M ETHO D FINDER (Ke y on p a g e M F!

34]

M eth Flow Ra te Vol. (L) E x tr a c ti o n A n a ly t ic a l

Chemical No. M e th od Na m e ( L /m i n ) T e c h n iq u e Sampler
min max

Acenaphthene 5506 PO LYN UC LEA R A RO M ATIC 2.0 200 - 1000 ac eto nitr ile HPLC !FL/U V P T F E & X A D !2
HYDR OC ARBO NS by H PLC

Acenaphthene 5515 PO LYN UC LEA R A RO M ATIC 2.0 200 - 1000 va r ies G C !FID P T F E & X A D !2
HYDROCARBONS

Acenaphthylene 5506 PO LYN UC LEA R A RO M ATIC 2.0 200 - 1000 ac eto nitr ile HPLC !FL/U V P T F E & X A D !2
HYDR OC ARBO NS by H PLC

Acenaphthylene 5515 PO LYN UC LEA R A RO M ATIC 2.0 200 ! 1000 va r ies G C !FID P T F E & X A D !2
HYDROCARBONS

A c e talde hyde 2018 ALIPHATIC ALDEHYDES 0.1 - 1.5 1 - 15 ACN HP LC /UV SG-DNPH

A c e talde hyde 2538 A C E T AL D E HY D E 0.01 - 0.05 1 ! 12 t ol G C !F ID X A D !2 /H M P

A c e talde hyde 2539 A L D EH Y D E S, SC R E E N IN G 0.01 - 0.05 5-5 t ol G C !F ID /M S X AD -2 /H M P

A c e talde hyde 3507 A C E T AL D E HY D E 0.1 - 0.5 6 - 60 r ea g HPLC !U V BuB

Ac etic ac id 1603 AC ETIC AC ID 0.01 - 0.1 20 - 300 formic a G C !FID CCT

A c e tic anhydride 3506 A C E T IC A N H Y D R ID E 0.2 - 1.0 25 - 100 r ea g VIS BuB

Ac eto in 2558 AC ETO IN 0.01 - 0.2 1 - 10 Ac et-M eth G C -FID A -C M S

Acetone 1300 KETONES I 0.01 - 0.2 0.5 - 3 C S2 G C !FID CCT

Acetone 2549 V O L A TI LE O R G A N IC C P D S 0.01 - 0.05 1-6 t h erma l TD /G C !M S TD

(Screen in g)

Acetone 3800 ORG ANIC AND INORGAN IC GASES 0.1 - 2.0 Inst r. D ep . NA FTIR Di r. R e a d
BY EXTR ACTIV E FTIR SPEC T R O MET R Y

Acetone 2555 KETONES I 0.01 - 0.2 0.5 - 3.0 C S2 G C -FID A -C M S

Ac eto ne cy an oh yd rin 2506 AC ETO NE CY AN O HY DR IN 0.2 0.3 - 12 Et Ac G C !NPD P or Q S

Ac eto nitr ile 1606 AC ETON ITRILE 0.01 - 0.2 1 - 25 M e C l/M e O H G C !FID CCT

A c e tyle ne dic hlor ide 1003 H Y D R O C A R B O N S , H A L O G E N A TE D 0.01 - 0.2 0.2 - 5 C S2 G C !FID CCT

A c e tyle ne te trabr o m ide 2003 1,1,2,2 !T E TR A B R O M O E T H AN E 0.2 - 1.0 50 - 100 T HF G C !FID SG

A c e tyle ne te trac hlo r ide 1019 1,1,2,2 !T E TR A C H L O R O E TH A N E 0.01 - 0.2 3.0 - 30 C S2 G C !FID PCT
- 2-
Ac ids , ino rg an ic 7903 AC IDS , INO RG AN IC 0.2 - 0.5 3.0 - 100 H C O 3 /C O 3 IC SG(washed)

ACN 1606 AC ETON ITRILE 0.01 - 0.2 1 - 25 M e C l/M e O H G C !FID C C T lg

Ac ro lein 2501 AC RO LEIN 0.01 - 0.1 1.5 - 48 t ol G C !NPD X A D !2 /H M P

Ac ro lein 2539 A L D EH Y D E S, SC R E E N IN G 0.01 - 0.05 5-5 t ol G C !F ID /M S X A D !2 /H M P

Ac rylo nitr ile 1604 AC RYLO NITRILE 0.01 - 0.2 3.5 - 20 a c et/C S 2 G C !FID CCT

Ae ro bic ba cte ria 0801 A ER O BIC B AC TE RIA by G C -F AM E 28.3 50 - 300 hex/MTBE G C -FID i m p a c to r

Alach lor 5603 ALA C HLO R in AIR 1 70 - 1750 met h a nol ELISA SPE disk

A l ac hlo r 5602 CHLORINATED ORG ANONITROGEN 0.2 - 1 12 - 480 reagent G C /E C D OV S-2

H ER BIC ID ES (A IR SA M PL IN G )

A l ac hlo r 9200 CHLORINATED ORG ANONITROGEN NA NA NA G C - EC D polyethylene

HER BICIDES (HAND WAS H) bag

A lac hlo r 9201 CHLORINATED ORG ANONITROGEN NA NA IPA/diazomethane G C - EC D PUF pad

HE RBIC IDES (DER M AL P ATC H))

Aldehydes, screening 2539 A L D EH Y D E S, SC R E E N IN G 0.01 - 0.05 5-5 t ol G C !F ID /M S X A D !2

Aldicarb 5601 ORG ANONITROGEN PESTICIDES 0.1 - 1 var-480 reagent HP LC - U V OV S-2

Ald rin 5502 A L D R IN & L IN D A N E 0.2 - 1.0 18 - 240 isooct G C !E C N GFF & BuB

Alka line du sts 7401 ALKA LINE DU STS 1-4 70 - 1000 HCl T it ra t ion PTFE

A llyl alc oho l 1402 ALC O HO LS III 0.01 - 0.2 1 - 10 IP A/C S 2 G C !FID CCT

A llyl alc oho l 1405 ALCOHO LS COM BINED 0.01 - 0.2 2 - 10 IP A -C S 2 G C -FID CCT

A llyl c hlor ide 1000 A L LY L C H LO R I D E 0.01 - 1.0 16 - 100 bz G C !FID CCT

3/15/2003 MF!1 NIOSH Manual of Analytical Methods

 M eth Flow Ra te Vol. (L) E x tr a c ti o n A n a ly t ic a l
Chemical No. M e th od Na m e ( L /m i n ) T e c h n iq u e Sampler
min max

Al lyl glyc idyl ethe r 2545 ALLYL GLYCIDYL ETHER 0.01 - 0.2 1.5 - 8 d ieth y l et h er G C !FID Tenax

A l lyl tric hlo r ide 1003 HYDROC ARBONS, HALOG ENATED 0.01 - 0.2 2 - 60 CS2 G C !FID CCT

Alumina 0500 PARTICU LATES N.O.R . 1-2 7 - 133 ! Grav P VC , ta re d

A l um inum 7300 E LE M E NT S b y IC P 1-4 5 - 100 H N O 3/HC lO 4 IC P !AES MC EF

A l um inum 7303 E LE M EN TS by IC P (H O T 1-4 Se e Ta ble H C l /H N O 3 ICP-AES MC EF

B L O C K /H C l /H N O 3 D IG E S T IO N )

A l um inum 7301 ELE M EN TS b y IC P (A Q UA RE G IA 1-4 5 - 100 H C l /H N O 3 ICP-AES MC EF

A SH IN G )

A l um inum 7013 ALUMINUM & CPDS, as Al 1-3 10 - 400 HNO3 FAAS MC EF

Am ine s, a liph atic 2010 AM INE S, A LIPH ATIC 0.01 - 1.0 3 - 30 H 2SO 4/a q M e O H G C !FID SG

Am ine s, a ro m atic 2002 AM INE S, A RO M ATIC 0.2 - 1.0 30 - 150 Et h a nol G C !FID SG

Aminobenzene 2002 AM INE S, A RO M ATIC 0.2 - 1.0 30 - 150 Et h a nol G C !FID SG

Aminobenzene 2017 A N IL IN E , o - TO L U ID I NE , A N D 0.2 5 - 50 Et h a nol G C -FID GFF + SG

N I TR O B E N Z EN E

2 !A m ino e thano l 2007 AMINOETHANO L COM POUNDS I 0.01 - 0.2 4 - 24 M eO H/H 2O G C !FID SG

2 !A m ino e thano l 3509 AM INO ETH AN O L C O M PO UN DS II 0.5 - 1.0 5 - 300 HSA IC IM P

2-aminotoluene 2017 A N IL IN E , o - TO L U ID I NE , A N D 0.2 5 - 50 et h a nol G C -FID GFF + SG

N I TR O B E N Z EN E

p !Am ino ph en yla rso nic ac id 5022 A R S E N IC , O R G A N O ! 1-3 50 - 1000 b u ffer IC !HYAAS PTFE

2 !Aminotoluene 2002 AM INE S, A RO M ATIC 0.02 - 1.0 10 - 150 Et h a nol G C !FID SG

Am m on ia 6015 AM M O NIA by VIS 0.1 - 0.2 0.1 - 90 H 2O VIS !Au to S G + H 2SO 4

Am m on ia 6016 AM M O NIA by IC 0.1 - 0.5 0.1 - 96 H 2O IC S G + H 2SO 4

n ! and s e c !Am yl ac etate 1450 ESTERS I 0.01 - 0.2 1 - 10 C S2 G C !FID CCT

n-Am yl ac etate 1450 ESTERS I 0.01 - 2 1 - 10 C S2 G C -FID CCT

Am yl ac etate 2549 V O L A TI LE O R G A N IC C P D S 0.01 - 0.05 1-6 t h erma l TD /G C !M S TD

(Screen in g)

iso-A my lace tate 1450 ESTERS I 0.01 - 2 1 - 10 C S2 G C -FID CCT

Aniline 2002 AM INE S, A RO M ATIC 0.02 - 0.2 5 - 30 Et h a nol G C !FID SG

Aniline 2017 ANILINE , O -TOLU IDINE, & 0.2 5 - 50 et h a nol G C -FID GFF+SG
N I TR O B E N Z EN E

Aniline 8317 ANALINE an d @ -TOLUIDINE in urine NA NA Alk H P LC /E C D NA

Anisidine 2514 A N IS ID I NE 0.5 - 1.0 24 - 320 MeOH HPLC !U V X A D !2

Anthracene 5506 PO LYN UC LEA R A RO M ATIC 2.0 200 - 1000 ac eto nitr ile HPLC !FL/U V P T F E & X A D !2
HYDR OC ARBO NS by H PLC

Anthracene 5515 PO LYN UC LEA R A RO M ATIC 2.0 200 - 1000 va r ies G C !FID P T F E & X A D !2
HYDROCARBONS

Antimony 7303 E LE M EN TS by IC P (H O T 1-4 Se e Ta ble H C l /H N O 3 ICP-AES MC EF

B L O C K /H C l /H N O 3 D IG E S T IO N )

Antimony 7301 ELE M EN TS b y IC P (A Q UA RE G IA 1-4 50 - 2000 H C l /H N O 3 ICP-AES MC EF

A SH IN G )

p !Ar sa nilic ac id 5022 ARSENIC, organo! 1-3 50 - 1000 b u ffer IC !HYAAS PTFE

Ar se nic 7900 AR SENIC & compoun ds , a s As 1-3 30 - 1000 H N O 3/H 2SO 4/HC lO 4 HYAAS MC EF

Ar se nic 7300 E LE M E NT S b y IC P 1-4 5 - 2000 H N O 3/HC lO 4 IC P !AES MC EF

Ar se nic 9102 ELEMENTS on WIPES NA NA NA ICP-AES Wipe

Ar se nic 7303 E LE M EN TS by IC P (H O T 1-4 Se e Ta ble H C l /H N O 3 ICP-AES MC EF

B L O C K /H C l /H N O 3 D IG E S T IO N )

Ar se nic 7301 ELE M EN TS b y IC P (A Q UA RE G IA 1-4 5 - 2000 H C l /H N O 3 ICP-AES MC EF

A SH IN G )

A r senic trio xide 7901 AR SENIC TR IOX IDE, as A s 1-3 30 - 1000 H N O 3/H 2O 2 G FAAS MC EF

3/15/2003 MF!2 NIOSH Manual of Analytical Methods

 M eth Flow Ra te Vol. (L) E x tr a c ti o n A n a ly t ic a l
Chemical No. M e th od Na m e ( L /m i n ) T e c h n iq u e Sampler
min max

Arsine 6001 A R S IN E 0.01 - 0.2 0.1 - 10 HNO3 G FAAS CCT

A sbe sto s 7400 A S BE ST O S F IB ER S b y PC M 0.5 - 16 400 - va r NA PCM MCEF open

A sbe sto s 7402 ASBESTOS FIBERS by TEM 0.5 - 16 400 - va r NA TEM MCEF open

A sbe sto s 9000 ASBESTOS, CHRYSOTILE b y XR D NA NA NA XR D bu lk

A sbe sto s 9002 ASBES TOS (bulk) by PLM NA NA NA PLM bu lk

A sp arta m e 5031 A SP AR TA M E 1-3 70 - 1200 eluent HPLC !U V PTFE

A sp ha lt fu m e 5042 B E N Z EN E S O LU B LE F R AC T IO N A N D 1-4 28 - 400 benzene G RA VIM ETR IC Tared PTFE

TOTAL PARTICULATE (ASPHALT FUME)

Atrazine 5602 CHLORINATED ORG ANONITROGEN 0.2 - 1 12 - 480 reagent G C /E C D OV S-2

H ER BIC ID ES (A IR SA M PL IN G )

Atrazine 8315 TR IAZ INE HE RB IC IDE S a nd the ir NA NA NA GC-M SD Urine

METABOLITES

Atrazine 9200 CHLORINATED ORG ANONITROGEN NA NA NA G C - EC D polyethylene

HER BICIDES (HAND WAS H) bag

Atrazine 9201 CHLORINATED ORG ANONITROGEN NA NA IP A/ G C - EC D PUF pad

HE RBIC IDES (DER M AL P ATC H)) diazomethane

Az ela ic a cid 5019 AZ ELA IC A C ID 1-3 200 - 1000 Et h a nol G C !FID P VC

Azinphos methyl 5600 ORG ANOPHO SPHORUS PESTICIDES 0.2 - 1.0 12 - 240 t ol/a cet G C !FPD O VS !2

Ba cte ria 0801 A ER O BIC B AC TE RIA by G C -F AM E 28.3 50 - 300 hex/MTBE G C -FID i m p a c to r

B[a]P 5506 PO LYN UC LEA R A RO M ATIC 2.0 200 - 1000 ac eto nitr ile HPLC !FL/U V P T F E & X A D !2
HYDR OC ARBO NS by H PLC

B[a]P 5515 PO LYN UC LEA R A RO M ATIC 2.0 200 - 1000 va r ies G C !FID P T F E & X A D !2
HYDROCARBONS

Bar ium 7056 B A R IU M , S O LU B LE C O M P O U N D S 1-4 50 - 2000 H 2O FAAS MC EF

Bar ium 9102 ELEMENTS on WIPES NA NA NA ICP-AES Wipe

Bar ium 7303 E LE M EN TS by IC P (H O T 1-4 Se e Ta ble H C l /H N O 3 ICP-AES MC EF

B L O C K /H C l /H N O 3 D IG E S T IO N )

Bar ium 7301 ELE M EN TS b y IC P (A Q UA RE G IA 1-4 50 - 2000 H C l /H N O 3 ICP-AES MC EF

A SH IN G )

Benomyl 5601 ORG ANONITROGEN PESTICIDES 0.1 - 1 var - 480 reagent HP LC - U V OV S-2

Be nzalde hyde 2549 V O L A TI LE O R G A N IC C P D S 0.01 - 0.05 1-6 t h erma l TD /G C !M S TD

(Screen in g)

Benz[a]anthracene 5506 PO LYN UC LEA R A RO M ATIC 2.0 200 - 1000 ac eto nitr ile HPLC !FL/U V P T F E & X A D !2
HYDR OC ARBO NS by H PLC

Benz(a)anthracene 5515 PO LYN UC LEA R A RO M ATIC 2.0 200 - 1000 va r ies G C !FID P T F E & X A D !2
HYDROCARBONS

Benzene 2549 V O L A TI LE O R G A N IC C P D S 0.01 - 0.05 1-6 t h erma l TD /G C !M S TD

(Screen in g)

Benzene 3700 B EN ZE NE by po rta ble G C > 0.02 80% vol NA GC air bag

Benzene 1501 HY DR O C AR BO NS , AR O M ATIC 0.01 - 0.2 5 - 30 C S2 G C !FID CCT

Benzene 1500 HYDROC ARBONS, BP 36 !216 °C 0.01 - 0.2 2 - 30 C S2 G C !FID CCT

Benzene 3800 ORG ANIC and INORGANIC G ASES 0.1 - 2.0 Inst r. D ep . NA FTIR Di r. R e a d
by EX TR ACTIV E FTIR SPE C T R O MET R Y

Be nzene so lubles 5042 B E N Z EN E S O LU B LE F R AC T IO N A N D 1-4 28 benzene Grav Tared PTFE

TOTAL PARTICULATE (ASPHALT FUME)

1, 3-be nze ne diol 5701 R ES O RC IN O L 0.2 - 1 5 - 160 met h a nol G C -FID OV S-7

Be nzidine D ye s 5013 DYES 1-3 150 - 500 H 2O HPLC !U V PTFE

Benzidine 5509 BENZIDINE and 0.2 20 - 100 triethyl amine HPLC !U V GFF
3,3'!DICHLORO !B E N Z ID I NE /M e O H

Benzo[a]pyrene 5506 PO LYN UC LEA R A RO M ATIC 2.0 200 - 1000 ac eto nitr ile HPLC !FL/U V P T F E & X A D !2
HYDR OC ARBO NS by H PLC

Benzo(a)pyrene 5515 PO LYN UC LEA R A RO M ATIC 2.0 200 - 1000 va r ies G C !FID P T F E & X A D !2
HYDROCARBONS

3/15/2003 MF!3 NIOSH Manual of Analytical Methods

 M eth Flow Ra te Vol. (L) E x tr a c ti o n A n a ly t ic a l
Chemical No. M e th od Na m e ( L /m i n ) T e c h n iq u e Sampler
min max

Benzo[a]fluoranthene 5506 PO LYN UC LEA R A RO M ATIC 2.0 200 - 1000 ac eto nitr ile HPLC !FL/U V P T F E & X A D !2
HYDR OC ARBO NS by H PLC

Benzo(b)fluoranthene 5515 PO LYN UC LEA R A RO M ATIC 2.0 200 - 1000 va r ies G C !FID P T F E & X A D !2
HYDROCARBONS

Benzo[e]pyrene 5506 PO LYN UC LEA R A RO M ATIC 2.0 200 - 1000 ac eto nitr ile HPLC !FL/U V P T F E & X A D !2
HYDR OC ARBO NS by H PLC

Benzo(e)pyrene 5515 PO LYN UC LEA R A RO M ATIC 2.0 200 - 1000 va r ies G C !ID P T F E & X A D !2
HYDROCARBONS

Benzo[k]fluoranthene 5506 PO LYN UC LEA R A RO M ATIC 2.0 200 - 1000 ac eto nitr ile HPLC !FL/U V P T F E & X A D !2
HYDR OC ARBO NS by H PLC

Benzo(k)fluoranthene 5515 PO LYN UC LEA R A RO M ATIC 2.0 200 - 1000 va r ies G C !ID P T F E & X A D !2
HYDROCARBONS

Benzo[ghi]perylene 5506 PO LYN UC LEA R A RO M ATIC 2.0 200 - 1000 ac eto nitr ile HPLC !FL/U V P T F E & X A D !2
HYDR OC ARBO NS by H PLC

Benzo(ghi)perylene 5515 PO LYN UC LEA R A RO M ATIC 2.0 200 - 1000 va r ies G C !ID P T F E & X A D !2
HYDROCARBONS

