Thermo EXcirculator
Thermo EXcirculator
NESLAB EX Series
Bath/Circulator
Thermo Scientific Manual P/N U00696 Rev. 03/06/07
Installation
Operation
Basic Maintenance
Dieselstrasse 4
D-76227 Karlsruhe, Germany
Tel : +49 (0) 721 4094 444
Fax : +49 (0) 721 4094 300
Building 6, No. 27
Xin Jinqiao Rd., Shanghai 201206
Tel : +86(21) 68654588
Fax : +86(21) 64457830
info. [email protected]
Statement of Copyright
Users are forbidden to reproduce, republish, redistribute, or resell any materials from this manual
in either machine-readable form or any other form.
Table of Contents
Preface
Compliance .............................................................................................................. 2
WEEE/RoHS ............................................................................................................. 2
Unpacking ................................................................................................................ 2
After-sale Support.................................................................................................... 3
Warranty ................................................................................................................... 3
Feedback ................................................................................................................. 3
Section I Safety
Warnings .................................................................................................................. 4
Section V Troubleshooting
Error Codes ........................................................................................................... 39
External Sensor Connector ................................................................................... 40
Checklist ................................................................................................................. 41
Service Assistance ................................................................................................. 42
Controller PID Values ............................................................................................. 42
BOM Decoder ........................................................................................................ 42
Displaying Software Version Number .................................................................... 43
Appendix A Fluids
Appendix B NC Serial Communications Protocol
Appendix C International Quick Reference Guide
WARRANTY
-1-
Preface
Compliance
Listed to:
UL 61010-1 2nd Edition
CSA C22.2 #61010.1 2nd Edition
WEEE/RoHS
This product is required to comply with the European Union’s Waste Electrical
& Electronic Equipment (WEEE) Directive 2002/96/EC. It is marked with the
following symbol:
Unpacking
Retain all cartons and packing material until the unit is operated and found to
be in good condition. If the unit shows external or internal damage contact the
transportation company and file a damage claim. Under ICC regulations, this is
your responsibility.
-2-
After-sale Support
Thermo Fisher Scientific Corporation is committed to customer service both
during and after the sale. If you have questions concerning the unit operation,
contact our Sales Department. If your unit fails to operate properly, or if you
have questions concerning spare parts or Service Contracts, contact our
Service Department. See the back side of the cover for contact information.
The unit’s BOM number and serial number are printed on the name plate label
located on the rear of the unit. See page 42 for instructions on how to decode
your unit's BOM number. See page 43 for instructions on how to display the
software version.
BOM#: XXXXXXXXXXXX
S/N: XXXXXXXXX
XXX VOLT XX HZ X PH X.X AMP
Warranty
Thermo Scientific NESLAB EX units have a warranty against defective parts
and workmanship for 24 months from date of shipment. See back page for
more details.
Feedback
We appreciate any feedback you can give us on this manual. Please e-mail us
at [email protected]. Be sure to include the manual part
number and the revision date listed on the front cover.
-3-
Section I Safety
Warnings
Warnings are posted throughout the manual. These warnings are designated
by an exclamation mark inside an equilateral triangle and text highlighted in
bold. Read and follow these important instructions. Failure to observe these
instructions can result in permanent damage to the unit, significant property
damage, or personal injury or death.
The lightning flash with arrow symbol, within an equilateral triangle, is intended
to alert the user to the presence of non-insulated "dangerous voltage" within
the unit's enclosure. The voltage may be of significant magnitude to constitute
a risk of electrical shock.
This label, engraved into the front of the tank lip, indicates the presence of hot
surfaces.
Make sure you read and understand all instructions and safety precautions
listed in this manual before installing or operating your unit. If you have any
questions concerning the operation of your unit or the information in this
manual, contact our Sales Department.
The user is responsible for the fluid used. Never use pure ethylene
glycol as a bath fluid, the flash point of 100% ethylene glycol is 111°C.
100% ethylene glycol may produce flammable vapors that can be
ignited by an open flame or an ignition source. When mixed with
water, ethylene glycol is not flammable. Also, at high temperatures
pure ethylene glycol may produce hazardous vapors.
Always turn off the unit and disconnect the line cord from the power
source before performing any service or maintenance procedures, or
before moving the unit.
-4-
General Information
Section II General Information
Indicates heater status.
See page 17.
Press to sequence
Indicates the controller is through the three indicators
displaying the setpoint. Press and accept the displayed
the arrow buttons to change the value. See page 17.
value. See page 17. NOTE: None of the three
setpoint indicators are
visible unless this key is
pressed.
Press to mute the alarm. See
page 22. Digital Plus controller
only. Press to select the
temperature offset
mode. See page 23.
Press to select external Digital Plus controller only.
Press to select the timer
sensor. See page 22. Digital
function. See page 23. Indicates the controller is displaying
Plus controller only.
Digital Plus controller only. the high temperature alarm
Indicates the controller is setpoint. Press the arrow buttons
Press to select the serial
displaying the unit's low to change the value. See page 17.
communication mode.
temperature alarm setpoint.
See page 22. Digital Plus
Press the arrow buttons to
controller only.
change the value. See page 17.
Autorefill connection.
RS-232/RS-485 Circuit
connections. See Breaker(s).
Appendix B. Digital
Plus controller only.
Power connection.
Reservoir. See page 16. See page 11.
1/8" OD Autorefill fluid
connection. See page 29.
-5-
Quick Reference Operating Procedures
General Information
Operation
Before starting the unit, double-check all electrical
and plumbing connections. Make sure the bath is
properly filled with fluid.
press again.
-6-
Description
General Information
The Thermo Scientific NESLAB EX Bath/Circulators are designed to provide
temperature control for applications requiring a fluid work area or pumping to an
external system.
Units consist of a circulation pump, seamless stainless steel bath, work area
cover, and a microprocessor temperature controller.
