zone of crystallization to dissolve false grains. It is also
used in pans with insufficient materials during boiling to avoid over brix. It is also used to
check the level of materials in the pan flash washing the watch glasses.
Proof stick
It is used to discharge small contents of materials in pan for brix checking and for sample
collection purposes. It is also used to shocking pan at intermediate zone to induce crystals
by causing disturbance in the pans by inducing air bubbles.
It is a pipe with a valve connected below the dome. It contains vapours that are used for
washing the pan after discharging contents as well as to boost temperature of the pan
before footing.
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Watch glasses
Saucer
Vacuum breaker
Used to withdraw vacuum from a pan before striking massecuites from the pan.
Discharge valve
High grade pans have pneumatic valves that uses pressure to operate. They are used to
allow massecuites into the crystallizer when striking and also when washing out. It has
discharge and lock valve.
They are used to transmit massecuite, grains or magma from one pan to another or from a
receiver to a pan by application of vacuum. It connects pans and receivers for each grade.
It is used for feeding the pan. It connects materials valves to the pan. It regulates the
amounts of materials entering the pan.
Slurry is made by crushing sugar crystals using a ball drum crusher into a thick slurry in
methylated spirit. Methylated spirit a product of isopropyl alcohol is used since it does not
dissolve sucrose. Essential oils can also be used such as glycerol and coconut oil.
After graining, and hardening using hot water to remove false crystals, feeding of the pan is
done using A- heavy or B- molasses in old house pans. Enough time is given for brixing.
They massecuite is then dropped into a crystallizer that feeds continuous pan. The pan cures
B massecuite and increases the brix percentage to 96%.
Continuous pan is used for crystal growth for B-massecuite. It has two modules and 8
compartments where B-massecuites meets A-heavy molasses and small contents of water to
dilute, it reduces chances of over brixing. On a normal working, the first four compartments
are feed with A-heavy open to maximum, the other compartment hot water valves are slightly
opened to allow small volumes of water to the compartments. It has a jigger system that vents
in non- compressible gases which may reduces the vacuum of the pan. They gases helps in
circulating the massecuite through the compartments. It discharges its content into a
horizontal crystallizer that pumps B-massecuite to a vertical crystallizer. The purity of B
massecuite ranges 67-74%
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2.7.4.1.3 C-Boiling
C- light molasses is used for seeding in this pan. There are four pans used here. The first 3
pans can be used for graining and striking while the last pan used for feeding and striking.
The capacities of this pans are 60 Tones. 5- liters of slurry is added to the pan for graining. A
brix of 98-99% must be attained in C-boiling. Usually, pan3 is used for graining then cuts its
content to any of two of the three pans. It is then washed and graining done again. The cut
contents are fed with B-molasses up to the fifth glass. Concentrating is then done to increase
brix, after which they are dropped. The purity should be 47%
Use of slurry- this is through introduction of fine crystals into mother liqour
Waiting- concentrating the mother liquor to super saturation for crystals to form
Shock method- use of proof stick to cause disturbance in concentrated liquor which
induces crystal formation.
2.7.4.2.2 Striking
vi. Open vacuum breaker valve
vii. Unlock and open discharge valve checking the volume of crystallizers not to pour
the contents outside. Drop all the contents into crystallizer then wash your pan.
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Feeding- addition of mother liquor to grains
2.7.4.2 CRYSTALLIZERS
Massecuite is stored in the crystallizer momentarily before curing though A-massecuite is can
be cured immediately. The massecuite cools in the crystallizer to temperatures of about 50 0C.
This further enhances formation of sugar crystals. Also, in the crystallizer is a slow rotating
stirrer that prevents the massecuite from settling and hardening.
Low grade massecuite is passed through the vertical crystallizer where it is stored for a
minimum of 21 hours. Vertical crystallizers work by adjusting the temperatures of the
massecuite to 500c. They are long cylindrical vessels with cold water pipes from the bottom
and hot water pipes from the top. Massecuite enters through the top, travels to the bottom and
back through another shell. The overflow discharges in pug mills. This enhances further
crystal formation in low grade sugar.
The massecuite is transmitted to the pug mill where it is also stored momentarily with
continued stirring to enhance further cooling before entering centrifugal.