Be nzo su lfon az ole 2550 B EN ZO TH IA ZO LE IN AS PH A LT F UM E 1.0 - 2.0 480 - 960 hexane G C - SC D PTFE + X D-2

Be nzo thia zo le 2550 B EN ZO TH IA ZO LE IN AS PH A LT F UM E 1.0 - 2.0 480 - 960 hexane G C - SC D PTFE + X D-2

Be nzoyl pe r o xide 5009 B E N Z O Y L P E R O X ID E 1-3 40 - 400 d ieth y l et h er HPLC !U V MC EF

Be nzyl c hlo ride 1003 HYDROC ARBONS, HALOG ENATED 0.01 - 0.2 6 - 50 C S2 G C !FID CCT

Be r yllium 7300 E LE M E NT S b y IC P 1- 4 1250-2000 H N O 3/HC lO 4 IC P !AES MC EF

Be r yllium 9102 ELEMENTS on WIPES NA NA NA ICP-AES Wipe

Be r yllium 7303 E LE M EN TS by IC P (H O T 1-4 Se e Ta ble H C l /H N O 3 ICP-AES MC EF

B L O C K /H C l /H N O 3 D IG E S T IO N )

Be r yllium 7301 ELE M EN TS b y IC P (A Q UA RE G IA 1-4 1250-2000 H C l /H N O 3 ICP-AES MC EF

A SH IN G )

Be r yllium & c o m po und s 7102 BERYLLIUM and cpds, as Be 1-4 25 - 2000 H N O 3/H 2SO 4 G FAAS MC EF

Bio ae r o so l 0800 BIOA ERO SO L SAM PLING (Indoor A ir) 28.3 va r ies NA va r ies I m p a c to r

Biphenyl 2530 DIPHENYL 0.01 - 0.5 15 - 30 C C l4 G C !FID Te na x G C

Bism uth 7303 E LE M EN TS by IC P (H O T 1-4 Se e Ta ble H C l /H N O 3 ICP-AES MC EF

B L O C K /H C l /H N O 3 D IG E S T IO N )

B itu m en fu m e 5042 B E N Z EN E S O LU B LE F R AC T IO N A N D 1-4 28 - 400 benzene Grav Tared PTFE

TOTAL PARTICULATE (ASPHALT FUME)

Bo r o n 7303 E LE M EN TS by IC P (H O T 1-4 Se e Ta ble H C l /H N O 3 ICP-AES MC EF

B L O C K /H C l /H N O 3 D IG E S T IO N )

Bo r o n c ar bide 7506 B O R O N C A R B ID E 1.7 or 2 .2 100 - 1000 ash XR D C Y C & P VC

Bo r o n o xide 0500 PARTICU LATES N.O.R . 1.5 - 2.0 25 - 133 NA Grav P VC

Brom oform 1003 HYDROC ARBONS, HALOG ENATED 0.01 - 0.2 4 - 70 C S2 G C -FID CCT

Bromine 6011 C H L O R IN E a n d B R O M I N E 0.3 - 1.0 8 - 360 N a 2S 2O 3 IC Ag F

1-Bromopropane 1025 1 - a n d 2 -B R O M O P R O P A N E 0.01 - 0.2 0.1 - 12 C S2 G C -FID CCT

2-Bromopropane

Brom oform 1003 HYDROC ARBONS, HALOG ENATED 0.01 - 0.2 4 - 70 C S2 G C !FID CCT

Bromotrifluoromethane 1017 T R IF L UO R O B R O M O M E T HA N E 0.01 - 0.05 0.3 - 1.0 C H 2C l2 G C !FID 2 C C T (lg + sm )

Bro m ox yn il 5010 BRO MO XYN IL and B 'OC TANO ATE 1-3 2 - 400 C H 3C N HPLC !U V PTFE

Brom oxy nil octa noa te 5010 BRO MO XYN IL and B 'OC TANO ATE 1-3 90 - 400 C H 3C N HPLC !U V PTFE

1,3 !Butadiene 1024 1,3 !B U TA D IE N E 0.01 - 0.5 5 - 25 C H 2C l2 G C !FID CCT

2 !Butanone 2500 M E T H YL E TH Y L K E TO N E 0.01 - 0.2 1 - 12 C S2 G C !FID C a rb o n b e a d s

2 !Butanone 2549 V O L A TI LE O R G A N IC C P D S 0.01 - 0.05 1-6 t h erma l TD /G C !M S TD

(Screen in g)

2-Butanone 3800 ORG ANIC and INORGANIC G ASES 0.1 - 2.0 Inst r. D ep . NA FTIR Di r. R e a d
by EX TR ACTIV E FTIR SPE C T R O MET R Y

3/15/2003 MF!4 NIOSH Manual of Analytical Methods

 M eth Flow Ra te Vol. (L) E x tr a c ti o n A n a ly t ic a l
Chemical No. M e th od Na m e ( L /m i n ) T e c h n iq u e Sampler
min max

Bu tox ya ce tic a cid 8316 BUTOXYACETIC ACID in urine NA NA NA G C - EC D NA

2 !Buto xye thyano l 2549 V O L A TI LE O R G A N IC C P D S 0.01 - 0.05 1-6 t h erma l TD /G C !M S TD

(Screen in g)

2 !Buto xye thano l 1403 ALC O HO LS IV 0.01 - 0.05 2 - 10 C H 2C l2/M e O H G C !FID CCT

n !, s ec !, & t!Buty l ace tate 1450 ESTERS I 0.01 - 0.2 1 - 10 C S2 G C !FID CCT

Buty l ace tate 2549 V O L A TI LE O R G A N IC C P D S 0.01 - 0.05 1-6 t h erma l TD /G C !M S TD

(Screen in g)

iso-Bu tyl ac etate 1450 ESTERS I 0.01 - 2 1 - 10 C S2 G C -FID CCT

1-Bu tyl ac etate 1450 ESTERS I 0.01 - 2 1 - 10 C S2 G C -FID CCT

Butyl alc o ho l 2549 V O L A TI LE O R G A N IC C P D S 0.01 - 0.05 1-6 t h erma l TD /G C !M S TD

(Screen in g)

tert !Butyl alc o ho l 1400 ALCOHO LS I 0.01 - 0.2 1 - 10 C S2 G C !FID CCT

n ! & s e c !Butyl alc o hol 1401 ALC O HO LS II 0.01 - 0.2 2 - 10 C S2 G C !FID CCT

n- Butyl alc oho l 1405 ALCOHO LS COM BINED 0.01 - 0.2 2 - 10 IP A -C S 2 G C -FID CCT

se c -Butyl alc o ho l 1405 ALCOHO LS COM BINED 0.01 - 0.2 2 - 10 IP A -C S 2 G C -FID CCT

n !Butylamine 2012 n !B U TY L AM I N E 0.01 - 1.0 2 - 100 MeOH G C !FID S G + H 2SO 4

Butyl cellosolve 2549 V O L A TI LE O R G A N IC C P D S 0.01 - 0.05 1-6 t h erma l TD /G C !M S TD

(Screen in g)

Butyl cellosolve 1403 ALC O HO LS IV 0.01 - 0.05 1 - 10 C H 2C l2/M e O H G C !FID CCT

1,3 !Butyle ne glygo l 5523 GLYC OLS 0.5 - 2 5 - 60 MeOH G C !FID O VS !7

Butyl glyc idyl e the r 1616 BUTYL GLYCIDYL ETHER 0.01 - 0.2 15 - 30 C S2 G C !FID CCT

n !Butyl me rc aptan 2525 n !BU TYL MER CAPTAN 0.01 - 0.05 1-4 a cet G C !FPD Chrom 104

n !Butyl me rc aptan 2542 M E R C A P TA N S 0.1 - 0.2 10 - 150 H C l/D C E G C !FPD GFF/HgAc

p !tert !Butyltoluene 1501 HY DR O C AR BO NS , AR O M ATIC 0.01 - 0.2 1 - 29 C S2 G C !FID CCT

Butyr alde hyde 2539 A L D EH Y D E S, SC R E E N IN G 0.05 5-5 t ol G C !F ID /M S X A D !2 /H M P

C a dm ium 7300 E LE M E NT S b y IC P 1-4 13 - 2000 H N O 3/HC lO 4 IC P !AES MC EF

C a dm ium 9102 ELEMENTS on WIPES NA NA NA ICP-AES Wipe

C a dm ium 7303 E LE M EN TS by IC P (H O T 1-4 Se e Ta ble H C l /H N O 3 ICP-AES MC EF

B L O C K /H C l /H N O 3 D IG E S T IO N )

C a dm ium 7301 ELE M EN TS b y IC P (A Q UA RE G IA 1-4 13 - 2000 H C l /H N O 3 ICP-AES MC EF

A SH IN G )

C a dm ium & c o m po un ds 7048 C A D M IU M a nd c pd s, as C d 1-3 25 - 1500 H N O 3/H C l FAAS MC EF

C a lc ium 7300 E LE M E NT S b y IC P 1-4 5 - 200 H N O 3/HC lO 4 IC P !AES MC EF

C a lc ium 7303 E LE M EN TS by IC P (H O T 1-4 Se e Ta ble H C l /H N O 3 ICP-AES MC EF

B L O C K /H C l /H N O 3 D IG E S T IO N )

C a lc ium 7301 ELE M EN TS b y IC P (A Q UA RE G IA 1-4 5 - 200 H C l /H N O 3 ICP-AES MC EF

A SH IN G )

C a lc ium & c o m po und s 7020 C A LC IU M a nd c pd s a s C a 1-3 20 - 400 H N O 3/HC lO 4 FAAS MC EF

C a m pho r 1301 KE TO NE S II 0.01 - 0.2 1 - 25 M e O H /C S 2 G C !FID CCT

C a m pho r 2553 KE TO NE S II 0.01 - 0.2 1 - 25 IP A -C S 2 G C -FID A -C M S

C ap sa icin 5041 C AP SA ICIN an d D IHY DR O C AP SA ICIN 1-3 5 - 1000 C H 3C N HPLC !FL GFF

C a ptan 5601 ORG ANONITROGEN PESTICIDES 0.1 - 1 var-480 reagent HP LC - UV OV S-2

C a ptan 9205 CAPTAN and THIOPHENATE-METHYL NA NA IP A /A C N HP LC - U V Patch

o n D E RM A L P A TC H

C a ptan 9202 CAPTAN and THIOPHENATE-METHYL NA NA NA HP LC - U V Hand wa sh

in Handrinse

Carbaryl 5601 ORG ANONITROGEN PESTICIDES 0.1 - 1 var-480 reagent HP LC - UV OV S-2

Carbaryl (Sevin) 5006 CARBARYL 1-3 20 - 400 reagent VIS GFF

3/15/2003 MF!5 NIOSH Manual of Analytical Methods

 M eth Flow Ra te Vol. (L) E x tr a c ti o n A n a ly t ic a l
Chemical No. M e th od Na m e ( L /m i n ) T e c h n iq u e Sampler
min max

C ar be nd az im 5601 ORG ANONITROGEN PESTICIDES 0.1 - 1 var - 480 reagent HP LC - U V OV S-2

C a r bito l 2549 V O L A TI LE O R G A N IC C P D S 0.01 - 0.05 1-6 t h erma l TD /G C !M S TD

(Screen in g)

C a r bo fur an 5601 ORG ANONITROGEN PESTICIDES 0.1 - 1 var-480 reagent HP LC - U V OV S-2

C a r bo n blac k 5000 C A R BO N B LA C K 1-2 30 - 570 NA Grav P VC

C a r bo n, e le m e ntal 5040 ELEM ENTA L CA RBO N (DIES EL PA RT.) 2-4 142-19000 t h erma l E G A/TO A QFF

C a r bo n dio xide 6603 C A R B O N D IO X I D E 0.02 - 0.1 80% vol NA G C !T C D air bag

C a r bo n disulfide 1600 C A R B O N D IS U LF ID E 0.01 -0 .2 2 - 25 toluene G C !FPD CC T & d ry tu b e

C a r bo n m o no xide 6604 CARBON MONOXIDE NA NA NA Sens or Port In str

C a r bo n te trac hlo r ide 1003 HYDROC ARBONS, HALOG ENATED 0.01 - 0.2 3 - 150 C S2 G C !FID CCT

* -3-Carene 1552 TERPENES 0.01 - 0.02 2 - 30 C S2 G C !FID CCT

Cellulose 7404 C E LL UL OS E IN SU LA TIO N 1 NA NA SEM ACF

Chlordane 5510 CHLORDANE 0.5 - 1.0 10 - 200 t ol G C !E C D M C E F & Ch ro m

102

Chlorinated camphene 5039 C H L O R IN A T ED C A M P H E N E 0.2 - 1 2 - 30 p et eth er G C !E C D MC EF

C hlo rinate d diphe nyl ox ide 5025 C H L O R IN A T ED D IP H E N YL O X ID E 0.5 - 1.5 8 - 200 isooctane G C !E C N MC EF

Chlorinated terphenyl 5014 CH LORINA TED TERPH ENYL 1-3 100 - 1500 isooctane G C !E C D GFF

Chlorine 6011 C H L O R IN E a n d B R O M I N E 0.3 - 1.0 2 - 90 N a 2S 2O 3 IC Ag F

C hlo ro ac e talde hyde 2015 C H L O R O A C E T AL D E HY D E 0.05 - 0.2 3 - 16 MeOH G C !E C D SG

C hlo ro ac etic ac id 2008 C HLO RO AC ETIC AC ID 0.05 - 0.2 1 - 100 H 2O IC SG

Chlorobenzene 1003 HYDROC ARBONS, HALOG ENATED 0.01 - 0.2 1.5 - 40 C S2 G C !FID CCT

p -Chlo r o be nzo tr ifluo r id e 1026 p - C H LO R O B E N Z O T RI FL U O R ID E 0.01 - 0.2 0.1 - 10 C S 2/M e O H G C -FID CCT

Chlorobromomethane 1003 HYDROC ARBONS, HALOG ENATED 0.01 - 0.2 0.5 - 60 C S2 G C -FID CCT

Chlorobromomethane 1003 HYDROC ARBONS, HALOG ENATED 0.01 - 0.2 0.5 - 8 C S2 G C !FID CCT

Chlorodifluoromethane 1018 D I C H LO R O D I F LU O R O M E T H A N E 0.01 - 0.05 1-4 C H 2C l2 G C !FID 2 C C T (lg + sm )

Chlorodiphenyl (42 & 54% 5503 POLY CH LORO BIPHENY LS 0.05 - 0.2 1 - 50 hexane G C !E C D G FF & F lor isil
C I)

2 !Chlo ro e thano l 2513 ETH YLE NE CH LO RO HY DR IN 0.01 - 0.2 2 - 35 IP A /C S 2 G C !FID PCT

Ch loroform 1003 HYDROC ARBONS, HALOG ENATED 0.01 - 0.2 1 - 50 C S2 G C !FID CCT

4 !Chloronitrobenzene 2005 N I TR O A R O M A T IC C O M P O U N D S 0.01 - 1.0 1 - 150 MeOH G C !FID SG

p !Chlo ro phe no l 2014 p !C H L O RO P H EN O L 0.05 - 0.2 1.5 - 40 C H 3C N HPLC !U V SG

Chloroprene 1002 $!C H L O R O P R E N E 0.01 - 0.1 1.5 - 8 C S2 G C !FID CCT

C hlo rpr o pham 5601 ORG ANONITROGEN PESTICIDES 0.1 - 1 var-480 reagent HP LC , U V OV S-2

C hlo rpyr ifo s 5600 ORG ANOPHO SPHORUS PESTICIDES 0.2 - 1.0 12 - 240 t ol/a cet G C !FPD O VS !2

C hr om ic a cid 7600 C H R O M I U M , HE X A V A LE N T 1-4 8 - 400 reagent VIS P VC

C hr om ic a cid 7604 C H R O M I U M , HE X A V A LE N T 1-4 100 - 1000 N a O H / N a2 C O 3 IC P VC

C hr o m ium 7024 C H R O M IU M a nd c pd s, as C r 1-3 10 - 1000 H C l /H N O 3 FAAS MC EF

C hr o m ium 7300 E LE M E NT S b y IC P 1-4 5 - 1000 H N O 3/HC lO 4 IC P !AES MC EF

C hr o m ium 7301 ELE M EN TS b y IC P (A Q UA RE G IA 1-4 5 - 1000 H C l /H N O 3 ICP-AES MC EF

A SH IN G )

C hr o m ium 7303 E LE M EN TS by IC P (H O T 1-4 Se e Ta ble H C l /H N O 3 ICP-AES MC EF

B L O C K /H C l /H N O 3 D IG E S T IO N )

C hr o m ium 9102 ELEMENTS on WIPES NA NA NA ICP-AES Wipe

Chromium, hexavalent 7600 C H R O M I U M , HE X A V A LE N T 1-4 8 - 400 reagent VIS P VC

Chromium, hexavalent 7604 C H R O M I U M , HE X A V A LE N T 1-4 100 - 1000 N a O H / N a2 C O 3 IC P VC

3/15/2003 MF!6 NIOSH Manual of Analytical Methods

 M eth Flow Ra te Vol. (L) E x tr a c ti o n A n a ly t ic a l
Chemical No. M e th od Na m e ( L /m i n ) T e c h n iq u e Sampler
min max

Chromium, hexavalent 7605 C H RO M IU M HE XA VA LE NT b y IO N 0.1 - 4 1 - 400 N a O H - N a2C O 3 IC P VC

CHROM ATOGRAPHY

Chromium, hexavalent 7703 CHROM IUM, HEXAV ALENT b y Field - 1-4 10 - 1200 ( N H4) 2SO 4/ N H4O H VIS PVC, MCE, PTFE
Portab le Spe ctroph otom etry

Chromium, hexavalent 9101 CHROM IUM, HEXAV ALENT in s ett led NA NA NA Sp ot Te st s trip
dust

Chrysene 5506 PO LYN UC LEA R A RO M ATIC 2.0 200 - 1000 ac eto nitr ile HPLC !FL/U V P T F E & X A D !2
HYDR OC ARBO NS by H PLC

Chrysene 5515 PO LYN UC LEA R A RO M ATIC 2.0 200 - 1000 va r ies G C !FID P T F E & X A D !2
HYDROC ARBONS

C oal tar naphtha 1550 NAPHTHAS 0.01 - 0.2 1.3 - 20 C S2 G C !FID CCT

C oal tar pitc h vo latile s 5042 B E N Z EN E S O LU B LE F R AC T IO N A N D 1-4 28 - 400 benzene Grav tared PTFE
TOTAL PARTICULATE (ASPHALT FUME)

C ob alt 7300 E LE M E NT S b y IC P 1-4 25 - 2000 H N O 3/HC lO 4 IC P !AES MC EF

C ob alt 9102 ELEMENTS on WIPES NA NA NA ICP-AES Wipe

C ob alt 7301 ELE M EN TS b y IC P (A Q UA RE G IA 1-4 25 - 2000 H C l /H N O 3 ICP-AES MC EF

A SH IN G )

C ob alt 7303 E LE M EN TS by IC P (H O T 1-4 Se e Ta ble H C l /H N O 3 ICP-AES MC EF

B L O C K /H C l /H N O 3 D IG E S T IO N )

C obalt & c o m po unds 7027 C O B A LT an d c p ds , a s C o 1-3 30 - 1500 a q re g /H N O 3 FAAS MC EF

C oppe r 7300 E LE M E NT S b y IC P 1-4 5 - 1000 H N O 3/HC lO 4 IC P !AES MC EF

Co ppe r 7301 ELE M EN TS b y IC P (A Q UA RE G IA 1-4 5 - 1000 H C l /H N O 3 ICP-AES MC EF

A SH IN G )

Co ppe r 9102 ELEMENTS on WIPES NA NA NA ICP-AES Wipe

Co ppe r 7303 E LE M EN TS by IC P (H O T 1-4 Se e Ta ble H C l /H N O 3 ICP-AES MC EF