Specifications
EX 7 EX 10 EX 17 EX 35
Process Fluid
Temperature Range2 Ambient +12°C to +200°C
3.7 12
Pressure
2.4 8
1.2 4
Heater (Watts)
115V/60 Hz Models 800 1600
230V/50 Hz Models 2000 2000
100V/50-60Hz Models 800 1200
Bath Work Area5
(W x L x D)
Inches 6 5/8 x 7 x 6 8 ¾ x 8 1/8 x 6 8¾ x 8 1/8 x 9 8 ¾ x 15 ½ x 12
Centimeters 16.8 x 17.8 x 15.2 22.4 x 20.6 x 15.2 22.4 x 20.6 x 22.9 22.4 x 39.4 x 30.5
Bath Volume
Gallons 1.9 3.0 4.8 9.6
Liters 7.2 11.3 18.1 36.3
Weight6
Pounds 27 32 36 53
Kilograms 12.2 14.5 16.3 24.0
1. Specifications subject to change.
2. Above 80°C, baths are tested with silicone oil. This fluid is known to release a formalde-
hyde vapor (which is carcinogenic) above 150°C.
3. 37°C, 45°C, 60°C bath temperature. 20°C ambient. Measured at the center of the work area,
stable ambient. Sea level. For 37°C the work area cover was off, for 45°C and 60°C the work
area cover was on. No external flow. For some applications, agitation and stability above
ambient may be improved by connecting a small length of hose between the pump connections
on the rear of the unit.
4. 20°C ambient. 20°C bath temperature using water. Pump fully loaded. Sea level.
5. See next page for additional dimensions.
6. Add approximately 3 pounds (1.4 kilograms) for shipping weight.
-7-
General Information
F
7
/8 ½
30°
A
3¼ 17/8
105°
15/8
D
23/8
15/8
B
1½
Unit Dimensions EX 7 EX 10 EX 17 EX 35
Time to Temperature
115V/60 Hz Models
-8-
Time to Temperature
115V/60 Hz Models
General Information
230V/50 Hz Models
230V/50Hz Models
-9-
Blank Page.
- 10 -
Section III Installation and Operation
Site
Ambient Temperature Range +50°F to +104°F (+10°C to +40°C)
Overvoltage Category II
Electrical
Requirements
The unit construction provides protection against the risk of electrical
shock by grounding appropriate metal parts. The protection may not
function unless the power cord is connected to a properly grounded
outlet. It is the user's responsibility to assure a proper ground connec-
tion is provided.
The user is responsible to ensure that the power cord provided meets local
electrical codes. If not, contact qualified installation personnel.
The unit is intended for use on a dedicated outlet. The EX has an internal
circuit protection that is equivalent (approx.) to the branch circuit rating. This
is to protect the EX, and is not intended as a substitute for branch circuit
protection.
Refer to the serial number label on the rear of the unit to identify the specific
electrical requirements of your unit.Ensure the voltage of the power source
meets the specified voltage, ±10%.
- 11 -
The following power options are available:
- 12 -
Plumbing Requirements
Ensure the unit is off before connecting tubing to the unit.
Hose Connections
The pump connections are located at the rear of the pump box and are labelled
(pump outlet) and (pump inlet). These connections are bent upward
The pump lines have ¼" MPT for mating with standard plumbing fittings. For
your convenience stainless steel adapters, ¼" FPT to 3/8" O.D. serrated fitting,
are provided. (To assure proper fit, they should be installed using 1½ turns of
Teflon® tape around the threads.)
Make sure all tubing connections are securely clamped. Avoid running
tubing near radiators, hot water pipes, etc. If substantial lengths of tubing
are necessary, insulation may be required to prevent loss of cooling capacity.
Tubing and insulation are available from Thermo Fisher. Contact our Sales
Department for more information (see Preface, After-sale Support).
It is important to keep the distance between the unit and the external system
as short as possible, and to use the largest diameter tubing practical. Tubing
should be straight and without bends. If diameter reductions must be made,
make them at the inlet and outlet of the external system, not at the unit.
If substantial lengths of lines are required, they should be pre-filled with bath
fluid before connecting them to the unit. This will ensure that an adequate
amount of fluid will be in the bath once it is in operation.
Drain
The unit is equipped with a drain located at the back of the unit labelled .
To drain the reservoir attach a hose to the barb and loosen the fitting. The
fitting has a stop to prevent it from coming off.
Pumping
The pump is designed to deliver a flow of 15 liters per minute (4 gallons per
minute) at 0 feet head. To prevent external circulation, the pump inlet and
outlet lines on the rear of the unit are capped. The caps must be removed when
external circulation is required.
To properly secure external hose connections to the unit, wrap Teflon® tape
around the pipe line threads before installation. Once the hose connections are
made, the hoses must be properly plumbed to an external system. It is
important the bath is not in operation until all plumbing is complete.
- 13 -
Tap Water
Cooling Coils
The unit is equipped with a cooling coil located behind the stainless steel baffle
in the bath, see page 5. The coil is useful for maintaining near-ambient tem-
peratures, or when cooling from elevated temperatures. Temperature stability
can also improve by circulating cold fluid through the coil. For best results, the
fluid should be at least 5°C below the temperature setpoint. The required fluid
flow rate depends on the type of fluid, the setpoint, and the desired stability.
Installation and Operation
The plumbing connections for the cooling coil are 3/8 inch OD stainless steel
tubes located on the lower rear of the unit. These connections will accept
3
/8 inch or 5/16 inch ID tubing. Tubing is available from Thermo Fisher.
Connect the cold fluid source to either fitting. Connect the other fitting to the
cold fluid return (or drain if tap water is being used).
- 14 -
Circulating to an open container
Levelling
Device
Outlet Inlet
Support the leveling device over the open container with a ringstand. Stagger
the tubes in the leveling device so one tube is submerged in the vessel fluid,
and the other tube is level with the fluid surface. Connect the deeper tube to
the pump outlet and the shorter tube to the pump inlet.
Adjust the flow rate using the accessory flow control valve connected to the
pump outlet, or by partially restricting the outlet tubing. When properly
adjusted, the pump inlet will draw an occasional air bubble to prevent over
flow, and the pump outlet will force fluid through the submerged tube to
prevent aeration of the vessel.
To avoid siphoning the bath work area when the unit is shut off, lift the
leveling device out of the vessel and above the level of the unit.