2.7.4.3 CENTRIFUGAL
Massecuite from pug mill is conveyed through a chute to the centrifugal bottom bulb. The
bulb is spinning at a high velocity. Due to effect of centrifugal force, the massecuite is pushed
to the screen of the basket. The basket is also spinning. The wash valve opens on the set delay
time and sprays hot water on the screen. The centrifugal spins at an increased speed to dry the
sugar. A heavy molasses is collected at first wash at the separator which feeds the A-heavy
tank. After the set spinning time, the bottom bulb is lifted by hood lifter, and the plough sets
to plough off sugar in the basket and moves downwards cutting sugar to the bottom. Sugar
drops to receiving hooper. The bottom bulb the closes the discharge. Second wash is done to
get A wash molasses.
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It is called batch because massecuite addition into it is not continuous. It is majorly used in
the separation of A-massecuite to A-sugar A-wash and A-heavy molasses.
2.7.4.3.1Batch Centrifugal
Works by the action of pressure sensors set on time.
The valve is closes and massecuite is let into the centrifuge. The machine then accelerates
and run for a while a speed of 200rpm. This causes the massecuite to spread evenly to the
side of the screen. Also, excess molasses is separated via the screen to the molasses storage
tank.
It then accelerates to a speed of 1500rpm and void molasses in between the sugar crystals is
separated and moves to the molasses tank. Water of temperature of 1100C is then sprayed on
the sugar and removes molasses on the surface of sugar crystals called A-wash.
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Driver motor
Motor brake
Pug mill
Charge sensor
Plough
Diagram
Funnel
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funnel pipe
Screen
distributor
rotating motor
connecting belt
molasses chamber
motion of sugar
Massecuite is mixed with water at the funnel and flows through the central funnel duct into
the distributor. The distributer distributes massecuite evenly around the centrifugal as well as
retains foreign material around the basket.
The molasses is then separated via the conical screens and moves to the molasses chamber
while the magma is retained and moves upward the conical screen. Magma from the B and C
centrifugal is stored in receiver tanks and used as seed in A and B sugar growth respectively.
2.7.4.4 DRYING
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carried with a belt conveyer to the grader via an electromagnet which traps the metal
impurities in the sugar.
ID fan- creates vacuum in the dryer pulling sugar from the dryer as well as collecting dust
and transmitting it to a dust dissolver tank.
FD fan- creates air pressure in the dryer which bubbles sugar to allow hot air pass through it
aiding in drying.
Radiator- it is a liquid-gas heat exchanger system. Cold air is pumped by FD fan into the
tubes of radiator, hot water is forced to pass on the tubes of the radiator heating air in. Hot air
controlled by air control dampers, flows through screens below the sugar holder plates and
bubbles sugar crystals on the first two chambers. The first chamber temperature should not
exceed 700C and of the second chamber at 50 0C. The other two chambers are connected with
cold water tubes on the sugar carrier plates. They cool the temperature of sugar to 33 0C this
ensures sugar does not burn the packaging bags. At the outlet of the dryer are two magnet that
traps any metal on sugar.
2.7.4.5 GRADER
Works under the principle of weight imbalance caused by eight crates connected on opposite
sites by a motor. The body of the grader is mounted on springs that enhance vibration due to
high revolving irregular crates. A vibron motor is connected at the top of the grater that
vibrates to spread sugar crystals on grader sieve.
The grader contains three screens which first separate lump sugar, then commercial sugar and
finally fine powdery sugar. The lump and powdery sugar is not suitable for consumption and
is therefore sent to the dissolution tank where water is added to it. It is then conveyed to the
re-melt tank by a screw conveyer, where its temperature is boosted which further enhances
dissolution then to the A-pan boiler.
The commercial sugar is carried by bucket elevators to the sugar bins where it is stored
momentarily while awaiting bagging.
Weighing and bagging is done by an automated system. The bag is placed into position by
the bagging operator. It is held to position by arms that employ a pressure system and filled
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with sugar to the required weight. Pressure is the released which intern releases the arms and
the filled bag. Pressure release is done by a weight sensor, that is, it releases only if the
required weight has been reached. The bags are then carried by a manually controlled
conveyer and sewed, then carried by hand to a convey to the warehouse where it is stored
prior to transportation to the market for sale.
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20 grams of sugar was accurately measured in an aluminum dish.
It was then placed in an oven for 4 hours.
The sample was the removed and placed in a desiccator.