B L O C K /H C l /H N O 3 D IG E S T IO N )

Co ppe r (dust & fum e ) 7029 CO PPER (dust & fumes) 1-3 50 - 1500 H N O 3/H C l FAAS MC EF

Cr e so l 2549 V O L A TI LE O R G A N IC C P D S 0.01 - 0.05 1-6 t h erma l TD /G C !M S TD

(Screen in g)

Cre sol, all isome rs 2546 C R ES O LS an d P HE NO L 0.01 - 0.1 1 - 24 MeOH G C !FID X A D !7

Cr o tonalde hyde 2539 A L D EH Y D E S, SC R E E N IN G 0.01 - 0.05 5-5 t ol G C !F ID /M S X A D !2 /H M P

Cr o tonalde hyde 3516 C R O T O N A L D EH Y D E 0.1 - 0.2 1 - 49 b u ffer DPP BuB

Cryofluorane 1018 DICHLORODIFLUORO METHANE, 0.01 - 0.05 1-4 C H 2C l2 G C !FID 2 CCT

1,2 !DICHLOROTETR AFLU O R O !
ETHA NE, &
C H L O R O D IF L UO R O M E T H A N E

Cum ene 1501 HY DR O C AR BO NS , AR O M ATIC 0.01 - 0.2 1 - 30 C S2 G C !FID CCT

Cyanides 7904 CYANIDES, aerosol an d g a s 0.5 - 1.0 10 - 180 KOH ISE MCEF & BuB

Cyanides 6010 H Y D R O G E N C Y A N ID E 0.05 - 0.2 0.6 - 90 H 2O VIS s od a lim e

C ya nu ric ac id 5030 C YA NU RIC AC ID 1-3 10 - 1000 rea ge nts HPLC !U V P VC

Cyanazine 5602 CHLORINATED ORG ANONITROGEN 0.2 - 1 12 - 480 reagent G C /E C D OV S-2

H ER BIC ID ES (A IR SA M PL IN G )

Cyanazine 8315 TR IAZ INE HE RB IC IDE S a nd the ir NA NA NA GS-MSD Urine

METABOLITES

Cyanazine 9200 CHLORINATED ORG ANONITROGEN NA NA NA G C - EC D polyethylene

HER BICIDES (HAND WAS H) bag

Cyanazine 9201 CHLORINATED ORG ANONITROGEN NA NA IPA/diazomethane G C - EC D PUF pad

HE RBIC IDES (DER M AL P ATC H))

Cyclohexane 1500 HYDROC ARBONS, BP 36 !216 °C 0.01 - 0.2 2.5 - 5 C S2 G C !FID CCT

Cyc lo he xano l 1402 ALC O HO LS III 0.01 - 0.2 1 - 10 IP A /C S 2 C G !FID CCT

Cyc lo he xano l 1405 ALCOHO LS COM BINED 0.01 - 0.2 2 - 10 IP A -C S 2 G C -FID CCT

3/15/2003 MF!7 NIOSH Manual of Analytical Methods

 M eth Flow Ra te Vol. (L) E x tr a c ti o n A n a ly t ic a l
Chemical No. M e th od Na m e ( L /m i n ) T e c h n iq u e Sampler
min max

Cyclohexanone 2549 V O L A TI LE O R G A N IC C P D S 0.01 - 0.05 1-6 t h erma l TD /G C !M S TD

(Screen in g)

Cyclohexanone 2555 KETONES I 0.01 - 0.2 1 - 10 C S2 G C -FID A -C M S

Cyclohexanone 1300 KETONES I 0.01 - 0.2 1 - 10 C S2 C G !FID CCT

Cyclohexene 1500 HYDROC ARBONS, BP 36 !216 °C 0.01 - 0.2 5-7 C S2 C G !FID CCT

1,3 !Cyclopentadiene 2523 1,3 !C Y C L O P E N TA D IE N E 0.01 - 0.05 1-5 Et Ac G C !FID Chrom104/

maleic anhy

2,4 !D 5001 2,4 !D an d 2,4,5 !T 1-3 15 - 200 MeOH HPLC !U V GFF

2,4-D a cid; 5602 CHLORINATED ORG ANONITROGEN 0.2 - 1 12 - 480 reagent G C - EC D OV S-2
2,4-D,2 -ethylhe xyl ester; H ER BIC ID ES (A IR SA M PL IN G )
2, 4-D , 2-buto xye thyl ester

2,4-D a cid; 9200 CHLORINATED ORG ANONITROGEN NA NA NA G C - EC D polyethylene

2,4-D,2 -ethylhe xyl ester; HER BICIDES (HAND WAS H) bag
2, 4-D , 2-buto xye thyl ester

2,4-D a cid; 9201 CHLORINATED ORG ANONITROGEN NA NA IPA/diazomethane G C - EC D PUF pad

2,4-D,2 -ethylhe xyl ester; HE RBIC IDES (DER M AL P ATC H))
2, 4-D , 2-buto xye thyl ester

D ec abr o mo diphe nyl Ox i de 2559 D E C A B R O M O D I PH E N Y L O X I D E 2.0 48 - 960 T ol G C /N C D GFF

n !Decane 2549 V O L A TI LE O R G A N IC C P D S 0.01 - 0.05 1-6 t h erma l TD /G C !M S TD

(Screen in g)
o
n-Decane 1500 HYDROC ARBONS, BP 36 o-216 C NA NA C S2 G C -FID CCT

D eme to n 5514 D EM E TO N 0.2 - 1.0 30 - 500 toluene G C !FPD M CE F & X A D !2

Desethylatrazine 8315 TR IAZ INE HE RB IC IDE S a nd the ir NA NA NA GC-M SD Urine

METABOLITES

Desisopropylatrazine 8315 TR IAZ INE HE RB IC IDE S a nd the ir NA NA NA GC-M SD Urine

METABOLITES

D i ac eto ne alc oho l 1402 ALC O HO LS III 0.01 - 0.2 1 - 10 IP A /C S 2 G C !FID CCT

D i ac eto ne alc oho l 1405 ALCOHO LS COM BINED 0.01 - 0.2 1 - 10 IP A -C S 2 G C -FID CCT

Diacetyl 2557 DIACETYL 0.01 - 0.2 1 - 10 Ac et-M eth G C -FID A -C M S

o !Dianisidine 5013 DYES 1-3 150 - 500 H 2O HPLC !U V PTFE

Diato ma ce ou s ea rth 7501 SILICA, AMOR PHOUS 1-3 50 - 400 ash XR D PVC/CYC

D i azino n 5600 ORG ANOPHO SPHORUS PESTICIDES 0.2 - 1 12 - 240 toluene/acetone G C !FPD O VS !2

Diazomethane 2515 D I AZ O M E T H A N E 0.2 6 - 30 C S2 G C !FID X A D !2 ( c o at e d )

Dibenz[a,h]anthracene 5506 PO LYN UC LEA R A RO M ATIC 2.0 200 - 1000 ac eto nitr ile HPLC !FL/U V P T F E & X A D !2
HYDR OC ARBO NS by H PLC

Dibenz(a,h) anthracene 5515 PO LYN UC LEA R A RO M ATIC 2.0 200 - 1000 va r ies G C !FID P T F E & X A D !2
HYDROCARBONS

Diborane 6006 D I BO R A N E 0.5 - 1.0 60 - 260 H 2O 2 PES P TF E & C C T

w / o xi d iz e r

Dibromodifluoromethane 1012 D I FL U O R O D IB R O M O M E T H A N E 0.01 - 0.2 2.5 - 10 IPA G C !FID 2 CCT

2 !D ibutylam ino e thanol 2007 A M I N O E TH A N O L C O M P O U N D S 0.01 - 0.2 4 - 24 M eO H/H 2O G C !FID SG

Dibu tyl ph osp ha te 5017 DIBUTY L PHO SPH ATE 1-3 50 - 250 C H 3C N G C !FPD PTFE

Dibu tyl ph tha late 5020 D I BU T YL P HT H A LA T E & 1-3 6 - 200 C S2 G C !FID MC EF

DI(2 !ETHY LHEX YL) PHTH ALATE

Dibutyltin bis(isooctyl 5504 O R G A N O T IN C O M P O U N D S 1 - 1.5 50 - 500 A c etic a /C H 3C N HP LC /G FAAS G F F + X A D !2

m e r c apto ac e tate )

o !, p !Dichlorobenzene 2549 V O L A TI LE O R G A N IC C P D S 0.01 - 0.05 1-6 va r ies TD /G C !M S TD

(Screen in g)

o-Dichlorobenzene 1003 HYDROC ARBONS, HALOG ENATED 0.01 - 0.2 1 - 10 C S2 G C -FID CCT

3/15/2003 MF!8 NIOSH Manual of Analytical Methods

 M eth Flow Ra te Vol. (L) E x tr a c ti o n A n a ly t ic a l
Chemical No. M e th od Na m e ( L /m i n ) T e c h n iq u e Sampler
min max

p-Dichlorobenzene 1003 HYDROC ARBONS, HALOG ENATED 0.01 - 0.2 1-8 C S2 G C -FID CCT

p !Dichlorobenzene 1003 HYDROC ARBONS, HALOG ENATED 0.01 - 0.2 1 - 10 C S2 G C !FID CCT

3,3'!Dichlorobenzidine 5509 BENZIDINE an d 0.2 20 - 100 TE A/M e O H HPLC !U V GFF

3,3'!D I C H LO R O B E N Z ID I NE

Dichlorodifluoromethane 1018 DICHLORODIFLUORO METHANE, 0.01 - 0.05 1-4 C H 2C l2 G C !FID 2 CCT

1,2 !DICHLOROTETR AFLUO R O ! (lg + sm )
ETHANE &
C H L O R O D IF L UO R O M E T H A N E

1,1 !Dichloroethane 1003 HYDROC ARBONS, HALOG ENATED 0.01 - 0.2 0.5 - 15 C S2 G C !FID CCT

1,2 !Dichloroethane 1003 HYDROC ARBONS, HALOG ENATED 0.01 - 0.2 0.5 - 50 C S2 G C !FID CCT

D i c hlo r o e thyl e the r 1004 DICHLOROETHYL ETHER 0.01 - 1.0 2 - 15 C S2 G C !FID CCT

1,2 !Dichloroethylene 1003 HYDROC ARBONS, HALOG ENATED 0.01 - 0.2 0.2 - 5 C S2 G C !FID CCT

Dichlorofluoromethane 2516 D I C H LO R O F L U O R O M E T HA N E 0.01 - 0.05 0.25 - 3 C S2 G C !FID 2 C CT ( lg )

Dichloromethane 1005 M E T H YL E N E C H L O R ID E 0.01 - 0.2 0.5 - 2.5 C S2 G C !FID 2 CCT

Dichloromethane 2549 V O L A TI LE O R G A N IC C P D S 0.01 - 0.05 1-6 t h erma l TD /G C !M S TD

(Screen in g)

1,1 !Dichlo ro !1 !nitroethane 1601 1,1 !DICHLORO !1 !N I TR O E T H AN E 0.01 - 1.0 1.5 - 15 C S2 G C !FID PCT

1,2 !Dichloropropane 1013 P R O P Y LE N E D IC H L O R ID E 0.01 - 0.2 0.1 - 3.5 Acet/cyclohexane G C !E C N PCT

1,2 !D ic hlo r o te tra- 1018 DIC HLO RO DIFLUO RO ME THAN E, 0.01 - 0.05 1-4 C H 2C l2 G C !FID 2 CCT
fluoroethane 1,2 !DICHLOROTETR AFLUO R O ! (lg + sm )
ETHANE &
C H L O R O D IF L UO R O M E T H A N E

D i c ro to pho s 5600 ORG ANOPHO SPHORUS PESTICIDES 0.2 - 1 12 - 240 t ol/a cet G C !FPD O VS !2

Diesel exhaust 5040 ELEM ENTA L CA RBO N (DIES EL PA RT.) 1-4 142 -19000 t h erma l E G A/TO A QFF

Diethanolamine 3509 AM INO ETH AN O L C O M PO UN DS II 0.5 - 1.0 5 - 300 HSA IC IM P

Diethylamine 2010 AM INE S, A LIPH ATIC 0.01 - 1.0 3 - 30 H 2SO 4/M e O H G C !FID SG

2 !D ie thylam ino e thanol 2007 AMINOETHANO L COM POUNDS I 0.01 - 0.2 4 - 24 M eO H/H 2O G C !FID SG

D i e thyle ne glyc o l 5523 GLYC OLS 0.5 - 2 5 - 60 MeOH G C !FID O VS !7

D i e thyle ne glyc o l e ther 2549 V O L A TI LE O R G A N IC C P D S 0.01 - 0.05 1-6 t h erma l TD /G C !M S TD

(Screen in g)

Diethylenetriamine 2540 ETHYLENEDIAMINE, 0.01 - 0.1 1 - 20 DMF HPLC !U V X A D !2

DIETHY LENE TRIAM INE, & w/10 % N ITC
T R IE T HY L EN E TE T RA M I N E

D i!(2 !ethy lhexy l) phth alate 5020 DIBUTYL PHTHALATE an d 1-3 10 - 200 C S2 G C !FID MC EF
DI(2 !ETHY LHEX YL) PHTH ALATE

Difluorodibromom ethane 1012 D I FL U O R O D IB R O M O M E T H A N E 0.01 - 0.2 2.5 - 10 IPA G C !FID 2 CCT

Difluorodichloromethane 1018 DIC HLO RO DIFLUO RO ME THAN E, 0.01 - 0.05 1-4 C H 2C l2 G C !FID 2 CCT
1,2 !DICHLOROTETR AFLU O R O !ET HAN
E & C H L O R O D IF L UO R O M E T H A N E

Dih yd ro ca ps aic in 5041 C AP SA ICIN an d D IHY DR O C AP SA ICIN 1-3 7 - 1000 C H 3C N HPLC !FL GFF

Diisobutyl ketone 1300 KETONES I 0.01 - 0.2 1 - 10 C S2 G C !FID CCT

Diisobutyl ketone 2555 KETONES I 0.01 - 0.2 1 - 10 C S2 G C -FID A -C M S

D i m e thylac e tam ide 2004 DIMETHYLACETAMIDE and 0.01 - 1.0 15 - 80 MeOH G C !FID SG
D I M E TH Y L FO R M A M I D E

Dimethylamine 2010 AM INE S, A LIPH ATIC 0.01 - 1.0 3 - 30 H 2SO 4/M e O H G C !FID SG

2-(D im e thylam ino )e thanol 2561 2 -(D IM E TH YL AM IN O )E TH A NO L 0.02 - 0.1 10 - 24 MeOH G C -FID XAD
1-D im e thylam ino -2-propan ol 1 -D IM E TH YL AM IN O -2 -P RO P AN O L

N,N !Dimethylaniline 2002 AM INE S, A RO M ATIC 0.02 - 1.0 3 - 30 Et h a nol G C !FID SG

Dim eth yla rsin ic a cid 5022 A R S E N IC , O R G A N O ! 1-3 50 - 1000 b u ffer IC !HYAAS PTFE

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 M eth Flow Ra te Vol. (L) E x tr a c ti o n A n a ly t ic a l
Chemical No. M e th od Na m e ( L /m i n ) T e c h n iq u e Sampler
min max

Dim e thylfo rmamide 2004 DIMETHYLACETAMIDE & 0.01 - 1.0 15 - 80 MeOH G C !FID SG
D I M E TH Y L FO R M A M I D E

1,1 !Dimethylhydrazine 3515 1,1 !D I M E TH Y L HY D R A Z IN E 0.2 - 1.0 2 - 100 reagent VIS BuB (0.1 M HC l)

N,N !Dimethyl!p !toluidine 2002 AM INE S, A RO M ATIC 0.02 - 1.0 20 - 100 Et h a nol G C !FID SG

Dim ethy l sulfate 2524 DIM ETHY L SULFA TE 0.01 - 0.2 0.25 - 12 d iEt eth er G C !E C N Por P

Dioxane 1602 D I O X AN E 0.01 - 0.2 0.5 - 15 C S2 G C !FID CCT

Diphenyl 2530 DIPHENYL 0.01 - 0.5 15 - 30 C C l4 G C !FID Te na x G C

D i pro pyle ne glyc o l 2554 GLYCOL ETHER S 0.1 - 0.2 3 - 25 M e C l2/Me th G C -FID A-747
mo no m e thyl e the r

D i sulfo to n 5600 ORG ANOPHO SPHORUS PESTICIDES 0.2 - 1 12 - 240 t ol/a cet G C !FPD O VS !2

D i uro n 5601 ORG ANONITROGEN PESTICIDES 0.1 - 1 var-480 reagent HP LC , U V OV S-2

o o
n-Dodecane 1500 HYDROC ARBONS, BP 36 -216 C NA NA C S2 G C -FID CCT

D y e s ! benzidine !, 5013 D Y E S , B E N ZI D IN E !, o ! T O LI D IN E !, 1-3 150 - 500 H 2O HPLC !U V PTFE

o !tolidine !, o !dianisidine ! o ! D IA N IS ID I NE

E le me ntal c ar bo n 5040 ELEM ENTA L CA RBO N (DIES EL PA RT.) 2-4 142 -19000 t h erma l E G A-TO A QFF

Elem ents 7300 E LE M E NT S b y IC P 1-4 V a r ies H N O 3/HC lO 4 IC P !AES MC EF

Elem ents 7301 ELEMENTS by ICP (Aqu a R eg ion 1-4 V a r ies Aq R eg ICP-AES MC EF
Ashin g) PVCF

Elem ents 7303 E LE M EN TS by IC P (H O T 1-4 Se e Ta ble H C l /H N O 3 ICP-AES MC EF

B L O C K /H C l /H N O 3 D IG E S T IO N )

En dr in 5519 EN DR IN 0.5 - 1.0 12 - 400 t ol G C !E C D MCEF &

Chrom 102

Ep ich lor oh yd rin 1010 EP ICH LO RO HY DR IN 0.01 - 0.2 2 - 30 C S2 G C !FID CCT

EPN 5012 EPN 1-2 15 - 700 isooctane G C !FPD GFF

1,2 !Epoxypropane 1612 P R O P Y LE N E O X ID E 0.01 - 0.2 0.5 - 5 C S2 G C !FID CCT

$ -Estradiol 5044 E S TR O G E N I C C O M P O U N D S 1 150 - 1000 M eth HP LC - U V PTFE

Estrone 5044 E S TR O G E N I C C O M P O U N D S 1 150 - 1000 M eth HP LC - U V PTFE

$ -Estro diol-3 -Ben zoa te 5044 E S TR O G E N I C C O M P O U N D S 1 150 - 1000 M eth HP LC - U V PTFE

E thano l 2549 V O L A TI LE O R G A N IC C P D S 0.01 - 0.05 1-6 t h erma l TD /G C !M S TD

(Screen in g)

E thano l 1400 ALCOHO LS I 0.01 - 0.05 0.1 - 1 2 -b u ta n ol/C S 2 G C !FID CCT

Ethanolamine 2007 AMINOETHANO L COM POUNDS I 0.01 - 0.2 4 - 24 5600 G C !FID SG

E thio n 5600 ORG ANOPHO SPHORUS PESTICIDES 0.2 - 1 12 - 240 t ol/a cet G C !FPD O VS !2

E tho pr o p 5600 ORG ANOPHO SPHORUS PESTICIDES 0.2 - 1 12 - 240 t ol/a cet G C !FPD O VS !2

2 !Etho xye thano l 1403 ALC O HO LS IV 0.01 - 0.05 1-6 MeOH G C !FID CCT

2 !Etho xye thyl a ce tate 1450 ESTERS I 0.01 - 0.2 1 - 10 C S2 G C !FID CCT

Ethy l ace tate 2549 V O L A TI LE O R G A N IC C P D S 0.01 - 0.05 1-6 t h erma l TD /G C !M S TD

(Screen in g)