Pump Box
System #1
Bath
Work Area
System #2
The pump can be used to circulate through two closed-loop systems. Connect
the shortest practical length of flexible tubing from the pump outlet to the inlet
of external system #1. Connect the outlet of system #1 directly into the bath
work area. Connect tubing from the bath work area to the inlet of system #2.
Connect the outlet of system #2 to the pump inlet.
- 15 -
Fluids
The user is always responsible for the fluid used. Never use flammable
or corrosive fluids with this unit. The use of chlorine or sodium
hypochlorite in the baths will cause pitting that could damage the
heater coils.
Wetted materials of bath include; 316 and 304 Stainless steels, Ryton® (PPS),
Teflon®(PTFE) and Ethlyene-Propylene rubber (EPDM).
Ethylene glycol and water, propylene glycol and water, silicone oil, and filtered
water are acceptable fluids. See Appendix A for additional information.
Please call Thermo Fisher customer service to discuss high temperature fluid
selections. However, we will often refer you to chemical companies specializ-
ing in heat transfer fluids.
Filling
Requirements
Ensure the drain on the back of the unit is closed before filling the unit.
The bath work area has a high and low level marker to guide filling. The
markers are 1 inch horizontal slits located in the center of the stainless steel
baffle separating the work area and the pump assembly. The correct fluid
level falls between these two markers.
NOTE: The unit is equipped with a reservoir level float switch. The switch
prevents the unit from starting if the fluid is below the lower slit.
- 16 -
Controller
(Digital One/Digital Plus)
The controller controls temperature using a Proportional-Integral-Derivative
(PID) algorithm. It is designed with self-diagnostic features and easy to use
operator interface. Two controller options are available: Digital One and Digital
Plus. The information on the following two pages applies to both controllers.
The information on the following two pages applies to both controllers.
ON/OFF. Use this key to toggle the unit on or off and to clear error mes-
sages.
SCROLL . Use this key to scroll through the controller's LEDs. It is also
used to save new changes.
Indicates heater status. It illuminates to indicate the heater is adding heat from
the bath fluid. The indicator is off when heat is not being added.
- 17 -
NOTE: The following indications are not visible until is depressed.
To adjust the displayed value use the arrow buttons. Pressing an arrow button
will cause the display to stop flashing and to indicate the new setpoint value.
Save the change by pressing SCROLL. The new setpoint value will rapidly flash
for two cycles and then the controller will return to the reservoir fluid tempera-
ture display.
If SCROLL is not pressed within 60 seconds the change will time out and revert
to the original setpoint. The controller will automatically return to the reservoir
fluid temperature display.
NOTE: You can not adjust the setpoint closer than 0.1°C of either temperature
limit, and you can not adjust either temperature limit within 0.1°C of the
setpoint. Trying to do so will cause the indicator to flash and, on Digital Plus
controllers, the alarm to beep.
On units with the Digital Plus controller, pressing the Mute button prior to
pressing SCROLL will abort any changes and return to the reservoir fluid
temperature display.
- 18 -
Start Up/Shut Down
(Digital One/Digital Plus)
Pre-Start Before starting the unit, double check all electrical and plumbing connections.
Ensure the bath reservoir is properly filled. The unit will not start if the reservoir
fluid level is below the lower horizontal slit.
The unit can be configured for automatic restart. If the unit shuts down as
a result of a losing power, once power is restored the unit will restart.
See Setup/Tuning Loop on page 21 to enable this feature.
Starting Press . The controller does a self-test (sequences through the LEDs, and
Digital Plus units momentarily sound the alarm), then quickly displays the
setpoint before displaying the reservoir fluid temperature. The pump will start.
NOTE: If the unit's recirculating fluid is outside either temperature limit, the unit
will start but the appropriate indicator will flash until the fluid is within the limit.
On units with the Digital Plus controller, pressing Mute prior to pressing
SCROLL will abort any change and return you to the fluid temperature display.
- 19 -
Low Temp Alarm To display/change the low temperature alarm setting press until
illuminates. The display will flash the current limit value. Use the arrow buttons
to change the value. You can not set the alarm closer than 0.1°C below the
setpoint. Attempting to causes the indicator to flash and, on Digital Plus
controllers, sounds the alarm.
On units with the Digital Plus controller, pressing Mute prior to pressing
Installation and Operation
SCROLL will abort any change and return you to the fluid temperature display.
Once the desired setting is displayed, press again to confirm the change.
The display will rapidly flash the new value twice and then return to the recircu-
lating fluid temperature. If the new value is not confirmed within 60 seconds the
display will return to the fluid temperature and ignore any change.
High Temp Alarm To display/change the high temperature alarm setting press until
illuminates. The display will flash the current setting value. Use an the arrow
buttons to change the value. You can not set the alarm closer than 0.1°C
above the setpoint. Attempting to causes the indicator to flash and, on Digital
Plus controllers, sounds the alarm.
On units with the Digital Plus controller, pressing Mute prior to pressing
SCROLL will abort any change and return you to the fluid temperature display.
Once the desired limit is displayed, press again to confirm the change.
The display will rapidly flash the new value twice and then return to the recircu-
lating fluid temperature. If the new value is not confirmed within 60 seconds the
display will return to the fluid temperature and ignore any change.
Stopping To turn the unit off, press . The pump will stop.
- 20 -
Setup/Tuning Loop
(Digital One/Digital Plus)
The Setup/Tuning Loop is used to tune the controller's PID parameters (HEAt);
enable/disable auto restart (AStrt); determine how the unit will react when a
fault occurs (FAUlt) — either shut down (on) or continue to run (oFF); and to
configure the temperature display to indicate to a tenth or a hundredth of a
degree (rES).
Changes made in the Tuning/Setup Loop take affect when Yes is pressed at
No
the StorE prompt. Pressing at the prompt aborts all changes.
- 21 -
Controller
(Digital Plus)
Alarm. If the alarm sounds, use this button to toggle the alarm off and on. If
the cause of the alarm is cleared but then reoccurs, the alarm will sound again.
Mute
The button is also used to abort changes to the setpoint and temperature
alarms. It is also used to abort changes when configuring the unit for external
Installation and Operation
NOTE: Pressing and holding any of the following buttons for five seconds takes
you to their calibration or setup loop.