(initial weight −finalweight )
moisture content = ×100
initial weight
absorbance ×100
sugar colour=
concentration
g
( )
cm3
× cell diameter
2.8.3 pH determination
The electric method was used. This was carried out for the raw juice, limed juice, syrup,
boiler water, service water and the condensate.
Procedure
i. The pH meter was calibrated using a buffer solution.
ii. The sample was then cooled to room temperature.
iii. The electrodes were then rinsed with the sample to be tested.
iv. The beaker was filled with enough sample to cover the bulb of the glass electrode.
v. The system was then left to come to equilibrium and the pH read and recorded.
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vi. On reading the electrode was washed with distilled water and left in the distilled water
or buffer.
X−W
water insoluble matter=
10000 mg/kg
2.8.5 Determination of moisture in bagasse
Procedure
Weight of the tray was taken and recorded as M.
100grams of bagasse or filter cake sample was measured while on the tray.
The tray with bagasse or filter cake was then placed in an oven at 1050C for 3 hours.
The sample was then removed and weighed immediately and recorded as P.
Calculation
Weight of tray=M
Weight of sample on tray=N
Weight of sample dry=P-M=V
Weight loss=N-V
weight loss
moisture content = ×100
initial weight
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The sample was taken in a test tube and cooled.
5 drops of 1-naphtol were added and shaken well.
Concentrated sulfuric acid was then slowly added from the side and checked for the
color of the ring.
If it was purple then there were sugar traces else if it was green there were no sugar
traces.
(d) Molarity -it is the number of moles per liter of a solution in 1000ml
(f)Normality - it is the number of moles of active ions taking part in a chemical reaction
(g) Juices:
•First expressed juice-Juice from the first and second rollers of the milling tandem
•Last expressed juice- Juice expressed from last two rollers of the milling tandem
•Mixed juice-
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volume or weight of juice in the tank. It should be such that the volume collected at end of
two hours is about three liters. The analysis should be for each two hours composite.
•Limed juice- Juice that has undergone liming process by addition of lime
(h)Filter mud-The material removed from the process by filtration including aid.
(i) Filtrate-Liquid that has passed through the screen or cloth or filter.
(b) Measure 2.5kg of sugar and drive it to machine by help of its funnel on top of it
(c) Measure 3litres of methylated spirit, drive it inside the machine via funnel
(d)Start the machine, check and remove it after six hours of a solution =(Density × Assay ×
1000) / 100x molecular weight Or. M = (density ×Assay ×10) /molecular weight
CHAPTER THREE
3.1 CHALLENGES
During the attachment training we face several challenges which include;
•At the boiler there was a lot of dust and dirt due to bagasse waste and carbon
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•Language barrier-various operators were not that fluent as they were highly affected by
mother tongue
• False information-some operators gave false information in fear of we may come back and
substitute their relevant position.
3.2 RECOMMENDATIONS
During the 12 weeks of attachment, I felt like the following should be improved.
Recharging of the carbon bed used in water treatment should be done by use live steam from
the boiler instead of replacement which is more costly.
The line carrying exhaust steam in the process that bursts at times due to high pressure should
be installed with a spring valve to bleed out steam when the pressure increases.
The lab attendants should be supplied with gas masks, goggles and gloves to prevent them
from effects of harmful gases, spurting and corrosive chemicals during the mixing of the
chemicals
The workers at the boiler should be provided with goggles due to the high amount of dust
produced by the bagasse and unburnt carbon
All workers in process should also be given ear muffs just the same way dusts coats and
helmets by the company
The company also to allocate a special training team for all those students on attachment at
their respective departments
3.3 CONCLUSION
My experience at Sony Sugar Company was very enriching. I was able to relate classroom
theory to practical situation by assimilation of theoretical information which was otherwise
hard to picture without its practicality. I also got some experience of how an industry operates
and the different responsibilities expected of me as well as different problem-solving
methods.
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b. Steam generation, at the boiler we learnt various concepts that we had covered in
class about, the quantity of steam to be produced and the pressure needed. We also
learnt the importance of the economizers and air preheaters for efficiency in working
of the boiler by recirculation of condensed water.
c. Heat transfer, we learnt on the importance of controlling the amount of heat to be
transferred to the material from the heating steam in the pans and evaporators.
d. Thermodynamics, we leant on the effect of introduction of vacuum to the boiling
point of a liquid in the pans and evaporators where the boiling temperatures were
greatly reduced.
3.4 REFERENCE
www.sugarprocessingtech.com
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