Ethy l ace tate 1457 ETHY L AC ETATE 0.01 - 0.2 0.1 - 10 C S2 G C !FID CCT

Ethy l acry late 1450 ESTERS I 0.01 - 0.2 1 - 10 C S2 G C !FID CCT

Ethyl amyl ketone 1301 KE TO NE S II 0.01 - 0.2 1 - 25 M e O H /C S 2 G C !FID CCT

Ethylbenzene 1501 HY DR O C AR BO NS , AR O M ATIC 0.01 - 0.2 1 - 24 C S2 G C !FID CCT

E thyl bro m ide 1011 E T HY L BR O M I D E 0.01 - 0.2 0.5 - 4 IPA G C !FID CCT

Ethyl butyl ketone 1301 KE TO NE S II 0.01 - 0.2 1 - 25 M e O H /C S 2 G C !FID CCT

E thyl c hlo ride 2519 E T HY L C H LO R I D E 0.02 - 0.05 0.3 - 3 C S2 G C !FID 2 CC T ( lg )

Eth yle ne ch lor oh yd rin 2513 ETH YLE NE CH LO RO HY DR IN 0.01 - 0.2 2 - 35 IP A /C S 2 G C !FID PCT

3/15/2003 MF!10 NIOSH Manual of Analytical Methods

 M eth Flow Ra te Vol. (L) E x tr a c ti o n A n a ly t ic a l
Chemical No. M e th od Na m e ( L /m i n ) T e c h n iq u e Sampler
min max

Ethylenediamine 2540 ETHY LENE DIAM INE, 0.01 - 0.1 1 - 20 DMF HPLC !U V X A D !2
DIETHY LENE TRIAM INE, & w/10 % N ITC
T R IE T HY L EN E TE T RA M I N E

E thyle ne dibr o m ide 1008 E T HY L EN E D IB R O M I D E 0.02 - 0.2 0.1 - 25 b z/M e O H G C !E C D CCT

E thyle ne dic hlor ide 1003 HYDROC ARBONS, HALOG ENATED 0.01 - 0.2 1 - 50 C S2 G C !FID CCT

E thyle ne glyc o l 5523 GLYC OLS 0.5 - 2 5 - 60 MeOH G C !FID O VS !7

Ethy lene glyc ol dinitra te 2507 N ITR O G LY C ER IN & ETH YL EN E G LY C O L 0.2 - 1.0 3 - 100 Et h a nol G C !E C D Te na x G C
DINITRA TE

E thyle ne o xide 1614 E T HY L EN E O X ID E 0.05 - 0.15 1 - 24 DMF G C !E C D PC T w/HB r

E thyle ne o xide 3702 E TH YL EN E O X ID E b y p orta ble G C > 0.02 80% vol NA G C !PID air bag

E thyle ne o xide 3800 ORG ANIC and INORGANIC G ASES 0.1 - 2.0 Inst r. d ep . NA FTIR Di r. R e a d
by EX TR ACTIV E FTIR SPE C T R O MET R Y

E thyle ne thio ur e a 5011 ETHYLENE THIOUREA 1-3 200 - 800 H 2O VIS PVC or MCEF

Ethylenimine 3514 E T HY L EN I M IN E 0.2 1 - 48 C H C l3 HPLC !U V BuB

E thyl ethe r 1610 ETHYL ETHER 0.01 - 0.2 0.25 - 3 C S2 G C -FID CCT

E thyl ethe r 1610 ETHYL ETHER 0.01 - 0.2 0.25 - 3 Et Ac G C !FID CCT

Ethy l form ate 1452 ETHY L FO RM ATE 0.01 - 0.2 0.3 - 10 C S2 G C !FID CCT

E thyl m e rc aptan 2542 M E R C A P TA N S 0.1 - 0.2 10 - 150 H C l/D C E G C !FPD GFF/HgAc

Ethy l me tha cryta te 2537 ME THYL a nd ETH YL M ETHA CR YLATE 0.01 - 0.05 1-8 C S2 G C -FID XAD

F e nam ipho s 5600 ORG ANOPHO SPHORUS PESTICIDES 0.2 - 1 12 - 240 t ol/a cet G C !FPD O VS !2

Fibrous glass 7400 A S BE ST O S & o th e r F IB ER S b y PC M 0.5 - 16 400 !va r ies ! PCM MC EF

Fluoranthene 5506 PO LYN UC LEA R A RO M ATIC 2.0 200 - 1000 ac eto nitr ile HPLC !FL/U V P T F E & X A D !2
HYDR OC ARBO NS by H PLC

Fluoranthene 5515 PO LYN UC LEA R A RO M ATIC 2.0 200 - 1000 va r ies G C !FID P T F E & X A D !2
HYDROCARBONS

Fluorene 5506 PO LYN UC LEA R A RO M ATIC 2.0 200 - 1000 ac eto nitr ile HPLC !FL/U V P T F E & X A D !2
HYDR OC ARBO NS by H PLC

Fluorene 5515 PO LYN UC LEA R A RO M ATIC 2.0 200 - 1000 va r ies G C !FID P T F E & X A D !2
HYDROCARBONS

F luo r ide s 7902 FLUORIDES, aerosol & ga s 1-2 12 - 800 N a OH ISE MCEF & pad
w / N a2 C O 3

F luo r ide s 7906 FLU O RID ES by IC 1-2 s 1 - 800 N a OH IC MCEF & pad w/
i 120 - 800 N a 2C O 3

Fluorotrichloromethane 1006 F L UO R O T R IC H L O R O M E T H A NE 0.01 - 0.05 0.3 - 7 C S2 G C !FID C CT ( lg )

F o no fo s 5600 ORG ANOPHO SPHORUS PESTICIDES 0.2 - 1.0 12 - 240 t ol/a cet G C !FPD O VS !2

F o r malde hyde 2016 F O R M A L D E HY D E 0.1 - 1.5 1 - 15 ac eto nitr ile HP LC - U V SG/DNPH

F o r malde hyde 2541 F O R M A L D E HY D E 0.01 - 0.1 1 - 36 t ol G C !FID X A D !2 /H M P

F o r malde hyde 3500 F O R M A L D E HY D E 0.2 - 1.0 1 - 100 NaHSO 3 VIS P TF E & 2 IM P

F o r malde hyde 2539 A L D EH Y D E S, SC R E E N IN G 0.01 - 0.05 5-5 t ol G C !F ID /M S X A D !2 /H M P

F o r malde hyde 3800 ORG ANIC and INORGANIC G ASES 0.1 - 2.0 Inst r. d ep . NA FTIR Di r. R e a d
by EX TR ACTIV E FTIR SPE C T R O MET R Y

F o r malde hyde 5700 FORM ALDEHYDE on dust 2 240 - 1050 H 2O /D N PH /C H 3C N HPLC !U V I O M / P VC

F o rm e ta n ate .H C I 5601 ORG ANONITROGEN PESTICIDES 0.1 - 1 var-480 reagent HP LC , U V OV S-2

Fo rm ic a cid 2011 FO RM IC A C ID 0.05 - 0.2 1 - 24 H 2O IC PTFE & SG

( w a sh e d )

F ur fur al 2529 FU R FU R AL 0.01 - 0.05 1 - 12 t ol G C !FID X A D !2 /H M P

F ur fur al 2539 A L D EH Y D E S, SC R E E N IN G 0.05 5-5 t ol G C !F ID /M S X A D !2 /H M P

3/15/2003 MF!11 NIOSH Manual of Analytical Methods

 M eth Flow Ra te Vol. (L) E x tr a c ti o n A n a ly t ic a l
Chemical No. M e th od Na m e ( L /m i n ) T e c h n iq u e Sampler
min max

F u r fur yl alco ho l 2505 F UR FU RY L A LC O H O L 0.01 - 0.05 3 - 25 a cet G C !FID Por Q

G allium 7303 E LE M EN TS by IC P (H O T 1-4 Se e Ta ble H C l /H N O 3 ICP-AES MC EF

B L O C K /H C l /H N O 3 D IG E S T IO N )

G lutar alde hyde 2532 G L U TA R A LD E H Y D E 0.01 - 0.08 4 - 39 C H 3C N HPLC !U V SG/DNPH

Glycerin mist 0500 PARTICU LATES N.O.R . 1-2 7 - 133 NA Grav P VC

G lyc ido l 1608 G LY C ID O L 0.01 - 1.0 5 - 100 T HF G C !FID CCT

G lyc ols 5523 GLYC OLS 0.5 - 2 5 - 60 MeOH G C !FID O VS !7

G old 7303 E LE M EN TS by IC P (H O T 1-4 Se e Ta ble H C l /H N O 3 ICP-AES MC EF

B L O C K /H C l /H N O 3 D IG E S T IO N )

H eptanal 2539 A L D EH Y D E S, SC R E E N IN G 0.01 - 0.05 5-5 t ol G C !F ID /M S X A D !2 /H M P

n !Heptane 2549 V O L A TI LE O R G A N IC C P D S 0.01 - 0.05 1-6 t h erma l TD /G C !M S TD

(Screen in g)

n !Heptane 1500 HYDROC ARBONS, BP 36 !216 °C 0.01 - 0.2 NA C S2 G C !FID CCT

2-Heptanone 2553 KE TO NE S II 0.01 - 0.2 1 - 25 IP A -C S 2 G C -FID A -C M S

3-Heptanone 2553 KE TO NE S II 0.01 - 0.2 1 - 25 IP A -C S 2 G C -FID A -C M S

H er bic ides 5602 CHLORINATED ORG ANONITROGEN 0.2 - 1 12 - 480 reagent G C /E C D OV S-2
H ER BIC ID ES (A IR SA M PL IN G )

H er bic ides 9200 CHLORINATED ORG ANONITROGEN NA NA NA G C - EC D polyethylene

HER BICIDES (HAND WAS H) bag

H er bic ides 9201 CHLORINATED ORG ANONITROGEN NA NA IPA/diazomethane G C - EC D PUF pad

HE RBIC IDES (DER M AL P ATC H))

Hexachlorobutadiene 2543 H E X A C H LO R O B U T A D IE N E 0.05 - 0.2 1 - 100 hexane G C !E C D X A D !2

Hexa chloro !1,3 !cy clo 2518 HEXACHLOR O !1,3 !CY CLO PEN TA 0.01 - 0.2 0.25 - 90 hexane G C !E C D 2 Por T
pentadiene D I EN E

Hexachloroethane 1003 HYDROC ARBONS, HALOG ENATED 0.01 - 0.2 3 - 70 C S2 G C !FID CCT

Hexamethylene! 5522 ISOCYANATES 1-2 15 - 360 tryptamine/DMSO HPLC !FL IM P

diisoc ya nate

1,6-Hexamethylene ! 5521 ISO C YA NA TES , M O NO M ER IC 1.0 5 - 500 rea ge nts HPLC !EC HD IM P
diisoc ya nate

1,6-Hexamethylene 5525 ISOCYANATES, TOTAL (MAP) 1-2 1 - 500 MAP HP LC /UV G F F, IM P

diiso cy an ate (HD I)

H exanal 2539 A L D EH Y D E S, SC R E E N IN G 0.01 - 0.05 5-5 t ol G C !F ID /M S X A D !2 /H M P

H exanal 2549 V O L A TI LE O R G A N IC C P D S 0.01 - 0.05 1-6 t h erma l TD /G C !M S TD

(Screen in g)

n !Hexane 2549 V O L A TI LE O R G A N IC C P D S 0.01 - 0.05 1-6 t h erma l TD /G C !M S TD

(Screen in g)

n !Hexane 1500 HYDROC ARBONS, BP 36 !216 °C 0.01 - 0.2 4-4 C S2 G C !FID CCT

n-Hexane 3800 ORG ANIC and INORGANIC G ASES 0.1 - 2.0 Inst r. d ep . NA FTIR Di r. R e a d
by EX TR ACTIV E FTIR SPE C T R O MET R Y

2 !Hexanone 1300 KETONES I 0.01 - 1.0 1 - 10 C S2 G C !FID CCT

2-Hexanone 2555 KETONES I 0.01 - 0.2 1 - 10 C S2 G C -FID A -C M S

Hip pu ric ac id 8301 HIP PU RIC an d M ETH YL H IPP UR IC NA NA Et a c HP LC - U V NA

ACID in urine

Hydrazine 3503 H Y D R A ZI N E 0.2 - 1.0 7 - 100 rea ge nts VIS BuB

- 2-
H y dr o ge n br o mide 7903 AC IDS , INO RG AN IC 0.2 - 0.5 3 - 100 H C O 3 /C O 3 IC SG
2-
H y dr o ge n c hlo r ide 7903 AC IDS , INO RG AN IC 0.2 - 0.5 3 - 100 H C O 3-/C O 3 IC SG

H y dr o ge n c yanide 6010 H Y D R O G E N C Y A N ID E 0.05 - 0.2 2 - 90 H 2O VIS s od a lim e

H y dr o ge n c yanide 6017 H Y D R O G E N C Y A N ID E 0.05 - 2 2 - 90 H 2O IC -D C Am p SL

3/15/2003 MF!12 NIOSH Manual of Analytical Methods

 M eth Flow Ra te Vol. (L) E x tr a c ti o n A n a ly t ic a l
Chemical No. M e th od Na m e ( L /m i n ) T e c h n iq u e Sampler
min max

H ydr o ge n c yanide 7904 CYANIDES, AEROSOL & G AS 0.5 - 1.0 7 - 100 KOH ISE MC EF
- 2-
H y dr o ge n flo ur ide 7903 AC IDS , INO RG AN IC 0.2 - 0.5 3 - 100 H C O 3 /C O 3 IC SG

H y dr o ge n flo ur ide 7902 FLUORIDES, AEROSOL & G AS 1-2 12 - 800 N a OH ISE M CE F & p a d
w / N a2C O 3

H y dr o ge n flo ur ide 7906 FLU O RID ES by IC 1-2 1 - 800 N a OH IC M CE F & p a d

w / N a2C O 3

H y dr o ge n sulfide 6013 H Y D R O G E N S UL F ID E 0.1 - 1.5 1.2 - 40 N H 4OH /H 2O 2 IC P T FE &

(withdrawn) C CT ( lg )

Hydroquinone 5004 H Y D R O Q U IN O N E 1-4 30 - 180 ac etic ac id HPLC !U V MC EF

Indeno[1,2,3-cd]pyrene 5506 PO LYN UC LEA R A RO M ATIC 2.0 200 - 1000 ac eto nitr ile HPLC !FL/U V P T F E & X A D !2
HYDR OC ARBO NS by H PLC

Inden o [1,2,3 !cd] pyrene 5515 PO LYN UC LEA R A RO M ATIC 2.0 200 - 1000 va r ies G C !FID P T F E & X A D !2
HYDROCARBONS

Iodine 6005 I O D IN E 0.5 - 1.0 15 - 225 N a 2C O 3 IC C C T w /alk ali

I ndium 7303 E LE M EN TS by IC P (H O T 1-4 Se e Ta ble H C l /H N O 3 ICP-AES MC EF

B L O C K /H C l /H N O 3 D IG E S T IO N )

I ron 9102 ELEMENTS on WIPES NA NA NA ICP-AES Wipe

I ron 7301 ELE M EN TS b y IC P (A Q UA RE G IA 1-4 5 - 100 H C l /H N O 3 ICP-AES MC EF

A SH IN G )

I ron 7303 E LE M EN TS by IC P (H O T 1-4 Se e Ta ble H C l /H N O 3 ICP-AES MC EF

B L O C K /H C l /H N O 3 D IG E S T IO N )

I ron 7300 E LE M E NT S b y IC P 1-4 5 - 100 H N O 3/HC lO 4 IC P !AES MC EF

Isoa my l ace tate 1450 ESTERS I 0.01 - 0.2 1 - 10 C S2 G C !FID CCT

I soam yl alc o ho l 1402 ALC O HO LS III 0.01 - 0.2 1 - 10 IP A /C S 2 G C !FID CCT

I soam yl alc o ho l 1405 ALCOHO LS COM BINED 0.01 - 0.2 1 - 10 IP A -C S 2 G C -FID CCT

Isob utyl a ce tate 1450 ESTERS I 0.01 - 0.2 1 - 10 C S2 G C !FID CCT

I sobutyl alco ho l 1401 ALC O HO LS II 0.01 - 0.2 2 - 10 IP A /C S 2 G C !FID CCT

I sobutyl alco ho l 1405 ALCOHO LS COM BINED 0.01 - 0.2 2 - 10 IP A -C S 2 G C -FID CCT

I sobutyraldehyde 2539 A L D EH Y D E S, SC R E E N IN G 0.01 - 0.05 5-5 t ol G C !F ID /M S X A D !2 /H M P

I soc yanate s 5521 ISO C YA NA TES , M O NO M ER IC 1.0 5 - 500 rea ge nts HPLC !EC HD IM P

I soc yanate s 5522 ISOCYANATES 1-2 15 - 360 tryptamine/DMSO HPLC !FL/EC HD IM P

Isophorone 2508 I SO P H O R O N E 0.01 - 1.0 2 - 25 C S2 G C !FID PCT

Isophorone 2556 I SO P H O R O N E 0.01 - 1 2 - 25 DEE G C -FID XAD

Isop ho rone diisoc ya nate 5525 ISOCYANATES, TOTAL (MAP) 1-2 1 - 500 MAP HP LC /UV G F F, IM P
(IPD I)

Isop rop yl ac etate 1454 ISOP RO PYL A CE TATE 0.02 - 0.2 0.1 - 9 C S2 G C !FID CCT

Isop rop yl ac etate 1460 ISOP RO PYL A CE TATE 0.02 - 0.2 0.1 - 9 C S 2-M eth G C -FID CCT

I sopr o pyl alco ho l 2549 V O L A TI LE O R G A N IC C P D S 0.01 - 0.05 1-6 t h erma l TD /G C !M S TD

(Screen in g)

I sopr o pyl alco ho l 1400 ALCOHO LS I 0.01 - 0.2 0.2 - 3 2 -b u ta n on e /C S 2 G C !FID CCT

I sopr o pyl e the r 1618 ISOPROPYL ETHER 0.01 - 0.05 0.1 - 3 C S2 G C !FID CCT

I sopr o pyl glyc idyl ether 1620 ISOPROPYL GLYCIDYL ETHER 0.01 - 0.2 1 - 30 C S2 G C !FID CCT

I sovale r alde hyde 2018 ALIPHATIC ALDEHYDES 0.1 - 1.5 1 - 15 ACN HP LC /UV SG-DNPH

I sovale r alde hyde 2539 A L D EH Y D E S, SC R E E N IN G 0.01 - 0.05 5-5 t ol G C !F ID /M S X A D !2 /H M P

Kepone 5508 KEPONE 0.5 - 1.0 50 - 600 b z/M e O H G C !E C D M C E F & IM P

Kerosene 1550 NAPHTHAS 0.01 - 0.2 1.3 - 20 C S2 G C !FID CCT

3/15/2003 MF!13 NIOSH Manual of Analytical Methods

 M eth Flow Ra te Vol. (L) E x tr a c ti o n A n a ly t ic a l
Chemical No. M e th od Na m e ( L /m i n ) T e c h n iq u e Sampler
min max

Lanthanum 7301 ELE M EN TS b y IC P (A Q UA RE G IA 1-4 5 - 1000 H C l /H N O 3 ICP-AES MC EF

A SH IN G )

La nthanum 9102 ELEMENTS on WIPES NA NA NA ICP-AES Wipe

Lead 7082 LEAD by FAAS 1-4 200 - 1500 H N O 3/H 2O 2 FAAS MC EF

Lead 7702 LEAD BY FIELD POR TABLE XRF 1-4 570 - 1900 NA XR F (po rt) MC EF

Lead 7105 LEAD by GFAAS 1-4 1 - 1500 H N O 3/H 2O 2 G FAAS MC EF

Lead 7701 LEAD BY ULTRASOUND /ASV 1-4 20 - 1500 HNO3 Port ASV MC EF

Lead 7300 E LE M E NT S b y IC P 1-4 1250 -2000 H N O 3/HC lO 4 IC P !AES MC EF

Lead 7700 LEAD in Air by Che mical Spot Test 2 10 - 240 ! Sp ot MC EF

Lead 9100 LEAD in Surface Wipe Sa mp les NA NA H N O 3/HC lO 4 A A S; IC P Wipes

Lead 7301 ELE M EN TS b y IC P (A Q UA RE G IA 1-4 50 - 2000 H C l /H N O 3 ICP-AES MC EF

A SH IN G )