External Probe. Pressing the Sensor button displays the external probe
temperature and lights the LED indicating that the bath is monitoring and
Sensor controlling to this temperature. The unit will continue to monitor the internal
bath temperature to ensure the bath is running in a safe operating mode.
NOTE: If there is no sensor attached (or the circuit is open), or serial communi-
cations is enabled, the button will flash, and the alarm will beep three times.
The display will momentarily show an error message and then return to the
reservoir fluid temperature.
NOTE: The temperature display may drift for up to 10-15 seconds when
transitioning between temperature sensors. This is normal operation.
Once enabled, the Computer LED will flash when sending and receiving
signals. See Appendix B for additional information.
You can also turn the unit off by pressing but the unit will remain in the
serial communication mode. To restart, send another start command.
NOTE: If the unit is shut down in the serial communication mode and you need
to start the unit using the local controller, simultaneously depress and hold
both arrow keys for approximately 10 seconds. The display will then show the
internal probe temperature, and the alarm will sound. Press the LED
Computer
and turn off the LED and disable serial communications. Turn the controller off
using . You can now start and operate the unit with the keypad.
To setup for serial communication see Computer Setup Loop on page 24.
- 22 -
Timer. Pressing the Timer button enables/disables the Timer function of the
bath. You can define the current time, a turn-on time, and a turn-off time.
Timer
To setup the bath for timer operation see Timer Setup Loop on page 25.
If the bath is turned off using with the timer mode enabled, the Timer LED
will go out and the timer mode will be disabled. With the bath off, you have to
If a power disruption occurs, the timer mode is disabled. The Timer Setup Loop
will have to be used to restore the settings.
Temperature Offset Mode. Pressing the Offset button, with the bath on,
enable/disables the temperature offset mode. This mode changes the tempera-
Offset ture displayed on the bath a user defined amount. The LED will be lit when this
mode is enabled indicating that the temperature displayed is an offset value.
NOTE: The temperature offset only affects the displayed value when the offset
mode is enabled, the other setpoint values still dictate unit performance.
To setup the bath for offset mode operation see Offset Setup Loop on page 26.
If you press the Offset button when an offset has not been previously defined,
or if serial communications is enabled, the button will flash, the unit will beep
three times, and the display will momentarily show an error message. In either
case the function can not be enabled.
NOTE: Use this feature only when the bath is at a stable temperature.
In either local or Computer mode with offset disabled, the unit controls to and
displays the calibrated value for the internal or external probe, whichever is
selected.
In local mode with offset enabled, the unit still controls to the calibrated value,
not the offset value, for the internal or external probe. The display shows the
calibrated value with the offset value added.
In Computer mode with offset enabled, the unit still controls to the calibrated
values, not the offset value, for the internal or external probe. The display
shows the calibrated value with the offset value added. If you send a signal to
the bath to display internal or external probe temperatures, the calibrated value
is returned. If you send a signal to change the display value the offset value is
returned.
- 23 -
Computer Setup Loop
(Digital Plus Only)
NOTE: The Computer Setup Loop is not available if the serial communications
mode is enabled. Review/change the settings before entering the mode.
Computer The Computer Setup Loop is used to set the serial communications protocol
parameters. With the bath on, press and hold the Computer button for five
seconds. The controller will display SErL. Press the arrow buttons to toggle
between 232 and 485. Press the Computer button to hold the protocol and
Installation and Operation
advance you through the loop to adjust the remaining parameters. Press the
arrow buttons to adjust any parameter. When StorE is displayed press YES to
accept any new values, NO to abort them.
If the Computer button is not pressed for 60 seconds the function will time-out
and the changes will not be saved. Pressing the Mute button will also exit the
Computer Setup Loop and return you to the reservoir fluid temperature display.
Once enabled, the Computer LED will flash when sending and receiving
signals. See Appendix B for additional serial communication information.
SErL 485
Computer
19200
9600 Yes
Factory preset = 19200
bAud 4800
2400 No
1200
600
Computer
300
Factory preset = 1
Yes (RS-485 only)
Addr 1 to 100
No
Computer
No
StorE
Yes
Accept All Changes
- 24 -
Timer Setup Loop
(Digital Plus Only)
To set the timer, with the bath on, press and hold the Timer button for five
seconds to access the controller's Timer Setup Loop. The display will indicate
diSP. Use the arrow buttons to select the desired clock display. Press the
Timer
Timer button and the controller will display cloc. Use the arrow buttons to
display the correct time.
Press the Timer button and the controller will display t-On. Press the arrow
If the Timer button is not pressed for 60 seconds the function will time-out and
the changes will not be saved. Pressing the Mute will also exit the Timer Setup
Loop and return you to the temperature display.
If the bath is turned off using with the timer mode enabled, the Timer LED
will go out and the timer mode will be disabled. With the bath off, you have to
press the Timer button to enable the timer mode and light the LED.
- 25 -
Offset Setup Loop NOTE: Use this feature only when the bath is at a stable temperature.
(Digital Plus Only)
Press the Offset button to display the current offset temperature value and
illuminate the LED.
Offset
To change the value press and hold the Offset button for five seconds to enter
the controller's Offset Setup Loop. The bath will alternately flash oFSEt with
the current temperature.
Use the arrow buttons to change the value. For example, if the bath is at
Installation and Operation
+40°C and the desired offset is +5°C, change the display to +45°C. Press the
Offset button once the desired offset is displayed. (If the Offset button is not
pressed the function will time-out and the change will not be saved.) The
display will show StorE. Press YES to accept the value, NO to abort it.
If, after pressing YES, the display returns to +40°C, not +45°C, the Offset
button was not depressed when you entered the Offset Setup Loop. Press the
Offset button to display the offset temperature and illuminate the LED.
Yes
OFSEt xxx.x
No
Offset
No
StorE
Yes
Accept All Changes
NOTE: Offset only changes the display of the enabled probe. Setpoint and
alarm values will display the non-offset value.
If you press the Offset button when an offset is 0 or not defined, or if serial
communications is enabled, the button will flash, the unit will beep three times,
and the display will momentarily show an error message (Er53 for offset
undefined, Er54 for serial comm on). In either case the function can not be
enabled.
With offset disabled, the unit controls to and displays the calibrated value for
the internal or external probe, whichever is selected.
With offset enabled, the unit still controls to the calibrated value, not the offset
value, for the internal or external probe. The display shows the calibrated value
with the offset value added.
- 26 -
Analog Port - Optional
(Digital Plus Only)
A I/O Analog Port
The 15-pin female receptacle located on the rear of the controller is used for
optional analog interface.
The analog signal is setup using the unit's Computer Setup Loop. With the
bath on, press and hold the Computer button for five seconds. The controller
will display SErL. If needed, press the arrow buttons to toggle between 232,
Pin # Function
1 Status relay NO. Status relay pins 1 and 3 close on start up, and open
8 765 43 2 1
2 Status relay NC. Status relay pins 2 and 3 open on start up, and close
on stop and all errors.
3 Status relay common
4-5 Not used
6 Analog Ground. The analog ground is physically separated from the
power ground throughout the unit. To prevent offsets that result from
ground currents, the analog and power grounds are only connected at
the unit's power supply. Analog ground should only be used as a
reference pin.
7 Temp out. The fluid temperature, as measured by the enabled sensor,
can be read at this pin. The temperature scale is 10mV/°C, referenced
to analog ground, pin 6 (example: +150mV = +15.0°C).
8 Not used
9 Digital output ground, reference for pin 14. Digital output ground should
only be used as a reference pin.
10-13 Not used
14 Digital output +5VDC at 15mA max. 70mA max inrush current. This
power supply energizes on start up and de-energizes on stop and all
errors.
15 Setpoint in. The temperature setpoint can be controlled by applying a
known voltage to this pin. The temperature scale is 10mV/°C, refer-
enced to analog ground, pin 6 (example: +230mV = +23.0°C).
- 27 -
High Temperature Cutout
(Digital One/Digital Plus)
Adjustable High Temperature Cutout
To protect your application, the adjustable High Temperature Cutout ensures
the heater will not exceed temperatures that can cause serious damage to
your unit. A single temperature sensor is located in the bath fluid. A High
Temperature fault occurs when the temperature of the sensor exceeds the set
temperature limit. The safety has a range of 0°C to 230±20°C.
In the event of a fault the unit will shut down and the controller will display HtC.
Installation and Operation
The cause of the fault must be identified and corrected before the unit can be
manually restarted.
The cutout is not preset and must be adjusted during initial installation. To set
the cutout, locate the small black adjustment dial on the rear of the controller.
Turn the dial fully clockwise and turn the power switch off then back on.
Start the unit. Adjust the setpoint for a few degrees higher than the highest
desired fluid temperature and allow the bath to stabilize at the temperature
setpoint. Turn the dial counterclockwise until you hear a click and the unit
shuts down.
Before you can restart the bath it has to cool down a few degrees. Then,
without moving the adjustment dial, turn the power switch off then back on.
If the bath is empty, the cutout has a typical trip point of 300°C. The heater
temperature can continue to rise after the cutout trips up to approximately
314°C.
There will be no indication the High Temperature Cutout activated other than an
audible click. The unit will continue to run but the heater will no longer operate.
Service will be required.
- 28 -
Accessories
(Digital One/Digital Plus)
Autorefill Accessory
The autorefill accessory attaches to the rear of the bath. The autorefill provides
makeup water to replace bath fluid lost to evaporation, etc. It will require a tap
water source. A reservoir level float switch and logic/signal are already installed
in the bath.
•Attach the autorefill module to the rear of the bath with the two 8-32 screws.
When tap water is available, the bath is turned on, and the fluid reaches the
lower 1 inch horizontal level indicator located in the reservoir the autorefill
begins filling the bath. The autorefill shuts off when the fluid reaches the upper
indicator, or if the bath is turned off.
Autorefill Control
Cable Attachment
Cap Tube
Autorefill Module
100-115V/50/60Hz 611012000001
200-240V/50/60Hz, No line cord 611028000001
- 29 -
Reservoir Overflow Device
The overflow device is designed to act as an automatic drain for the unit's
reservoir. The assembly is stainless steel with the exception of the drain fitting
which is Ryton®. The unit can still be drained as normal, but if the level reaches
the middle of the tee it will begin to overflow out the bent tube.
Installation and Operation
top.
•Reinstall the vertical tube assembly into the Swagelok® if it was removed.
•Install the drain fitting into the end of the new assembly - finger tight.
•Install the other supplied 4-40 x ¼"phillips head screw into the bottom of the
overflow assembly. (This prevents the drain fitting from falling off the unit.)
- 30 -
Stainless Steel Test Tube Racks
The following Stainless Steel test tube rack assemblies are available:
EX 7 49 13 126000000040
EX 7 25 18 126000000041
EX 10/17/35 42 18 126000000043
The EX 35's reservoir is 12" deep. The 6" shelf makes the bath effectively 6"
deep. The 3" shelf makes the bath effectively 9" deep. The shelves can also
be stacked making the reservoir effectively 3" deep.
The shelves are Stainless Steel and are simply positioned into the work area.
The shelves are fully perforated to allow circulation throughout the bath area.
The smaller shelf is designed to nest inside the larger one for storage.
- 31 -
The following accessories are also available from Thermo Fisher:
*Ground Fault Current Interrupter. An electrical safety device which opens a circuit upon
observation of electricity leaking to ground through an undefined path, most likely a human
being. GFCI receptacles are required by the NEC in many locations.
- 32 -
Accessories
(Digital Plus Only)
RPC Remote Box
An RPC can control the bath from a remote location. It mirrors the controller
displays; and has the ability to store and run up to 16 programs. It operates by
sending and receiving information by RS-485 serial communication. It attaches
to the unit by an RS-485 cable with 9-pin D subminature connectors.
The remote can be mounted to the wall with an included wall bracket, or it can
MENU
HEAT
COOL
120.0°C
SETPOINT
BATH ON
NOTE: Power the RPC with an AC Adapter that is UL Listed with the following
ratings:
- Class 2
- Input rated 100-240 VAC, 47-63 Hz, 0.4A
- Output rated 12VDC, 1.25A Max.