Lead 9102 ELEMENTS on WIPES NA NA NA ICP-AES Wipe

Lead 7303 E LE M EN TS by IC P (H O T 1-4 Se e Ta ble H C l /H N O 3 ICP-AES MC EF

B L O C K /H C l /H N O 3 D IG E S T IO N )

Lead 9105 LEAD in DUST WIPES by C h emica l NA NA NA Sp ot Wipe

Spot Test

Lead sulfide 7505 L E AD S U LF ID E 1.7 or 2 .2 600 - 1000 T HF XR D C Y C & P VC

Limonene 1552 TERPENES 0.01 - 0.2 2 - 30 C S2 G C !FID CCT

Limonene 2549 V O L A TI LE O R G A N IC C P D S 0.01 - 0.05 1-6 t h erma l TD /G C !M S TD

(Screen in g)

Lindane 5502 A L D R IN a n d LI N DA N E 0.2 - 1.0 18 - 240 isooctane G C !E C N GFF & BuB

Lithium 7300 E LE M E NT S b y IC P 1-4 100 - 2000 H N O 3/HC lO 4 IC P !AES MC EF

Lithium 7301 ELE M EN TS b y IC P (A Q UA RE G IA 1-4 100 - 2000 H C l /H N O 3 ICP-AES MC EF

A SH IN G )

Lithium hydr o xide 7401 ALKA LINE DU STS 1-4 70 - 1000 HCl T it ra t ion PTFE

M agne sium 7300 E LE M E NT S b y IC P 1-4 5 - 67 H N O 3/HC lO 4 IC P !AES MC EF

M agne sium 7301 ELE M EN TS b y IC P (A Q UA RE G IA 1-4 5 - 67 H C l /H N O 3 ICP-AES MC EF

A SH IN G )

M agne sium 7303 E LE M EN TS by IC P (H O T 1-4 Se e Ta ble H C l /H N O 3 ICP-AES MC EF

B L O C K /H C l /H N O 3 D IG E S T IO N )

M alathio n 5600 ORG ANOPHO SPHORUS PESTICIDES 0.2 - 1 12 - 60 t ol/a cet G C !FPD O VS !2

M ale ic A nhydride 3512 M A L E IC A N H Y D R ID E 0.2 - 1.5 40 - 500 H 2O HPLC !U V BuB

M ane b 3601 MANEB NA NA NA HP LC - U V Hand wa sh

M ane b 3600 MANEB NA NA Cy s/EDTA HP LC - U V Patch

Mang anese 7300 E LE M E NT S b y IC P 1-4 5 - 200 H N O 3/HC lO 4 IC P !AES MC EF

Mang anese 9102 ELEMENTS on WIPES NA NA NA ICP-AES Wipe

Mang anese 7301 ELE M EN TS b y IC P (A Q UA RE G IA 1-4 5 - 200 H C l /H N O 3 ICP-AES MC EF

A SH IN G )

Mang anese 7303 E LE M EN TS by IC P (H O T 1-4 Se e Ta ble H C l /H N O 3 ICP-AES MC EF

B L O C K /H C l /H N O 3 D IG E S T IO N )

MBK 1300 KETONES I 0.01 - 0.2 1 - 10 C S2 G C !FID CCT

MDI (4,4'!methylene ! 5521 ISO C YA NA TES , M O NO M ER IC 1.0 5 - 500 rea ge nts HPLC !EC HD IM P
b isphe nyl iso c yanate )

MDI (4,4'!methylene ! 5522 ISOCYANATES 1-2 15 - 360 tryptamine HPLC !FL/EC HD IM P

b isphe nyl iso c yanate )

Me rcury 6009 MER CURY 0.15 - 0.25 2 - 100 H N O 3/H C l AAS !cold va p Ho pc alite

3/15/2003 MF!14 NIOSH Manual of Analytical Methods

 M eth Flow Ra te Vol. (L) E x tr a c ti o n A n a ly t ic a l
Chemical No. M e th od Na m e ( L /m i n ) T e c h n iq u e Sampler
min max

Mercaptans 2542 M E R C A P TA N S 0.1 - 0.2 10 - 150 H C l/D C E G C !FPD GFF/HgAc

M e sityl o xide 1301 KE TO NE S II 0.01 - 0.2 1 - 25 M e O H /C S 2 G C !FID CCT

M e sityl o xide 2553 KE TO NE S II 0.01 - 0.2 1 - 25 IP A -C S 2 G C -FID A -C M S

M eta ls in air 7300 E LE M E NT S b y IC P 1-4 var - 2000 H N O 3/HC lO 4 IC P !AES MC EF

M e talwo r k ing F luids 5524 META LWO RKING FLUIDS (MW F) ALL 1.6 - 2.0 1000 - ND D C M/MeO H/T ol Grav PTFE/CYC
CATEGO RIES MeOH

M e thanal 2016 F O R M A L D E HY D E 0.1 - 1.5 1 - 15 ac eto nitr ile HP LC - U V SG/DNPH

M e tham ido pho s 5600 ORG ANOPHO SPHORUS PESTICIDES 0.2 - 1 12 - 240 t ol/a cet G C !FPD O VS !2

M e thano l 2000 M E TH A NO L 0.02 - 0.2 1-5 H 2O/IPA G C -FID SG

M e thano l 2549 V O L A TI LE O R G A N IC C P D S 0.01 - 0.05 1-6 t h erma l TD /G C !M S TD

(Screen in g)

M e thano l 3800 ORG ANIC and INORGANIC G ASES 0.1 - 20 Inst r. d ep . NA FTIR Di r. R e a d
by EX TR ACTIV E FTIR SPE C T R O MET R Y

Me thioca rb 5601 ORG ANONITROGEN PESTICIDES 0.1 - 1 var - 480 reagent HP LC - U V OV S-2

Methomyl 5601 ORG ANONITROGEN PESTICIDES 0.1 - 1 var - 480 reagent HP LC - U V OV S-2

M e to lac hlo r 5602 CHLORINATED ORG ANONITROGEN 0.2 - 1 12 - 480 reagent G C /E C D OV S-2
H ER BIC ID ES (A IR SA M PL IN G )

M e to lac hlo r 9200 CHLORINATED ORG ANONITROGEN NA NA NA G C - EC D polyethylene

HER BICIDES (HAND WAS H) bag

M e to lac hlo r 9201 CHLORINATED ORG ANONITROGEN NA NA IPA/diazomethane G C - EC D PUF pad

HE RBIC IDES (DER M AL P ATC H))

2 !M etho xye thyl a ce tate 1451 ME THYL C ELLO SO LVE A CE TATE 0.01 - 0.2 0.2 - 20 C S2 G C !FID CCT

2 !M e tho xye thano l 1403 ALC O HO LS IV 0.01 - 0.05 6 - 50 M e O H /C H 2C l2 G C !FID CCT

M ethy l ace tate 1458 ME THYL A CE TATE 0.01 - 0.2 0.2 - 10 C S2 G C !FID CCT

M ethy l acry late 1459 ME THYL A CR YLATE 0.01 - 0.2 1-5 C S2 G C !FID CCT

M ethy l acry late 2552 ME THYL A CR YLATE 0.01 - 0.2 1-5 C S2 G C -FID A -C M S

M e thyl alco ho l 2000 M E TH A NO L 0.02 - 0.2 1-5 H 2O/IPA G C !FID SG

M e thylal 1611 METHYLAL 0.01 - 0.2 1-3 hexane G C !FID CCT

4-M eth ylb en ze ne su lfon ic 5043 p -TO LUE NE SU LFO NIC AC ID 1-3 10 - 1000 IPA/H 20 HP LC - U V GFF
ac id

N -Methyl-y-butyrolactone 1302 N - M E TH Y L -2 - PY R R O L ID I NO N E 0.05 - 0.2 0.5 - 125 C H 2C l2/M e O H G C -NP D o r FID CCT

Methyl !(n !am yl) !ketone 1301 KE TO NE S II 0.01 - 0.2 1 - 25 M e O H /C S 2 G C !FID CCT

M eth yla rso nic ac id 5022 A R S E N IC , O R G A N O ! 1-3 50 - 1000 b u ffer IC !HYAAS PTFE

M e thyl br o m ide 2520 M E T H YL B RO M I D E 0.01 - 0.1 1-5 C S2 G C !AED P C T (2 ) +d ry t u b e

Methyl cellosolve 1403 ALC O HO LS IV 0.01 - 0.05 6 - 50 M e O H /C H 2C l2 G C !FID CCT

M ethy l celloso lve a ce tate 1451 ME THYL C ELLO SO LVE A CE TATE 0.01 - 0.2 0.2 - 20 C S2 G C !FID CCT

M e thyl c hlo r ide 1001 M E T H YL C H LO R I D E 0.01 - 0.1 0.4 - 3 C H 2C l2 G C !FID 2 C C T (lg + sm )

Me thyl chloro form 1003 HYDROC ARBONS, HALOG ENATED 0.01 - 0.2 0.1 - 8 C S2 G C !FID CCT

Me thyl chloro form 2549 V O L A TI LE O R G A N IC C P D S 0.01 - 0.05 1-6 t h erma l TD /G C !M S TD

(Screen in g)

M e thyl c yanide 1606 AC ETON ITRILE 0.01 - 0.2 3 - 25 MEC l/MEO H G C !FID CCT

Methyl cyclohexane 1500 HYDROC ARBONS, BP 36 !216 °C 0.01 - 0.2 4-4 C S2 G C !FID CCT

M e thylc yc lo he xano l 1404 M E TH YL CY C LO H EX AN O L 0.01 - 0.2 1 - 15 C H 2C l2 G C !FID CCT

Methylcyclohexanone 2521 M E T H YL C Y C LO H E X A N O N E 0.01 - 0.05 1-6 a cet G C !FID Por Q

4,4 '-M eth yle ne -b is (c yc lo 5525 ISOCYANATES, TOTAL (MAP) 1-2 1 - 500 MAP HP LC /UV G F F, IM P
he xyl iso cy an ate ) (HM DI)

3/15/2003 MF!15 NIOSH Manual of Analytical Methods

 M eth Flow Ra te Vol. (L) E x tr a c ti o n A n a ly t ic a l
Chemical No. M e th od Na m e ( L /m i n ) T e c h n iq u e Sampler
min max

4,4-Methylene-bis (phenyl 5525 ISOCYANATES, TOTAL (MAP) 1-2 1 - 500 MAP HP LC /UV G F F, IM P
isoc ya na te) (M DI)

M e thyle ne c hlo r ide 1005 M E T H YL E N E C H L O R ID E 0.01 - 0.2 0.5 - 2.5 C S2 G C -FID 2 CCT

M e thyle ne c hlo r ide 2549 V O L A TI LE O R G A N IC C P D S 0.01 - 0.05 1-6 t h erma l TD /G C !M S TD

(Screen in g)

M e thyle ne c hlo r ide 3800 ORG ANIC and INORGANIC G ASES 0.1 - 20 Inst r. d ep . NA FTIR Di r. R e a d
by EX TR ACTIV E FTIR SPE C T R O MET R Y

4,4'!Methylenedianiline 5029 4,4'!M E T H YL E N ED I AN I LI N E 1-2 10 - 1000 K O H/M e O H HPLC !U V GF F/H 2SO 4

4,4 !Methylene diphenyl 5522 ISOCYANATES 1-2 15 - 360 tryptamine HPLC !FL/EC HD IM P
diisoc ya nate

Methyl ethyl ketone 2549 V O L A TI LE O R G A N IC C P D S 0.01 - 0.05 1-6 t h erma l TD /G C !M S TD

(Screen in g)

Methyl ethyl ketone 2500 M E T H YL E TH Y L K E TO N E 0.01 - 0.2 0.25 - 12 C S2 G C !FID Carbon be ads

Methyl ethyl ketone 2555 KETONES I 0.01 - 0.2 1 - 10 C S2 G C -FID A -C M S

Methyl ethyl ketone 3508 M E T H YL E TH Y L K E TO N E P E R O X ID E 0.5 - 0.2 52 - 520 reagent VIS IM P

p er o xide

5 !Methyl !3 !heptanone 1301 KE TO NE S II 0.01 - 0.2 1 - 25 M e O H /C S 2 G C !FID CCT

5-Methyl-3-heptanone 2553 KE TO NE S II 0.01 - 0.2 1 - 25 IP A -C S 2 G C -FID A -C M S

M eth yl h ipp ur ic a cid 8301 HIP PU RIC an d M ETH YL H IPP UR IC NA NA Et a c HP LC - U V NA

ACID in urine

M e thyl io dide 1014 M E T H YL IO D I D E 0.01 - 1.0 15 - 50 t ol G C !FID CCT

M ethy l isoam yl ac etate 1450 ESTERS I 0.01 - 0.2 1 - 10 C S2 G C !FID CCT

M e thyl iso butyl c ar binol 1402 ALC O HO LS III 0.01 - 0.2 1 - 10 IP A /C S 2 G C !FID CCT

M e thyl iso butyl c ar binol 1405 ALCOHO LS COM BINED 0.01 - 0.2 1 - 10 IP A -C S 2 G C -FID CCT

Methyl isobutyl ketone 2549 V O L A TI LE O R G A N IC C P D S 0.01 - 0.05 1-6 t h erma l TD /G C !M S TD

(Screen in g)

Methyl isobutyl ketone 1300 KETONES I 0.01 - 0.2 1 - 10 C S2 G C !FID CCT

Methyl isobutyl ketone 2555 KETONES I 0.01 - 0.2 1 - 10 C S2 G C -FID A -C M S

M e thyl me r c aptan 2542 M E R C A P TA N S 0.1 - 0.2 10 - 150 H C l/D C E G C !FPD GFF/HgAc

M ethy l me tha cryla te 2537 ME THYL a nd ETH YL M ETHA CR YLATE 0.01 - 0.05 1-8 C S2 G C !FID XAD

M e thyl par athio n 5600 ORG ANOPHO SPHORUS PESTICIDES 0.2 - 1 12 - 240 t ol/a cet G C !FPD O VS !2

M e thyl phe no l 2549 V O L A TI LE O R G A N IC C P D S 0.01 - 0.05 1-6 t h erma l TD /G C !M S TD

(Screen in g)

N -methyl-2-pyrrolidinone 1302 N - M E TH Y L -2 - PY R R O L ID I NO N E 0.05 - 0.2 0.5 - 125 C H 2C l2/M e O H G C -NP D o r FID CCT

"!Methyl styrene 1501 HY DR O C AR BO NS , AR O M ATIC 0.01 - 0.2 1 - 30 C S2 G C !FID CCT

$ -Methylstyrene 1501 HY DR O C AR BO NS , AR O M ATIC 0.01 - 0.2 1 - 30 C S2 G C -FID CCT

M eth yl tert !butyl e ther 1615 METH YL tert !BUTYL ETHER 0.1 - 0.2 2 - 96 C S2 G C !FID 2 CC T ( lg )

M e thyltin c hlo r ide 5526 METHYLTIN CHLORIDES 0.25 - 1 15 - 75 AAA GC-FPD O VS

M e vinphos 5600 ORG ANOPHO SPHORUS PESTICIDES 0.2 - 1.0 12 - 240 t ol/a cet G C !FPD O VS !2

M inera l spirits 1550 NAPHTHAS 0.01 - 0.2 1.3 - 20 C S2 G C !FID CCT

M o lybde num 7300 E LE M E NT S b y IC P 1-4 5 - 67 H N O 3/HC lO 4 IC P !AES MC EF

M o lybde num 7301 EL EM EN TS b y IC P (A qu a R eg ia 1-4 5 - 67 H C l /H N O 3 ICP-AES MC EF

Ashin g)

M o lybde num 7303 EL EM EN TS b y IC P (H ot B loc k/H C l/ 1-4 Se e Ta ble H C l /H N O 3 ICP-AES MC EF

H N O 3 Digestion)

M o lybde num 9102 ELEMENTS on WIPES NA NA NA ICP-AES Wipe

M o no c r o to pho s 5600 ORG ANOPHO SPHORUS PESTICIDES 0.2 - 1 12 - 240 t ol/a cet G C !FPD O VS !2

3/15/2003 MF!16 NIOSH Manual of Analytical Methods

 M eth Flow Ra te Vol. (L) E x tr a c ti o n A n a ly t ic a l
Chemical No. M e th od Na m e ( L /m i n ) T e c h n iq u e Sampler
min max

Monom ethylaniline 3511 M O N O M E T HY L AN I LI N E 0.2 - 1.0 11 - 100 N a OH G C !FID BuB /H 2SO 4

Monom ethylhydrazine 3510 M O N O M E T HY L H YD R A Z IN E 0.5 - 1.5 3 - 20 P M A /H C l VIS B u B/H C l

M yc o bac te rium 0900 M YC O BA C TER IUM TUB ER C ULO SIS $4 va r ies PCR reagent PTFE

Nap htha (coal tar) 1550 NAPHTHAS 0.01 - 0.2 1.3 - 20 C S2 G C !FID CCT

Naphthalene 1501 HY DR O C AR BO NS , AR O M ATIC 0.01 - 1.0 100 - 200 C S2 G C !FID CCT

Naphthalene 5506 PO LYN UC LEA R A RO M ATIC 2.0 200 - 1000 ac eto nitr ile HPLC !FL/U V P T F E & X A D !2
HYDR OC ARBO NS by H PLC

Naphthalene 5515 PO LYN UC LEA R A RO M ATIC 2.0 200 - 1000 va r ies G C -FID P T F E & X A D !2
HYDROC ARBONS

1,5-Naphthalene 5525 ISOCYANATES, TOTAL (MAP) 1-2 1 - 500 MAP HP LC - U V G F F, IM P

diiso cy an ate (ND I)

N a phthylamine s 5518 NAPHTHYLAMINES 0.2 - 0.8 30 - 100 acetic a /IPA G C !FID GFF & SG

N eo dym ium 7303 EL EM EN TS b y IC P (H ot B loc k/H C l/ 1-4 Se e Ta ble H C l /H N O 3 ICP-AES MC EF

H N O 3 Digestion)

N i c ke l 7300 E LE M E NT S b y IC P 1 !4 25 - 1000 H N O 3/HC lO 4 IC P !AES MC EF

N i c ke l 7301 EL EM EN TS b y IC P (A qu a R eg ia 1-4 5 - 1000 H C l /H N O 3 ICP-AES MC EF

Ashin g)

N i c ke l 7303 EL EM EN TS b y IC P (H ot B loc k/H C l/ 1-4 Se e Ta ble H C l /H N O 3 ICP-AES MC EF

H N O 3 Digestion)

N i c ke l 9102 ELEMENTS on WIPES NA NA NA ICP-AES Wipe

Nickel carbonyl 6007 NICKEL CARBONYL 0.05 - 0.2 7 - 80 HNO3 G FAAS C C T (lo w N i)

Nicotine 2544 N I C O TI N E 1.0 60 - 400 Et Ac G C !NPD X A D !2

Nicotine 2551 N I C O TI N E 0.1 - 1.0 0.5 - 600 ethy l ace tate GC-NPD XA D-4
2-
Nit ric ac id 7903 AC IDS , INO RG AN IC 0.2 - 0.5 3 - 100 H C O 3-/C O 3 IC S G ( w a s h ed )

N i tr ic o xide 6014 N I TR IC O X I D E & N IT R O G E N D IO X I D E 0.025 1.5 - 6 reagent VIS M S w / T EA &

o x id i ze r

p !Nitroaniline 5033 p !N I TR O A N IL IN E 1-3 20 IPA HPLC !U V MC EF

Nitrobenzene 2005 N I TR O A R O M A T IC C O M P O U N D S 0.01 - 1 10 - 150 MeOH G C !FID SG