- 33 -
Blank Page.
- 34 -
Section IV Basic Maintenance
To avoid electrical shock, disconnect the mains cord prior to removing
any access panels or covers.
Service Contracts
Thermo Fisher Scientific offers on-site Service Contracts designed to provide
extended life and minimal down-time for your unit. For more information,
contact our Service Department (see Preface, After-sale Support).
Reservoir Fluid
Periodically inspect the reservoir fluid. If cleaning is necessary, flush the
reservoir with a cleaning fluid compatible with your application.
Reservoir Cleaning
Maintenance
Routine cleaning can be achieved by simply sponging down the seamless
stainless steel tank with tap water. (Dish washing detergent may be used but
the tank must be thoroughly rinsed.)
Algae
To restrict the growth of algae in the bath, we recommend that all circulation
lines be opaque. This will eliminate the entrance of light required for the growth
of most common algae.
- 35 -
Internal Temperature
Sensor (rdt1)
Calibration
Press and Hold
Should the bath fluid temperature display disagree with your calibrated refer-
ence thermometer, the internal temperature sensor (rtd1) may need calibration.
XX.X No
Do not pick calibration points that are outside the safe operating limits of the
fluid in your application. For example with water, 90°C and 5°C would be
Yes
typical calibration points.
No
Release NOTE: If it is more convenient, the low-end calibration can be performed before
doing the high-end.
No
CAL
Run the bath to a suitable high-
Yes
end calibration point. Place a
No
calibrated reference thermometer
rtd1 Yes
r1 H Yes r1 H Yes 200.0 in the bath. Ensure the fluid
No Yes
temperature is stabilized. Press
No
and hold the NO button and then
No
press the YES button three
times. Release the NO button.
r1 L r1 L -40.0
Maintenance
Press the SCROLL and NO buttons as shown until StorE is displayed, press
YES to accept the new value, press NO to abort it.
NOTE: Both the high and low temperatures must be entered for a valid calibra-
tion. If power is lost before the procedure is complete, critical data needed for
the calculation of calibration parameters will be lost. After pressing the YES
button at the StorE prompt wait several seconds before proceeding to ensure
that a bad calibration message does not appear. Premature use of the keypad
after pressing the YES button may cancel the bad calibration error message.
- 36 -
External Temperature
Sensor (rtd2)
Calibration
(Digital Plus Only)
When using any external sensor (rtd2) for the first time, Thermo Fisher recom-
mends a calibration. This calibration will only affect the temperature read by
the external sensor.
Do not pick calibration points that are outside the safe operating limits of the
fluid in your application. For example with water, 90°C and 5°C would be
typical calibration points.
Maintenance
r2 L Yes r2 L -40.0 Sensor button for five seconds. The
Yes
controller will display rtd2. Press YES
Yes
No and the controller will display r2 H.
Press YES and the display will
No
StorE
alternately flash r2 H and the current
probe temperature. Use the arrow
Yes Accept All Changes buttons to adjust the temperature to
match the reference thermometer.
Press the SCROLL and NO buttons until StorE is displayed, pressing YES
accepts the new value.
Repeat for the low-end temperature. Run the bath to a suitable low-end calibra-
tion point. At the r2 L display use the arrow buttons to adjust the temperature
to match a calibrated reference thermometer.
Pressing the SCROLL button after the low calibration will display StorE,
pressing YES accepts the new value.
If the SCROLL button is not pressed for 60 seconds the function will time-out
and the changes will not be saved. Pressing Mute will also exit the calibration
and return you to the reservoir fluid temperature display.
NOTE: Both the high and low temperatures must be entered for a valid calibra-
tion. If power is lost before the procedure is complete, critical data needed for
the calculation of calibration parameters will be lost. After pressing the YES
button at the StorE prompt wait several seconds before proceeding to ensure
that a bad calibration message does not appear. Premature use of the keypad
after pressing the YES button may cancel the bad calibration error message.
- 37 -
Optional Analog Port/
Calibration (Digital Plus Only)
Press and Hold
XX.X No The analog signal is setup using the unit's Computer Setup Loop. With the
bath on, press and hold the Computer button for five seconds. The controller
will display SErL. If needed, press the arrow buttons to toggle between 232,
Yes
485, and A In. With A In displayed, press the Computer button again until
StorE is displayed, press YES. The Computer button will flash when A in is
No enabled. Use the Computer button to enable/disable the analog signal.
Release
No
CAL The analog input and output are calibrated at the factory. If you need to
recalibrate follow the diagram until the display indicates A in.
Yes
Pressing YES at the A in display and the display will indicate A iH. Press
rtd1
YES and the display will alternate between A iH and some value. Apply 2.5V
No
to the analog input pin 15, see page 27 (analog ground is pin 6). Measure the
precise value with a voltmeter.
rdt3
No Change the value on the bath display to match the voltmeter reading.
Maintenance
At the StorE display press YES to save the calibration, press No to abort it.
- 38 -
Section V Troubleshooting
Error Codes
On Start Up:
ROM checksum. Check with Thermo Fisher
Operational Errors:
Asynchronous communication error, check serial interface
parameters
Troubleshooting
Faults require pressing I/0 to clear the error message and then pressing
I/0 again to start the unit after the cause of the error is identified and corrected.
- 39 -
Configuration error
Unit reaction to warning/fault errors depend on how the unit is configured, see
Setup/Tuning Loop on page 21. The unit is shipped configured to continue
running. If any other code appears contact Thermo Fisher customer service.
External Sensor
Connector
The unit is equipped with a male 9-pin D-connector located on the rear of the
control box. The connector is used with an optional external sensor.
123 4 5
67 8 9
Pin # Function
1 3-wire RTD connection A
2 No connection
3 No connection
4 3-wire RTD connection A
5 No connection
Troubleshooting
6 No connection.
7 3-wire RTD connection B
8 No connection
9 No connection
- 40 -
Checklist
Unit will not start
On Digital Plus controllers, check Serial Communication Mode on or off.
Check reservoir. Unit will not start if the reservoir fluid is below the lower slit.