Nitrobenzene 2017 A N IL IN E , o - TO L U ID I NE , A N D 0.2 5 - 50 et h a nol G C -FID GFF + SG

N I TR O B E N Z EN E

N i tr o be nzo l 2017 A N IL IN E , o - TO L U ID I NE , A N D 0.2 5 - 50 et h a nol G C -FID GFF + SG

N I TR O B E N Z EN E

p !Nitrochlorobenzene 2005 N I TR O A R O M A T IC C O M P O U N D S 0.01 - 1 1 - 150 MeOH G C !FID SG

Nitroethane 2526 N I TR O E T H AN E 0.01 - 0.05 1.5 - 3 Et Ac G C !FID 2 X A D !2

N i tr o ge n dio xide 6014 N I TR IC O X I D E & N IT R O G E N D IO X I D E 0.025 - 0.2 1.5 - 6 reagent VIS MS w/TEA

N i tr o ge n dio xide 6700 N I TR O G E N D IO X I D E NA NA reagent VIS Diffusive

N i tr o ge n pe r o xide 6700 N I TR O G E N D IO X I D E NA NA reagent VIS Diffusive

Nit ro gly ce rin 2507 N ITR O G LY C ER IN & ETH YL EN E G LY C O L 0.2 - 1.0 3 - 100 et h a nol G C !E C D T e n a x!G C
DINITRA TE

Nitromethane 2527 N I TR O M E T H A N E 0.01 - 0.05 1.2 - 3 Et Ac G C !FPD Chrom 106

2 !Nitropropane 2528 2 !N I TR O P R O P A N E 0.01 - 0.05 0.1 - 2 Et Ac G C !FID Chrom 106

1-Nitropyrene 2560 1-NITROPYRENE in DIESEL 1.0 - 2.0 480 - 960 T ol G C /N C D GFF

PARTICULATES

N i tr o samine s 2522 NITROSAMINES 0.2 - 2.0 15 - 1000 M e O H /C H 2C l2 G C !TEA T D tu b e

o - ,m - , p -Nitrotoluene 2005 N I TR O A R O M A T IC C O M P O U N D S 0.01 - 0.2 1 - 30 MeOH G C !FID SG

N i tr o us o xide 3800 ORG ANIC and INORGANIC G ASES 0.1 - 20 Inst r. d ep . NA FTIR Di r. R e a d
by EX TR ACTIV E FTIR SPE C T R O MET R Y

3/15/2003 MF!17 NIOSH Manual of Analytical Methods

 M eth Flow Ra te Vol. (L) E x tr a c ti o n A n a ly t ic a l
Chemical No. M e th od Na m e ( L /m i n ) T e c h n iq u e Sampler
min max

Nitr o us o xide 6600 N I TR O U S O X ID E NA 80% vol NA IR air bag

n-Nonane 1500 HYDROC ARBONS, BP 36-216 oC 0.01 - 0.2 4-4 C S2 G C -FID CCT

NMP 1302 N-Methyl-2-Pyrrolidinone 0.05 - 0.2 0.5 - 125 C H 2C l2/M e O H GC-FID/NPD CCT

Nuisance dusts 0500 PARTICU LATES N.O.R . 1-2 7 - 133 NA G R AV P VC

n !Octane 2549 V O L A TI LE O R G A N IC C P D S 0.01 - 0.05 1-6 t h erma l TD /G C !M S TD

(Screen in g)

n !Octane 1500 HYDROC ARBONS, BP 36 !216 °C 0.01 - 0.2 4-4 C S2 G C !FID CCT

Oc tam ethylcy clotetra ! 2549 V O L A TI LE O R G A N IC C P D S 0.01 - 0.05 1-6 t h erma l TD /G C !M S TD

siloxane (Screen in g)

1 !Oc tane thio l 2510 1 !O C TA N ETH IO L 0.01 - 0.2 1 - 15 a cet G C !FPD Te na x G C

O il m ist (m ine ra l) 5026 OIL MIST, MINER AL 1-3 20 - 500 C C l4 IR PVC or MCE

O r gano nitro ge n pe sticides 5601 ORG ANONITROGEN PESTICIDES 0.1 - 1 varies-480 reagent HP LC - U V OV S-2

O r gano pho spho r us 5600 ORG ANOPHO SPHORUS PESTICIDES 0.2 - 1 12 - 240 t ol/a cet G C !FPD O VS !2
Pestic ide s

Oxamyl 5601 ORG ANONITROGEN PESTICIDES 0.1 - 1 var - 480 reagent HP LC , U V OV S-2

O xyge n 6601 OXYG EN NA 1 - NA NA Sens or po rta ble

PA C 5800 POLY AROM ATIC COMPO UNDS, 1-2 5 - 1000 hexane FI-FL PTFE + X AD -2
TOTAL (PACs)

Palladium 7303 EL EM EN TS b y IC P (H ot B loc k/H C l/ 1-4 Se e Ta ble H C l /H N O 3 ICP-AES MC EF

H N O 3 Digestion)

Par aquat 5003 PARAQUAT 1-4 40 - 1000 H 2O HPLC !U V PTFE

Par athio n 5600 ORG ANOPHO SPHORUS PESTICIDES 0.2 - 1.0 12 - 240 t ol/a cet G C !FPD O VS !2

Par tic ulate s N . O. R. 0500 PARTICU LATES N.O.R ., TO T AL 1-2 7 - 133 NA G R AV P VC

Par tic ulate s N . O. R. 0600 PARTICU LATES, N.O .R, RESPIRAB LE 1.7, 2.2, 20 - 400 NA Grav. C Y C & P VC
2.5

Pentachlorobenzene 5517 POLYCHLORO BENZENES 0.01 - 0.2 3 - 12 hexane G C !E C D P T F E & X A D !2

Pentachloroethane 2517 P E N TA C H L O R O E TH A N E 0.01 - 0.2 1 - 10 hexane G C !E C D Por R

Pe ntac hlo r o phe no l 5512 P EN TA C HL OR O PH EN O L 0.5 - 1.0 48 - 480 MeOH HPLC !U V MCEF & BuB

Pentamidine 5032 PEN TAM IDINE ISETH ION ATE 1-2 50 - 1500 rea ge nts HPLC/FL P VC / o p a q u e

n !Pentane 2549 V O L A TI LE O R G A N IC C P D S 0.01 - 0.05 1-6 t h erma l TD /G C !M S TD

(Screen in g)

n !Pentane 1500 HYDROC ARBONS, BP 36 !216 °C 0.01 - 0.2 4-4 C S2 G C !FID CCT

2 !Pentanone 1300 KETONES I 0.01 - 2.0 1 - 10 C S2 G C !FID CCT

2-Pentanone 2555 KETONES I 0.01 - 0.2 1 - 10 C S2 G C -FID A -C M S

Perchloroethylene 3704 PE RC HL O RO ETH YL EN E (p or t G C ) in 0.02 - 5 < 80% ca p NA G C (po rt)-PID air bag
exha led bre ath a nd a ir

Perchloroethylene 2549 V O L A TI LE O R G A N IC C P D S 0.01 - 0.05 1-6 t h erma l TD /G C !M S TD

(Screen in g)

Pe stic ide s 5600 ORG ANOPHO SPHORUS PESTICIDES 0.2 - 1 12 - 240 t ol/a cet G C !FPD O VS !2

Pe stic ide s 5601 ORG ANONITROGEN PESTICIDES 0.1 - 1 var - 480 reagent HP LC - U V OV S-2

Pe tro leum e the r/naphtha 1550 NAPHTHAS 0.01 - 0.2 1.3 - 20 C S2 G C !FID CCT

Phenanthrene 5506 PO LYN UC LEA R A RO M ATIC 2.0 200 - 1000 ac eto nitr ile HPLC !FL/U V P T F E & X A D !2
HYDR OC ARBO NS by H PLC

Phenanthrene 5515 PO LYN UC LEA R A RO M ATIC 2.0 200 - 1000 va r ies G C -FID P T F E & X A D !2
HYDROC ARBONS

Phe no l 2549 V O L A TI LE O R G A N IC C P D S 0.01 - 0.05 1-6 t h erma l TD /G C !M S TD

(Screen in g)

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 M eth Flow Ra te Vol. (L) E x tr a c ti o n A n a ly t ic a l
Chemical No. M e th od Na m e ( L /m i n ) T e c h n iq u e Sampler
min max

Phe no l 2546 C R ES O LS an d P HE NO L 0.01 - 0.1 1 - 24 MeOH G C !FID X A D !7

Phe nyl e the r 1617 PHENYL ETHER 0.01 - 0.2 1 - 50 C S2 G C !FID CCT

Phe nyl e the r!diphenyl 2013 PHENYL ETHER !DIPHENYL MIXT U R E 0.01 - 0.2 1 - 40 bz G C !FID SG
mixture

Phe nyl glyc idyl ethe r 1619 PHENYL GLYCIDYL ETHER 0.01 - 1 80 - 150 C S2 G C !FID CCT

Phenylhydrazine 3518 P H E N YL H Y DR A Z IN E 0.2 - 1.0 25 - 120 PMA VIS B u B/H C l

Pho rate 5600 ORG ANOPHO SPHORUS PESTICIDES 0.2 - 1 12 - 240 t ol/a cet G C !FPD O VS !2

Phosdrin (mevinphos) 5600 ORG ANOPHO SPHORUS PESTICIDES 0.2 - 1 12 - 480 t ol/a cet G C !FPD O VS !2

Phosphine 6002 P H O S P H IN E 0.01 - 0.2 1 - 16 reagent VIS S G / H g( C N )2

- 2-
Ph os ph or ic a cid 7903 AC IDS , INO RG AN IC 0.2 - 0.5 3 - 100 H C O 3 /C O 3 IC S G ( w a s h ed )

Pho spho rus 7300 E LE M E NT S b y IC P 1-4 50 - 2000 H N O 3/HC lO 4 IC P !AES MC EF

Pho spho rus 7905 PHOSPHOR U S 0.01 - 0.2 5 - 100 xylene G C !FPD Te na x G C

Pho spho rus 7301 EL EM EN TS b y IC P (A qu a R eg ia 1-4 25 - 2000 H C l /H N O 3 ICP-AES MC EF

Ashin g)

Pho spho rus 7303 EL EM EN TS b y IC P (H ot B loc k/H C l/ 1-4 Se e Ta ble H C l /H N O 3 ICP-AES MC EF

H N O 3 Digestion)

Pho spho rus 9102 ELEMENTS on WIPES NA NA NA ICP-AES Wipe

Pho spho rus tr ic hlor ide 6402 P H O S P H O R U S T R IC H L O R ID E 0.05 - 0.2 11 - 100 rea ge nts VIS BuB /H 2O

Pinene 1552 TERPENES 0.01 - 0.2 2 - 30 C S2 G C !FID CCT

Pinene 2549 V O L A TI LE O R G A N IC C P D S 0.01 - 0.05 1-6 t h erma l TD /G C !M S TD

(Screen in g)

Pla tinum 7300 E LE M E NT S b y IC P 1-4 13 - 2000 H N O 3/HC lO 4 IC P !AES MC EF

PA H 5506 PO LYN UC LEA R A RO M ATIC 2.0 200 - 1000 va r ies HPLC !FL/U V P T F E & X A D !2
HYDROC ARBONS

Poly ac rylate 5035 SUPER ABSORBENT POLYMER 1-2 50 - 1500 C u (Ac)2 IC P or AAS P VC

PACs 5800 PO LYC YC LIC AR O M ATIC 1-2 5 - 1000 hexane FI-FL

COM POU NDS, TOTAL

Platinum 7303 EL EM EN TS b y IC P (H ot B loc k/H C l/ 1-4 Se e Ta ble H C l /H N O 3 ICP-AES MC EF

H N O 3 Digestion)

Po lyc hlo ro bip he ny l 5503 POLY CH LORO BIPHENY LS 0.05 - 0.2 1 - 50 hexane G C !E C D G FF & F lor isil
(42 % & 5 4% C l)

Po tassium 7301 EL EM EN TS b y IC P (A qu a R eg ia 1-4 5 - 1000 H C l /H N O 3 ICP-AES MC EF

Ashin g)

Po tassium 7303 EL EM EN TS b y IC P (H ot B loc k/H C l/ 1-4 Se e Ta ble H C l /H N O 3 ICP-AES MC EF

H N O 3 Digestion)

Po tassium hydr o xide 7401 ALKA LINE DU STS 1-4 70 - 1000 HCl t it ra t ion PTFE

Progesterone 5044 E S TR O G E N I C C O M P O U N D S 1 150 - 1000 M eth HP LC - U V PTFE

Propazine 8315 TR IAZ INE HE RB IC IDE S a nd the ir NA NA NA GC-M SD Urine

METABOLITES

Pr o pham 5601 ORG ANONITROGEN PESTICIDES 0.1 - 1 var - 480 reagent HP LC , U V OV S-2

Pr o pio nalde hyde 2539 A L D EH Y D E S, SC R E E N IN G 0.01 - 0.05 5-5 t ol G C !F ID /M S X A D !2 /H M P

Pr o pio nalde hyde 2018 ALIPHATIC ALDEHYDES 0.1 - 1.5 1 - 15 ACN HP LC - U V SG-DNPH

Pr o po xur 5601 ORG ANONITROGEN PESTICIDES 0.1 - 1 var - 480 reagent HP LC , U V OV S-2

n !Prop yl ac etate 1450 ESTERS I 0.01 - 0.2 1 - 10 C S2 G C !FID CCT

n !Pr o pyl alc o ho l 1401 ALC O HO LS II 0.01 - 0.2 1 - 10 IP A /C S 2 G C !FID CCT

n- Pro pyl alco ho l 1405 ALCOHO LS COM BINED 0.01 - 0.2 1 - 10 IP A -C S 2 G C -FID CCT

Pr o pyle ne dic hlor ide 1013 P R O P Y LE N E D IC H L O R ID E 0.01 - 0.2 0.1 - 3.5 a cet /cy ch ex G C !E C N PCT

3/15/2003 MF!19 NIOSH Manual of Analytical Methods

 M eth Flow Ra te Vol. (L) E x tr a c ti o n A n a ly t ic a l
Chemical No. M e th od Na m e ( L /m i n ) T e c h n iq u e Sampler
min max

Pro pyle ne glyc o l 5523 GLYC OLS 0.5 - 2 5 - 60 MeOH G C !FID O VS !7

Pr o pyle ne glyc o l 2554 GLYCOL ETHER S 0.1 - 0.2 3 - 25 M e C l2/Me th G C -FID A-747
m o no m e thyl e the r

Pr o pyle ne glyc o l 2554 GLYCOL ETHERS 0.1 - 0.2 3 - 25 M e C l2/Me th G C -FID A-747
mo nom ethy l ethe r ac etate

Pr o pyle ne o xide 1612 P R O P Y LE N E O X ID E 0.01 - 0.2 0.5 - 5 C S2 G C !FID CCT

Pyrene 5506 PO LYN UC LEA R A RO M ATIC 2.0 200 - 1000 ac eto nitr ile HPLC !FL/U V P T F E & X A D !2
HYDR OC ARBO NS by H PLC

Pyrene 5515 PO LYN UC LEA R A RO M ATIC 2.0 200 - 1000 va r ies G C !FID P T F E & X A D !2
HYDROCARBONS

Pyr e thr um 5008 PYRETHUM 1-4 20 - 400 C H 3C N HPLC !U V GFF

Pyridine 1613 P Y R ID I NE 0.01 - 1.0 18 - 150 C H 2C l2 G C !FID CCT

R eso rc ino l 5701 R ES O RC IN O L 0.2 - 1 5 - 160 MeOH G C -FID OV S-7

Rib av irin 5027 RIB AV IRIN 1-4 5 - 1000 H 2SO 4 HPLC !U V GFF

R onne l 5600 ORG ANOPHO SPHORUS PESTICIDES 0.2 - 1 12 - 60 t ol/a cet G C !FPD O VS !2

Rotenone 5007 ROTENONE 1-4 8 - 400 C H 3C N HPLC !U V PTFE

Rubber solvent 1550 NAPHTHAS 0.01 - 0.2 1.3 - 20 C S2 G C !FID CCT

S e le nium 7300 E LE M E NT S b y IC P 1-4 5 - 2000 H N O 3/HC lO 4 IC P !AES MC EF

S e le nium 7301 EL EM EN TS b y IC P (A qu a R eg ia 1-4 13 - 2000 H C l /H N O 3 ICP-AES MC EF

Ashin g)

S e le nium 7303 EL EM EN TS b y IC P (H ot B loc k/H C l/ 1-4 Se e Ta ble H C l /H N O 3 ICP-AES MC EF

H N O 3 Digestion)

S e le nium 9102 ELEMENTS on WIPES NA NA NA ICP-AES Wipe

S ilic a, amo rpho us 7501 SILICA, AMOR PHOUS 1.7 or 2 .2 50 - 400 ash XR D PVC (total)
PVC&C YC

Silica, crystalline 7500 SILICA, CRYSTALLINE, by XR D 1.7, 2.2, 400 - 1000 a s h or T HF XR D C Y C & P VC
2.5

Silica, crystalline 7601 S IL IC A , C R Y ST A LL IN E 1.7, 2.2, 400 - 800 H 3PO 4/HF VIS CYC & MC E or
2.5 P VC

Silica, crystalline 7602 SILICA, CRYSTALLINE (IR ) 1.7, 2.2, 400 - 800 ash IR CY C & M C E o r
2.5 P VC

S ilic o n dio xide 7500 S IL IC A , C R Y ST A LL IN E , b y X R D. 1.7, 2.2, 400 - 1000 a s h or T HF XR D C Y C & P VC

2.5

Silica in coal mine dust 7603 QUA RTZ in coal mine dust 1.7, 2.2, 300 - 1000 ash IR C Y C & P VC
2.5

S ilve r 7300 E LE M E NT S b y IC P 1-4 250 - 2000 H N O 3+ IC P !AES MC EF

S ilve r 7301 EL EM EN TS b y IC P (A qu a R eg ia 1-4 250 - 2000 H C l /H N O 3 ICP-AES MC EF

Ashin g)

S ilve r 9102 ELEMENTS on WIPES NA NA NA ICP-AES Wipe

Simazine 5602 CHLORINATED ORG ANONITROGEN 0.2 - 1 12 - 480 reagent G C /E C D OV S-2

H ER BIC ID ES (A IR SA M PL IN G )

Simazine 9200 CHLORINATED ORG ANONITROGEN NA NA NA G C - EC D polyethylene

HER BICIDES (HAND WAS H) bag

Simazine 9201 CHLORINATED ORG ANONITROGEN NA NA IPA/diazomethane G C - EC D PUF pad

HE RBIC IDES (DER M AL P ATC H))

S o dium 7303 EL EM EN TS b y IC P (H ot B loc k/H C l/ 1-4 Se e Ta ble H C l /H N O 3 ICP-AES MC EF

H N O 3 Digestion)

S o dium 7902 FLUORIDES, aerosol & ga s 1-2 12 - 800 N a OH ISE MCEF& pad
hexa fluoro !alum inate w / N a2C O 3

3/15/2003 MF!20 NIOSH Manual of Analytical Methods

 M eth Flow Ra te Vol. (L) E x tr a c ti o n A n a ly t ic a l
Chemical No. M e th od Na m e ( L /m i n ) T e c h n iq u e Sampler
min max

S odium 7906 FLU O RID ES by IC 1-2 120 - 800 N a OH IC MCEF& pad

hexa fluoro !alum inate w / N a2C O 3

S o dium hydr o xide 7401 ALKA LINE DU STS 1-4 70 - 1000 HCl T it ra t ion PTFE

Stibine 6008 S T IB IN E 0.01 - 0.2 4 - 50 HCl VIS S G w /H g C l2

Stoddard solvent 1550 NAPHTHAS 0.01 - 0.2 1.3 - 20 C S2 G C !FID CCT

S t ro ntium 7301 EL EM EN TS b y IC P (A qu a R eg ia 1-4 10 - 1000 H C l /H N O 3 ICP-AES MC EF