Check the position of the circuit breaker on the rear of the unit.
Make sure the voltage of the power source meets the specified voltage,
±10%. Refer to the serial number label on the rear of the unit to identify the
specific electrical requirements of your unit.
No external circulation
Check for obstructions, kinks, or leaks in the circulation tubing.
Circulation will cease when the pump head has been exceeded.
Check controller PID values. See next page for factory preset values.
NOTE: Using high viscosity fluids at low temperatures may require PID adjust-
ment, contact Thermo Fisher.
Troubleshooting
Check optional external sensor connection. Perform calibration.
Condensation
A gasket is available for EX 7 units to install under the controller in order to
prevent any condensation from leaking into the unit.
Part Numbers:
Gasket, Baffle 084900
Clamp 036198
Instructions U00922
No serial communications
All units are tested for serial communications before they leave the factory.
Ensure the Computer indicator on the controller is on.
Check all communications settings and commands, they must be exact. See
Appendix B.
- 41 -
Service Assistance
If, after following these troubleshooting steps, your unit fails to operate
properly, contact our Service Department for assistance (see Preface, After-
sale Support). Before calling, please obtain the following information:
P I D
Heat 0.6 0.6 0.0
Thermo Fisher does not recommend changing the PID values. Incorrect PID
values will hamper unit performance.
BOM Decoder
The Bill of Material (BOM) number helps identify the configuration of your unit.
The number is printed on the label located on the rear of the unit.
Digit#
Troubleshooting
- 42 -
Displaying Software
Version Number
(Digital One/Digital Plus)
These values will be needed when calling Thermo Fisher Scientific for sales/
service information. The controller can display the installed software version
number. For example, for a unit with software version 082645.1A:
No
2. Press and hold for at least 10 seconds. The display will show the first
two digits, for example: 08 .
3. Press
The display will show the remaining digits to the left of the decimal, for
example: 2645.
4. Press
The display will show the decimal point and the digit to the right of the
decimal point, for example, 1 .
5. Press
The display will show the revision letter, as its equivalent number, for
example, 1 = A.
6. Press
Troubleshooting
The display will flash between Csu and the software checksum value.
7. Press
The display returns to the reservoir fluid temperature.
- 43 -
Blank Page.
- 42 -
Appendix A Fluids
Water Quality Standard and Recommendations
Permissible (PPM) Desirable (PPM)
Microbiologicals
(algae, bacteria, fungi) 0 0
Inorganic Chemicals
Calcium <25 <0.6
Chloride <25 <10
Magnesium <12 <0.1
Sulfate <25 <1
Total Hardness <17 <0.05
Unfavorably high total ionized solids (TIS) can accelerate the rate of galvanic
corrosion. These contaminants can function as electrolytes which increase the
potential for galvanic cell corrosion and lead to localized corrosion such as
pitting.
High water hardness (Calcium and Maganese) can also produce scaling. For
example, tap water in the U.S. averages 171 ppm (of NaCl). The recommended
level for use in a water system is between 0.5 to 5.0 ppm (of NaCl).
Recommendation: Initially fill the tank with distilled/deionized water. Do not use
untreated tap water as the total ionized solids level may be too high.
Maintain this water quality at a resistivity of between 1 to 10 MOhmcm (com-
pensated to 25°C) by using a purification system. Although the initial fill may
be as high as 18 MOhmcm (compensated to 25°C), the desired level for long
time usage is 1 to 3 MOhmcm (compensated to 25°C).
The above two recommendations will reduce the electrolytic potential of the
water and prevent or reduce the galvanic corrosion observed.
Appendix A
A-1
EX Compatibility with
Recommended Fluids
ered “safe” to use in the food industry. Propylene is less dense than ethylene and therefore will
have a tendency to weep more through mechanical seals.
NEVER use flammable or corrosive fluids with this unit. Do not use automotive anti-
freeze. Commercial antifreeze contains silicates that can damage the unit. Use of
automotive antifreeze may void the manufacturer’s warranty.
A-2
Appendix B NC Serial Communications Protocol
(Digital Plus Only) NOTE: This appendix assumes you have a basic understanding of serial
communications protocols.
All data is sent and received in binary form, do not use ASCII. In the following
pages the binary data is represented in hexadecimal (hex) format.
NOTE: Before the unit will communicate, serial communication must be turned
on using the controller's Computer button.
The unit can be controlled through your computer’s serial port by using the
unit's standard female 9-pin connection.
RS-232 RS-485
1 No Connection 1-7 No connection
2 TX 8 T+
9-pin female
3 RX 9 T-
4 No Connection
5 Signal Ground
6-9 No Connection
All commands must be entered in the exact format shown in the tables on the
following pages. The tables on the last page of this Appendix show all com-
mands available, their format and responses. Controller responses are either
the requested data or an error message. The controller response must be
received before the host sends the next command.
then waits for the controller’s response. If the command is not understood or
the checksums do not agree, the controller responds with an error command.
Otherwise, the controller responds with the requested data. If the controller
fails to respond within 1 second, the host should re-send the command.
During RS-485 operation the bath will wait at least 5 milliseconds after receiv-
ing the checksum byte before asserting its transmitter for the purpose of
replying to the host. Therefore, when the host is done sending a command, it
must disable its transmitter in less than 5 milliseconds. When the bath is done
sending its reply, it will disable its transmitter in less than 5 milliseconds.
B-1
NC Serial Communications Protocol
NOTE: All byte values are shown in hex, hex represents the binary values that must be sent to the bath. Do not
use ASCII.
Checksum region
Lead char Addr-MSB Addr-LSB Command n d-bytes d-byte 1 ... d-byte n Checksum
CA or CC 00
The master requests information by sending one of the Read Functions as shown in Table 1 on page B-4. Since
no data is sent to the bath during a read request, the master uses 00 for the number of data bytes following the
command byte.
The bath will respond to a Read Function by echoing the lead character, address, and command byte, followed
by the requested data and checksum. When the bath sends data, a qualifier byte is sent first, followed by a two
byte signed integer (16 bit, MSB sent first). The qualifier byte indicates the precision and units of measure for
the requested data as detailed in Table 2.