Ashin g)

S t ro ntium 7303 EL EM EN TS b y IC P (H ot B loc k/H C l/ 1-4 Se e Ta ble H C l /H N O 3 ICP-AES MC EF

H N O 3 Digestion)

S t ro ntium 9102 ELEMENTS on WIPES NA NA NA ICP-AES Wipe

Strychnine 5016 S T RY C H N IN E 1-3 70 - 1000 rea ge nts HPLC !U V GFF

Styrene 1501 HY DR O C AR BO NS , AR O M ATIC 0.01 - 1.0 1 - 14 C S2 G C !FID CCT

Styrene 3800 ORG ANIC and INORGANIC G ASES 0.1 - 20 Inst r. D ep . NA FTIR Di r. R e a d
by EX TR ACTIV E FTIR SPE C T R O MET R Y

S ulfur dioxide 6004 S U LF U R D IO X I D E 0.5 - 1.5 4 - 200 H C O 3-/C O 32- IC MCEF& pad
w / N a2C O 3

S ulfur he xafluo ride 6602 S U LF U R H EX A F LU O R ID E 0.01 - 0.05 80% vol NA G C !E C D air bag
- 2-
Su lfur ic a cid 7903 AC IDS , INO RG AN IC 0.2 - 0.5 3 - 100 H C O 3 /C O 3 IC SG(washed)

S ulfuryl fluo r ide 6012 S U LF U R Y L F L UO R I D E 0.05 - 0.1 1.3 - 10 N a OH IC CC T ( lg )

S ulpr o fo s 5600 ORG ANOPHO SPHORUS PESTICIDES 0.2 - 1 12 - 240 t ol/a cet G C !FPD O VS !2

S upe r abso rbe nt po lymer 5035 SUPER ABSORBENT POLYMER 1-3 50 - 1500 C u (Ac)2 IC P or AAS P VC

Simazine 8315 TR IAZ INE HE RB IC IDE S a nd the ir NA NA NA GC-M SD Urine

METABOLITES

2,4,5 !T 5001 2,4 !D an d 2,4,5 !T 1-3 15 - 200 MeOH HPLC !U V GFF

TB 0900 MYCO BACTERIUM TUBERCULOSIS, $4 va r ies reagent PCR PTFE

A IR B O R N E

T ellurium 7300 E LE M E NT S b y IC P 1-4 25 - 2000 HNO3 IC P !AES MC EF

T ellurium 7301 EL EM EN TS b y IC P (A qu a R eg ia 1-4 25 - 2000 H C l /H N O 3 ICP-AES MC EF

Ashin g)

T ellurium 7303 EL EM EN TS b y IC P (H ot B loc k/H C l/ 1-4 Se e Ta ble H C l /H N O 3 ICP-AES MC EF

H N O 3 Digestion)

T ellurium 9102 ELEMENTS on WIPES NA NA NA ICP-AES Wipe

T erbufo s 5600 ORG ANOPHO SPHORUS PESTICIDES 0.2 - 1 12 - 240 t ol/a cet G C !FID O VS !2

T erpe ne s 1552 TERPENES 0.01 - 2 2 - 30 C S2 G C !FID CCT

o !Terphenyl 5021 o !TERPHENYL 1-3 2 - 30 C S2 G C !FID PTFE

1,1,2,2 !Te tra bro m o 2003 1,1,2,2 !T E TR A B R O M O E T H AN E 0.2 - 1.0 50 - 100 T HF G C !FID SG
ethane

Te tra bu tylt in 5504 O R G A N O T IN C O M P O U N D S 1 - 1.5 50 - 500 aaa HP LC /G FAAS G F F & X A D !2

1,2,4,5 !Tetrachlorobenzene 5517 POLYCHLORO BENZENES 0.01 - 0.2 3 - 12 hexane G C !E C D P T F E & X A D !2

1,1,2,2 !Tetrach loro ! 1016 1,1,2,2 !TETRACHLORO !2,2 ! 0.01 -0.035 0.5 - 2 C S2 G C !FID CCT
2,2-difluoroethane DIFLUOROETHANE &
1,1,2,2 !TETR ACHLOR O !1,2 !
D I FL U O R O E TH A N E

1,1,1,2 !Tetrach loro !1,2 -d iflu 1016 1,1,2,2 !TETRACHLORO !2,2 ! 0.01 -0.035 0.5 - 2 C S2 G C !FID CCT
oroethane DIFLUOROETHANE &
1,1,2,2 !TETR ACHLOR O !1,2 !
D I FL U O R O E TH A N E

1,1,2,2 !Tetrachloroethane 1019 1,1,2,2 !T E TR A C H L O R O E TH A N E 0.01 - 0.2 3 - 30 C S2 G C !FID PCT

1,1,2,2-Tetrachloroethane 2562 1 , 1, 2 ,2 - TE T RA C H L O R O E TH A N E 0.01 - 0.2 3 - 30 C S2 G C -FID A -C M S

3/15/2003 MF!21 NIOSH Manual of Analytical Methods

 M eth Flow Ra te Vol. (L) E x tr a c ti o n A n a ly t ic a l
Chemical No. M e th od Na m e ( L /m i n ) T e c h n iq u e Sampler
min max

Tetrachloroethylene 1003 HYDROC ARBONS, HALOG ENATED 0.01 - 0.2 1 - 40 C S2 G C -FID CCT

Tetrachloroethylene 3704 PE RC HL O RO ETH YL EN E (p or t G C ) in 0.1 - 1 < 80% ca p NA Po rt G C -PID air bag

exha led bre ath a nd a ir

T etr ae thyle ne glyc o l 5523 GLYC OLS 0.5 - 2 5 - 60 MeOH G C !FID O VS !7

T etr ae thyl lead 2533 TETR AETHYL LEAD (as Pb ) 0.01 - 1.0 30 - 200 pentane G C !PID X A D !2

Tetra ethy l pyro ph osp ha te 2504 TETRA ETHY L PYRO PHO SPH ATE 0.01 - 0.2 20 - 48 toluene G C !FPD 2 Chrom 102

Tetrafluoroethylene 3800 ORG ANIC and INORGANIC G ASES 0.1 - 20 Inst r. d ep . NA FTIR Di r. R e a d
by EX TR ACTIV E FTIR SPE C T R O MET R Y

T etr ahydro furan 1609 TETR AHYDR OFU R AN 0.01 - 0.2 1-9 C S2 G C !FID CCT

T etr ahydro furan 3800 ORG ANIC and INORGANIC G ASES 0.1 - 20 Inst r. d ep . NA FTIR Di r. R e a d
by EX TR ACTIV E FTIR SPE C T R O MET R Y

Te tra kis (hy dr ox ym eth yl) 5046 TETRKIS(HYDR OX YM ETHYL) 1 - 1.7 1 - 400 ACN HP LC - U V GFF
p ho spho nium c hlo ride P H O S P H O N IU M C H L O R ID E

T etr am e thyl lead 2534 TETRAMETHYL LEAD (as P b ) 0.01 - 0.2 15 - 100 pentane G C !PID X A D !2

T etr am e thyl thio ur e a 3505 TETRAMETHYL THIOUREA 0.2 - 1.0 50 - 250 rea ge nts VIS IMP /H 2O

Tetranitromethane 3513 T E TR A N IT R O M E TH A N E 0.5 - 1.0 20 - 250 ! G C !FID I M P /E t A c

T hallium 7300 E LE M E NT S b y IC P 1-4 25 - 2000 H N O 3/HC lO 4 IC P !AES MC EF

T hallium 7310 EL EM EN TS b y IC P (A qu a R eg ia 1-4 25 - 2000 H C l /H N O 3 ICP-AES MC EF

Ashin g)

T hallium 7303 EL EM EN TS b y IC P (H ot B loc k/H C l/ 1-4 Se e Ta ble H C l /H N O 3 ICP-AES MC EF

H N O 3 Digestion)

Thiobe nca rb 5601 ORG ANONITROGEN PESTICIDES 0.1 - 1 var - 480 reagent HP LC , U V OV S-2

Thiophenate-methyl 9205 CAPTAN and THIOPHENATE-METHYL NA NA IP A /A C N HP LC - U V Patch

o n D E RM A L P A TC H

Thiophenate-methyl 9202 CAPTAN and THIOPHENATE-METHYL NA NA NA HP LC - U V Hand wa sh

in Hand Rinse

Thiophenate-methyl 5606 THIO PH EN ATE -M ETH YL in AIR 0.1 - 1.0 20 - 480 IP A /A C N HP LC - U V QFF/SST

T hir am 5005 THIRAM 1-4 10 - 400 C H 3C N HPLC !U V PTFE

Tin 7301 EL EM EN TS b y IC P (A qu a R eg ia 1-4 5 - 1000 H C l /H N O 3 ICP-AES MC EF

Ashin g)

Tin 7303 EL EM EN TS b y IC P (H ot B loc k/H C l/ 1-4 Se e Ta ble H C l /H N O 3 ICP-AES MC EF

H N O 3 Digestion)

Tin, organic compds as Sn 5504 ORG ANOTIN CPDS. (as Sn) 1 - 1.5 50 - 500 a c etic a /C H 3C N HP LC /G FAAS G F F & X A D !2

T itanium 7300 E LE M E NT S b y IC P 1-4 5 - 100 H N O 3/HC lO 4 IC P !AES MC EF

T itanium 7301 EL EM EN TS b y IC P (A qu a R eg ia 1-4 5 - 100 H C l /H N O 3 ICP-AES MC EF

Ashin g)

T itanium 7303 EL EM EN TS b y IC P (H ot B loc k/H C l/ 1-4 Se e Ta ble H C l /H N O 3 ICP-AES MC EF

H N O 3 Digestion)

Toluene 2549 V O L A TI LE O R G A N IC C P D S 0.01 - 0.05 1-6 t h erma l TD /G C !M S TD

(Screen in g)

Toluene 4000 TOLU ENE (Diffusive sam pler) NA 15 min-8h C S2 G C !FID Diffusive

Toluene 1500 HYDROC ARBONS, BP 36 !216 °C 0.01 - 0.2 2-8 C S2 G C !FID CCT

Toluene 1501 HY DR O C AR BO NS , AR O M ATIC 0.01 - 0.2 1-8 C S2 G C !FID CCT

Toluene 3800 ORG ANIC and INORGANIC G ASES 0.1 - 20 Inst r. d ep . NA FTIR Di r. R e a d
by EX TR ACTIV E FTIR SPE C T R O MET R Y

2,4 & 2,6 !Toluenediamine 5516 2,4 ! & 2,6 !T O L UE N E D IA M I N E 1.0 30 - 500 a ce ty la te /M e O H HPLC !U V IM P

Toluene !2,4 !diisoc ya nate 2535 T O L UE N E !2,4 !DIISO CY ANA TE 0.2 - 1.0 2 - 170 MeOH HPLC !U V GW coated

Toluene !2,4 !diisoc ya nate 5521 ISO C YA NA TES , M O NO M ER IC 1.0 5 - 500 a ce ty la te /M e O H HPLC !EC HD IM P

3/15/2003 MF!22 NIOSH Manual of Analytical Methods

 M eth Flow Ra te Vol. (L) E x tr a c ti o n A n a ly t ic a l
Chemical No. M e th od Na m e ( L /m i n ) T e c h n iq u e Sampler
min max

Toluene !2,4 !diisoc ya nate 5522 ISOCYANATES 1-2 15 - 360 tryptamine/DMSO HPLC !FL/EC HD IM P

Tolue ne 2 ,4-d issoc ya nate 5525 ISOCYANATES, TOTAL (MAP) 1-2 1 - 500 MAP HP LC - U V G F F, IM P
(2,4 -TD I)

Toluene !2,6 !diisoc ya nate 5522 ISOCYANATES 1-2 15 - 360 tryptamine/DMSO HPLC !FL/EC HD IM P

Toluene !2,6 !diisoc ya nate 5521 ISO C YA NA TES , M O NO M ER IC 1.0 5 - 500 a ce ty la te /M e O H HPLC !EC HD IM P

Tolue ne-2 ,6-d iisocy ana te 5525 ISOCYANATES, TOTAL (MAP) 1-2 1 - 500 MAP HP LC - U V G F F, IM P
(2,6 -TD I)

p -To lue ne su lfon ic a cid 5043 P-TO LUE NE SU LFO NIC AC ID 1-3 10 - 1000 IPA/H 2O HP LC - U V GFF

o !Toluidine 2002 AM INE S, A RO M ATIC 0.02 - 1.0 10 - 150 Et h a nol G C !FID SG

o !Toluidine 2017 A N IL IN E , o - TO L U ID I NE , A N D 0.2 5 - 50 et h a nol G C -FID GFF + SG

N I TR O B E N Z EN E

o !Toluidine 5013 DYES 1-3 150 - 500 H 2O HPLC !U V PTFE

o !Toluidine 8317 ANALINE an d o-TOLUIDINE in urine NA NA ALK H P LC - EC D NA

o-Toluidine 8313 ANALINE an d o-TOLUIDINE in urine NA NA ALK H P LC - EC D NA

Tribromomethane 1003 HYDROC ARBONS, HALOG ENATED 0.01 - 0.2 4 - 70 C S2 G C !FID CCT

Tributy l pho sph ate 5034 TRIBUTY L PHO SPH ATE 1-3 2 - 100 d ieth y l et h er G C !FPD MC EF

T ri butyltin c hlo r ide 5504 O R G A N O T IN C O M P O U N D S 1 - 1.5 50 - 500 a c etic a /C H 3C N HP LC /G FAAS G F F & X A D !2

1,2,4 !Trichlorobenzene 5517 POLYCHLORO BENZENES 0.01 - 0.2 3 - 12 hexane G C !E C D P T F E & X A D !2

1,1,2 !Trichloroethane 1003 HYDROC ARBONS, HALOG ENATED 0.01 - 0.2 2 - 60 C S2 G C -FID CCT

1,1,1 !Trichloroethane 1003 HYDROC ARBONS, HALOG ENATED 0.01 - 0.2 0.1 - 8 C S2 G C -FID CCT

1,1,1 !Trichloroethane 2549 V O L A TI LE O R G A N IC C P D S 0.01 - 0.05 1-6 t h erma l TD /G C -M S TD

(Screen in g)

Trichloroethylene 1003 HYDROC ARBONS, HALOG ENATED 0.01 - 0.2 0.2 - 30 C S2 G C -FID CCT

Trichloroethylene 1022 T R IC H L O R O E TH Y L EN E 0.01 - 0.2 1 - 30 C S2 G C -FID CCT

Trichloroethylene 3701 TR IC H LO R O ETH YL EN E b y p ort G C > 0.02 80% vol NA GC -port air bag

Trichloroethylene 3800 ORG ANIC and INORGANIC G ASES 0.1 - 20 Inst r. d ep . NA FTIR Di r. R e a d
by EX TR ACTIV E FTIR SPE C T R O MET R Y

Trichlorofluoromethane 1006 F L UO R O T R IC H L O R O M E T H A NE 0.01 - 0.05 0.3 - 7 C S2 G C -FID CC T ( lg )

Trichloromethane 1003 HYDROC ARBONS, HALOG ENATED 0.01 - 0.2 1 - 50 C S2 G C -FID CCT

1,2,3 !Trichloropropane 1003 HYDROC ARBONS, HALOG ENATED 0.01 - 0.2 0.6 - 60 C S2 G C -FID CCT

T ri c hcylohe xyltin hydrox ide 5504 O R G A N O T IN C O M P O U N D S 1 - 1.5 50 - 500 a c etic a /C H 3C N HP LC - G FAAS GF F & X AD -2

1,1,2 !Tric hlo r o - 1020 1,1,2 !TRICHLOR O !1,2,2 ! 0.01 - 0.05 0.1 - 3 C S2 G C -FID CCT
1,2,2 !trifluoroethane T R IF L UO R O E T H A N E

1,1,2 !Tric hlo r o - 2549 V O L A TI LE O R G A N IC C P D S 0.01 - 0.05 1-6 t h erma l TD /G C -M S TD

1,2,2 !trifluoroethane (Screen in g)

Triethanolamine 3509 AM INO ETH AN O L C O M PO UN DS II 0.5 - 1.0 5 - 300 HSA IC IM P

T ri e thyle ne glyc o l 5523 GLYC OLS 0.5 - 2 5 - 60 MeOH G C -FID OV S-7

Triethylenetetramine 2540 ETHYLENEDIAMINE, 0.01 - 0.1 1 - 20 DMF HP LC - U V XA D-2

DIETHY LENE TRIAM INE, & W/1 0% NITC
T R IE T HY L EN E TE T RA M I N E

Trifluorobromomethane 1017 T R IF L UO R O B R O M O M E T HA N E 0.01 - 0.05 0.1 - 1 C H 2C l2 G C -FID 2 C C T(lg + sm )

T ri m e llitic anhydride 5036 T R IM E L LI TI C A N HY D R ID E 1.5 - 2 400 - 1000 MeOH G C -FID P VC

2,4,7 !Trin it ro flu o re n !9!o n e 5018 2,4,7 !TRINITR O !FLUOREN !9 !O N E 1-3 100 - 500 toluene HP LC - U V PTFE

Triortho cre syl ph osp ha te 5037 TRIOR THO CR ESYL P HO SPH ATE 1-3 2 - 100 d ieth y l et h er GC-FPD MC EF

Triphe nyl p ho sph ate 5038 TRIPHE NYL P HO SPH ATE 1-3 10 - 400 d ieth y l et h er GC-FPD MC EF

T ri phenyltin c hlo r ide 5527 T R IP H E N YL TI N C H L O R ID E 1-4 100 - 2000 TW M H P LC - IC P P VC

3/15/2003 MF!23 NIOSH Manual of Analytical Methods

 M eth Flow Ra te Vol. (L) E x tr a c ti o n A n a ly t ic a l
Chemical No. M e th od Na m e ( L /m i n ) T e c h n iq u e Sampler
min max

Tu be rc le b ac illi 0900 M YC O BA C TER IUM TUB ER C ULO SIS $4 va r ies reagent PCR PTFE

T ungste n 7301 EL EM EN TS b y IC P (A qu a R eg ia 1-4 50 - 1000 H C l /H N O 3 ICP-AES MC EF

Ashin g)

Tu ng ste n, s olu ble /ins olu ble 7074 TU NGSTEN (sol ubl e/i nso lu b le) 1-4 200 - 1000 H F /H N O 3 FAAS MC EF

Turpentine 1551 T U RP E N TI N E 0.01 - 0.2 1 - 10 C S2 G C -FID CCT

Turpentine 2549 V O L A TI LE O R G A N IC C P D S 0.01 - 0.05 1-6 t h erma l TD /G C -M S TD

(Screen in g)

n-Undecane 1500 HYDROC ARBONS, BP 36-216 oC 0.01 - 0.05 2-2 C S2 G C -FID CCT

V a ler alde hyde 2018 ALIPHATIC ALDEHYDES 0.1 - 1.5 1 - 15 ACN HP LC - U V SG-DNPH

V a ler alde hyde 2536 V A L ER A L D EH Y D E 0.01 - 0.04 0.5 - 10 toluene G C -FID X AD -2 /H M P

V a ler alde hyde 2539 A L D EH Y D E S, SC R E E N IN G 0.01 - 0.05 5-5 toluene G C -F ID /M S X AD -2 /H M P

V a nadium 7300 E LE M E NT S b y IC P 1-4 5 - 2000 H N O 3/HC lO 4 ICP-AES MC EF

V a nadium 7301 EL EM EN TS b y IC P (A qu a R eg ia 1-4 5 - 2000 H C l /H N O 3 ICP-AES MC EF

Ashin g)

V a nadium 7303 EL EM EN TS b y IC P (H ot B loc k/H C l/ 1-4 Se e Ta ble H C l /H N O 3 ICP-AES MC EF

H N O 3 Digestion)