0 bytes of data
If the temperature is 62.5°C, the bath would reply: The qualifier byte of 11 indicates a precision of 1
decimal point and units of °C. The temperature of
62.5°C is 625 decimal = 271 hex.
command byte
CA 00 01 20 03 11 02 71 57
The checksum is the bitwise inversion of A8
3 bytes to follow (00+01+20+03+11+02+71) = A8
A8 ^ FF = 57
^ = Bitwise XOR function
B-2
The master sets parameters in the bath by sending one of the Set Functions as shown in Table 1. The master
does not send a qualifier byte in the data field. The master should be pre-programmed to send the correct
precision and units (it could also read the parameter of interest first to decode the correct precision and units
needed).
As an RS-485 example, if the master wants to set the setpoint to 30°C, it would send :
The checksum is the bitwise inversion of 22
command byte (00+03+F0+02+01+2C) = 122
Take the LSB = 22
CC 00 03 F0 02 01 2C DD
2 bytes to follow The temperature of 30.0°C is 300 decimal = 012C hex.
CC 00 03 F0 03 11 01 2C CB
The checksum is the bitwise inversion of 34
3 bytes to follow (00+03+F0+03+11+01+2C) = 134
Take the LSB = 34
Appendix B
B-3
Table 1 (All bytes are in hex)
SET
Set Setpoint (control point)** CA 00 01 F0 02(d1)(d2)(cs) CA 00 01 F0 03(qb)(d1)(d2)(cs)
Set Low Temperature Limit** CA 00 01 C0 02(d1)(d2)(cs) CA 00 01 C0 03(qb)(d1)(d2)(cs)
Set High Temperature Limit** CA 00 01 E0 02(d1)(d2)(cs) CA 00 01 E0 03(qb)(d1)(d2)(cs)
Set Heat Proportional Band CA 00 01 F1 02(d1)(d2)(cs) CA 00 01 F1 03(qb)(d1)(d2)(cs)
(P = 0.1-99.9)
Set Heat Integral (I = 0-9.99) CA 00 01 F2 02(d1)(d2)(cs) CA 00 01 F2 03(qb)(d1)(d2)(cs)
Set Heat Derivative (D = 0-5.0) CA 00 01 F3 02(d1)(d2)(cs) CA 00 01 F3 03(qb)(d1)(d2)(cs)
B-4
Table 2 Read Status
BIT d1 d2 d3
b.7 = 1 RTD1 Open Fault RTD2 Open Fault High Fixed Temp Fault
b.6 = 1 RTD1 Shorted Fault RTD2 Shorted Fault Low Fixed Temp Fault
b.5 = 1 RTD1 Open RTD2 Open Warn High Temp Fault
b.4 = 1 RTD1 Shorted RTD2 Shorted Warn Low Temp Fault
b.3 = 1 0 RTD2 Open Low Level Fault
b.2 = 1 0 RTD2 Shorted High Temp Warn
b.1 = 1 0 RTD2 Controlling Low Temp Warn
b.0 = 1 0 HTC Fault Low Level Warn
BIT d4 d5
b.7 = 1 Buzzer On RTD2 Controlling
b.6 = 1 Alarm Muted Heat LED Flashing**
b.5 = 1 Unit Faulted Heat LED On
b.4 = 1 Unit Stopping 0
b.3 = 1 Unit On 0
b.2 = 1 Pump On 0
b.1 = 1 0 0
b.0 = 1 Heater On 0
Example: The temperature of 45.6°C would be represented by the qualifier 11 hex, followed by the 2 bytes 01 C8
hex (456 decimal).
Appendix B
B-5
Appendix C International Quick Reference Operating Procedures
C-1
WARRANTY
Thermo Fisher Scientific warrants for 24 months from date of shipment the Thermo Scientific NESLAB EX unit
according to the following terms.
Any part of the unit manufactured or supplied by Thermo Fisher Scientific and found in the reasonable judgment
of Thermo Fisher to be defective in material or workmanship will be repaired at an authorized Thermo Fisher
Repair Depot without charge for parts or labor. The unit, including any defective part must be returned to an
authorized Thermo Fisher Repair Depot within the warranty period. The expense of returning the unit to the
authorized Thermo Fisher Repair Depot for warranty service will be paid for by the buyer. Our responsibility in
respect to warranty claims is limited to performing the required repairs or replacements, and no claim of breach
of warranty shall be cause for cancellation or recision of the contract of sales of any unit. With respect to units
that qualify for field service repairs, Thermo Fisher Scientific’s responsibility is limited to the component parts
necessary for the repair and the labor that is required on site to perform the repair. Any travel labor or mileage
charges are the financial responsibility of the buyer.
The buyer shall be responsible for any evaluation or warranty service call (including labor charges) if no defects
are found with the Thermo Scientific product.
This warranty does not cover any unit that has been subject to misuse, neglect, or accident. This warranty does
not apply to any damage to the unit that is the result of improper installation or maintenance, or to any unit that
has been operated or maintained in any way contrary to the operating or maintenance instructions specified in
this Instruction and Operation Manual. This warranty does not cover any unit that has been altered or modified
so as to change its intended use.
In addition, this warranty does not extend to repairs made by the use of parts, accessories, or fluids which are
either incompatible with the unit or adversely affect its operation, performance, or durability.
Thermo Fisher Scientific reserves the right to change or improve the design of any unit without assuming any
obligation to modify any unit previously manufactured.
OUR OBLIGATION UNDER THIS WARRANTY IS STRICTLY AND EXCLUSIVELY LIMITED TO THE REPAIR OR
REPLACEMENT OF DEFECTIVE COMPONENT PARTS AND Thermo Fisher Scientific DOES NOT ASSUME
OR AUTHORIZE ANYONE TO ASSUME FOR IT ANY OTHER OBLIGATION.
This warranty applies to units sold in the United States. Any units sold elsewhere are warranted by the affiliated
marketing company of Thermo Fisher Scientific. This warranty and all matters arising pursuant to it shall be
governed by the law of the State of New Hampshire, United States. All legal actions brought in relation hereto shall
be filed in the appropriate state or federal courts in New Hampshire, unless waived by Thermo Fisher Scientific.