V a nadium 9102 ELEMENTS on WIPES NA NA NA ICP-AES Wipe

V a nadium o xide s 7504 VANADIUM OX IDES 1.7 or 2 .2 200 - 1000 T HF XR D C Y C & P VC

Viny l ace tate 1453 VINYL A CE TATE 0.1 - 0.2 0.75 - 24 C H 2C l2/M e O H G C -FID MS(carbon)

Vinyl benzene 1501 HY DR O C AR BO NS , AR O M ATIC .01 - 1 1 - 14 C S2 G C -FID CCT

V i nyl br o m ide 1009 V IN Y L B R O M I D E 0.01 - 0.2 2 - 10 Et h a nol G C !FID C CT ( lg )

V i nyl c hlor ide 1007 V IN Y L C H L O R ID E 0.05 0.7 - 5 C S2 G C !FID 2 CCT

V i nylide ne c hlo r ide 1015 V IN Y L ID E N E C H LO R I D E 0.01 - 0.2 2.5 - 7 C S2 G C !FID CCT

V i nylide ne F luo r ide 3800 ORG ANIC and INORGANIC G ASES 0.1 - 20 Inst r. d ep . NA FTIR Di r. R e a d
by EX TR ACTIV E FTIR SPE C T R O MET R Y

Vinyl tolueneuene 1501 HY DR O C AR BO NS , AR O M ATIC 0.01 - 0.2 1 - 24 C S2 G C !FID CCT

V M&P naphtha 1550 NAPHTHAS 0.01 - 0.2 1.3 - 20 C S2 G C !FID CCT

VOCs 2549 V O L A TI LE O R G A N IC C P D S 0.01 - 0.05 1-6 t h erma l TD /G C !M S TD

(Screen in g)

W ar far in 5002 W AR FA RIN 1-4 200 - 1000 MeOH HPLC !U V PTFE

W o o d alc o ho l 2000 M E TH A NO L 0.02 - 0.2 1-5 H 2O/IPA G C !FID SG

Xylene 2549 V O L A TI LE O R G A N IC C P D S 0.01 - 0.05 1-6 t h erma l TD /G C !M S TD

(Screen in g)

X yle ne (o,m ,p ) 1501 HY DR O C AR BO NS , AR O M ATIC 0.01 - 0.2 2 - 23 C S2 G C !FID CCT

p -Xylene 3800 ORG ANIC and INORGANIC G ASES 0.1 - 20 Inst r. d ep . NA FTIR Di r. R e a d
by EX TR ACTIV E FTIR SPE C T R O MET R Y

m -Xylene 3800 ORG ANIC and INORGANIC G ASES 0.1 - 20 Inst r. d ep . NA FTIR Di r. R e a d
by EX TR ACTIV E FTIR SPE C T R O MET R Y

o-Xylene 3800 ORG ANIC and INORGANIC G ASES 0.1 - 20 Inst r. d ep . NA FTIR Di r. R e a d
by EX TR ACTIV E FTIR SPE C T R O MET R Y

2,4 !Xylidine 2002 AM INE S, A RO M ATIC 0.02 - 0.2 3 - 20 Et h a nol G C !FID SG

Y ttr ium 7300 E LE M E NT S b y IC P 1-4 5 - 1000 H N O 3/HC lO 4 IC P !AES MC EF

Y ttr ium 7301 EL EM EN TS b y IC P (A qu a R eg ia 1-4 5 - 1000 H C l /H N O 3 ICP-AES MC EF

Ashin g)

Y ttr ium 7303 EL EM EN TS b y IC P (H ot B loc k/H C l/ 1-4 Se e Ta ble H C l /H N O 3 ICP-AES MC EF

H N O 3 Digestion)

Y ttr ium 9102 ELEMENTS on WIPES NA NA NA ICP-AES Wipe

3/15/2003 MF!24 NIOSH Manual of Analytical Methods

 M eth Flow Ra te Vol. (L) E x tr a c ti o n A n a ly t ic a l
Chemical No. M e th od Na m e ( L /m i n ) T e c h n iq u e Sampler
min max

Z in c and c o m po unds 7030 ZINC and compounds, as Zn 1-3 2 - 400 HNO3 FAAS MC EF

Zinc 7300 E LE M E NT S b y IC P 1-4 5 - 200 H N O 3/HC lO 4 IC P !AES MC EF

Zinc 7301 EL EM EN TS b y IC P (A qu a R eg ia 1-4 5 - 200 H C l /H N O 3 ICP-AES MC EF

Ashin g)

Zinc 7303 EL EM EN TS b y IC P (H ot B loc k/H C l/ 1-4 Se e Ta ble H C l /H N O 3 ICP-AES MC EF

H N O 3 Digestion)

Y ttr ium 9102 ELEMENTS on WIPES NA NA NA ICP-AES Wipe

Z inc o xide 7502 Z IN C O X I D E 1-3 10 - 400 -- XR D P VC

Z ir c o nium 7300 E LE M E NT S b y IC P 1-4 5 - 200 H N O 3/HC lO 4 IC P !AES MC EF

Z ir c o nium 7301 EL EM EN TS b y IC P (A qu a R eg ia 1-4 5 - 200 H C l /H N O 3 ICP-AES MC EF

Ashin g)

Z ir c o nium 9102 ELEMENTS on WIPES NA NA NA ICP-AES Wipe

METHODS BY NUM BER

0500 PARTICU LATES N.O.R . 1-2 7 - 133 NA G R AV P VC

0600 PARTICULATES, N.O.R, RESP. 1.7, 2.2 ,2.5 20 - 400 NA Grav. CY C & P VC

0800 B IO A E R O S O L SA M P L IN G 28.3 va r ies NA va r ies i m p a c to r

0801 A ER O BIC B AC TE RIA - G C -F AM E 28.3 50 - 300 hex/MTBE G C -FID I m p a c to r

0900 MYCO BACTERIUM TUBERCULOSIS 4 va r ies reagent PCR PTFE

1000 A L LY L C H LO R I D E 0.01 - 1.0 16 - 100 bz G C !FID CCT

1001 M E T H YL C H LO R I D E 0.01 - 0.1 0.4 - 3 C H 2C l2 G C !FID 2 C C T (lg + sm )

1002 $!C H L O R O P R E N E 0.01 - 0.1 1.5 - 8 C S2 G C !FID CCT

1003 HYDROC ARBONS, HALOG ENATED 0.01 - 0.2 3 - 70 C S2 G C !FID CCT

1004 DICHLOROETHYL ETHER 0.01 - 1.0 2 - 15 C S2 G C !FID CCT

1005 M E T H YL E N E C H L O R ID E 0.01 - 0.2 0.5 - 2.5 C S2 G C !FID 2 CCT

1006 F L UO R O T R IC H L O R O M E T H A NE 0.01 - 0.05 0.3 - 7 C S2 G C !FID C CT ( lg )

1007 V IN Y L C H L O R ID E 0.05 0.7 - 5 C S2 G C !FID 2 CCT

1008 E T HY L EN E D IB R O M I D E 0.02 - 0.2 0.1 - 25 b z/M e O H G C !E C D CCT

1009 V IN Y L B R O M I D E 0.01 - 0.2 2 - 10 Et h a nol G C !FID C CT ( lg )

1010 EP ICH LO RO HY DR IN 0.01 - 0.2 2 - 30 C S2 G C !FID CCT

1011 E T HY L BR O M I D E 0.01 - 0.2 0.5 - 4 IPA G C !FID CCT

1012 D I FL U O R O D IB R O M O M E T H A N E 0.01 - 0.2 2.5 - 10 IPA G C !FID 2 CCT

1013 P R O P Y LE N E D IC H L O R ID E 0.01 - 0.2 0.1 - 3.5 acet/cyclohexane G C !E C N PCT

1014 M E T H YL IO D I D E 0.01 - 1.0 15 - 50 t ol G C !FID CCT

1015 V IN Y L ID E N E C H LO R I D E 0.01 - 0.2 2.5 - 7 C S2 G C !FID CCT

1016 1,1,2,2 !TETRACHLORO !2,2 ! 0.01 -0.035 0.5 - 2 C S2 G C !FID CCT

DIFLUOROETHANE &
1,1,2,2 !TETR ACHLOR O !1,2 !
D I FL U O R O E TH A N E

1017 T R IF L UO R O B R O M O M E T HA N E 0.01 - 0.05 0.1 - 1 C H 2C l2 G C -FID 2 C C T(lg + sm )

1018 DICHLORODIFLUORO METHANE, 0.01 - 0.05 1-4 C H 2C l2 G C !FID 2 CCT

1,2 !DICHLOROTETR AFLU O R O ! (lg + sm )
ETHANE&
C H L O R O D IF L UO R O M E T H A N E

1019 1,1,2,2 !T E TR A C H L O R O E TH A N E 0.01 - 0.2 3 - 30 C S2 G C !FID PCT

1020 1,1,2 !TRICHLOR O !1,2,2 ! 0.01 - 0.05 0.1 - 3 C S2 G C -FID CCT

T R IF L UO R O E T H A N E

1022 T R IC H L O R O E TH Y L EN E 0.01 - 0.2 1 - 30 C S2 G C -FID CCT

3/15/2003 MF!25 NIOSH Manual of Analytical Methods

 M eth Flow Ra te Vol. (L) E x tr a c ti o n A n a ly t ic a l
Chemical No. M e th od Na m e ( L /m i n ) T e c h n iq u e Sampler
min max

1024 1,3 !B U TA D IE N E 0.01 - 0.5 5 - 25 C H 2C l2 G C !FID CCT

1025 1 - a n d 2 -B R O M O P R O P A N E 0.01 - 0.2 0.1 - 12 C S2 G C -FID CCT

1026 P- C H LO R O B E N Z O T RI FL U O R ID E 0.01 - 0.2 0.1 - 10 C S 2/M e O H G C -FID CCT

1300 KETONES I 0.01 - 2.0 1 - 10 C S2 G C !FID CCT

1301 KE TO NE S II 0.01 - 0.2 1 - 25 M e O H /C S 2 G C !FID CCT

1302 N - M E TH Y L -2 - PY R R O L ID I NO N E 0.05 - 0.2 0.5 - 125 C H 2C L 2/M e O H GC-FID/NPD CCT

1400 ALCOHO LS I 0.01 - 0.2 1 - 10 C S2 G C !FID CCT

1401 ALC O HO LS II 0.01 - 0.2 2 - 10 IP A /C S 2 G C !FID CCT

1402 ALC O HO LS III 0.01 - 0.2 1 - 10 IP A /C S 2 C G !FID CCT

1403 ALC O HO LS IV 0.01 - 0.05 6 - 50 M e O H /C H 2C l2 G C !FID CCT

1404 M E TH YL CY C LO H EX AN O L 0.01 - 0.2 1 - 15 C H 2C l2 G C !FID CCT

1405 ALCOHO LS COM BINED 0.01 - 0.2 2 - 10 IP A -C S 2 G C -FID CCT

1450 ESTERS I 0.01 - 0.2 1 - 10 C S2 G C !FID CCT

1451 ME THYL C ELLO SO LVE A CE TATE 0.01 - 0.2 0.2 - 20 C S2 G C !FID CCT

1452 ETHY L FO RM ATE 0.01 - 0.2 0.3 - 10 C S2 G C !FID CCT

1453 VINYL A CE TATE 0.1 - 0.2 0.75 - 24 C H 2C l2/M e O H G C -FID MS(carbon)

1454 ISOP RO PYL A CE TATE 0.02 - 0.2 0.1 - 9 C S2 G C !FID CCT

1457 ETHY L AC ETATE 0.01 - 0.2 0.1 - 10 C S2 G C !FID CCT

1458 ME THYL A CE TATE 0.01 - 0.2 0.2 - 10 C S2 G C !FID CCT

1459 ME THYL A CR YLATE 0.01 - 0.2 1-5 C S2 G C !FID CCT

1460 ISOP RO PYL A CE TATE 0.02 - 0.2 0.1 - 9 C S 2/Me th G C -FID CCT

1500 HYDROC ARBONS, BP 36 !216 °C 0.01 - 0.2 2-7 C S2 G C !FID CCT

1501 HY DR O C AR BO NS , AR O M ATIC 0.01 - 1.0 1 - 30 C S2 G C !FID CCT

1550 NAPHTHAS 0.01 - 0.2 1.3 - 20 C S2 G C !FID CCT

1551 T U RP E N TI N E 0.01 - 0.2 1 - 10 C S2 G C -FID CCT

1552 TERPENES 0.01 - 2 2 - 30 C S2 G C !FID CCT

1600 C A R B O N D IS U LF ID E 0.01 - 0.2 2 - 25 t ol G C !FPD C CT & d ry tu b e

1601 1,1 !DICHLORO !1 !N I TR O E T H AN E 0.01 - 1.0 1.5 - 15 C S2 G C !FID PCT

1602 D I O X AN E 0.01 - 0.2 0.5 - 15 C S2 G C !FID CCT

1603 AC ETIC AC ID 0.01 - 0.1 20 - 300 formic a G C !FID CCT

1604 AC RYLO NITRILE 0.01 - 0.2 3.5 - 20 a c et/C S 2 G C !FID CCT

1606 AC ETON ITRILE 0.01 - 0.2 1 - 25 C H 2C l2/M e O H G C !FID CCT

1608 G LY C ID O L 0.01 - 1.0 5 - 100 T HF G C !FID CCT

1609 TETR AHYDR OFU R AN 0.01 - 0.2 1-9 C S2 G C !FID CCT

1610 ETHYL ETHER 0.01 - 0.2 0.25 - 3 C S2 G C !FID CCT

1611 METHYLAL 0.01 - 0.2 1-3 hexane G C !FID CCT

1612 P R O P Y LE N E O X ID E 0.01 - 0.2 0.5 - 5 C S2 G C !FID CCT

1613 P Y R ID I NE 0.01 - 1.0 18 - 150 C H 2C l2 G C !FID CCT

1614 E T HY L EN E O X ID E 0.05 - 0.15 1 - 24 DMF G C !E C D PC T w/HB r

1615 METH YL tert !BUTYL ETHER 0.1 - 0.2 2 - 96 C S2 G C !FID 2 CC T ( lg )

1616 BUTYL GLYCIDYL ETHER 0.01 - 0.2 15 - 30 C S2 G C !FID CCT

1617 PHENYL ETHER 0.01 - 0.2 1 - 50 C S2 G C !FID CCT

3/15/2003 MF!26 NIOSH Manual of Analytical Methods

 M eth Flow Ra te Vol. (L) E x tr a c ti o n A n a ly t ic a l
Chemical No. M e th od Na m e ( L /m i n ) T e c h n iq u e Sampler
min max

1618 ISOPROPYL ETHER 0.01 - 0.05 0.1 - 3 C S2 G C !FID CCT

1619 PHENYL GLYCIDYL ETHER 0.01 - 1 80 - 150 C S2 G C !FID CCT

1620 ISOPROPYL GLYCIDYL ETHER 0.01 - 0.2 1 - 30 C S2 G C !FID CCT

2000 M E TH A NO L 0.02 - 0.2 1-5 H 2O/IPA G C !FID SG

2002 AM INE S, A RO M ATIC 0.2 - 1.0 30 - 150 Et h a nol G C !FID SG

2003 1,1,2,2 !T E TR A B R O M O E T H AN E 0.2 - 1.0 50 - 100 T HF G C !FID SG

2004 DIMETHYLACETAMIDE and 0.01 - 1.0 15 - 80 MeOH G C !FID SG

D I M E TH Y L FO R M A M I D E

2005 N I TR O A R O M A T IC C O M P O U N D S 0.01 - 1 1 - 150 MeOH G C !FID SG

2007 AMINOETHANO L COM POUNDS I 0.01 - 0.2 4 - 24 M eO H/H 2O G C !FID SG

2008 C HLO RO AC ETIC AC ID 0.05 - 0.2 1 - 100 H 2O IC SG

2010 AM INE S, A LIPH ATIC 0.01 - 1.0 3 - 30 H 2SO 4/a q M e O H G C !FID SG

2011 FO RM IC A C ID 0.05 - 0.2 1 - 24 H 2O IC P T FE &

S G ( w a s h ed )

2012 n !B U TY L AM I N E 0.01 - 1.0 2 - 100 MeOH G C !FID S G + H 2SO 4

2013 PHENYL ETHER !DIPHENYL MIXT U R E 0.01 - 0.2 1 - 40 bz G C !FID SG

2014 p !C H L O RO P H EN O L 0.05 - 0.2 1.5 - 40 C H 3C N HPLC !U V SG

2015 C H L O R O A C E T AL D E HY D E 0.05 - 0.2 3 - 16 MeOH G C !E C D SG

2016 F O R M A L D E HY D E 0.03 - 1.5 1 - 15 ac eto nitr ile HP LC - U V SG/DNPH

2017 A N IL IN E , o - TO L U ID I NE , A N D 0.2 5 - 50 et h a nol G C -FID GFF +

N I TR O B E N Z EN E SG w/H 2SO 4

2018 ALIPHATIC ALDEHYDES 0.1 - 1.5 1 - 15 ACN HP LC - U V SG-DNPH

2500 M E T H YL E TH Y L K E TO N E 0.01 - 0.2 0.25 - 12 C S2 G C !FID Carbon be ads

2501 AC RO LEIN 0.01 - 0.1 1.5 - 48 t ol G C !NPD X A D !2 /H M P

2504 TETRA ETHY L PYRO PHO SPH ATE 0.01 - 0.2 20 - 48 toluene G C !FPD 2 Chrom 102

2505 F UR FU RY L A LC O H O L 0.01 - 0.05 3 - 25 a cet G C !FID Por Q

2506 AC ETO NE CY AN O HY DR IN 0.2 0.3 - 12 Et Ac G C !NPD P or Q S

2507 N ITR O G LY C ER IN & ETH YL EN E G LY C O L 0.2 - 1.0 3 - 100 Et h a nol G C !E C D T e n a x!G C

DINITRA TE

2508 I SO P H O R O N E 0.01 - 1.0 2 - 25 C S2 G C !FID PCT

2510 1 !O C TA N ETH IO L 0.01 - 0.2 1 - 15 a cet G C !FPD Te na x G C

2513 ETH YLE NE CH LO RO HY DR IN 0.01 - 0.2 2 - 35 IP A /C S 2 G C !FID PCT

2514 A N IS ID I NE 0.5 - 1.0 24 - 320 MeOH HPLC !U V X A D !2

2515 D I AZ O M E T H A N E 0.2 6 - 30 C S2 G C !FID X A D !2 ( c oa t e d )

2516 D I C H LO R O F L U O R O M E T HA N E 0.01 - 0.05 0.25 - 3 C S2 G C !FID 2 CC T ( lg )

2517 P E N TA C H L O R O E TH A N E 0.01 - 0.2 1 - 10 hexane G C !E C D Por R

2518 HEXACHLOR O !1,3 !CYC LO P EN T A- 0.01 - 0.2 0.25 - 90 hexane G C !E C D 2 Por T

D I EN E

2519 E T HY L C H LO R I D E 0.02 - 0.05 0.3 - 3 C S2 G C !FID 2 CC T ( lg )

2520 M E T H YL B RO M I D E 0.01 - 0.1 1-5 C S2 G C !AED PC T(2)+d ry

tube

2521 M E T H YL C Y C LO H E X A N O N E 0.01 - 0.05 1-6 a cet G C !FID Por Q

2522 NITROSAMINES 0.2 - 2.0 15 - 1000 M e O H /C H 2C l2 G C !TEA The rma loso rb/N

2523 1,3 !C Y C L O P E N TA D IE N E 0.01 - 0.05 1-5 Et Ac G C !FID Chrom104/

ma leic anh .

3/15/2003 MF!27 NIOSH Manual of Analytical Methods

 M eth Flow Ra te Vol. (L) E x tr a c ti o n A n a ly t ic a l
Chemical No. M e th od Na m e ( L /m i n ) T e c h n iq u e Sampler
min max

2524 DIM ETHY L SULFA TE 0.01 - 0.2 0.25 - 12 d iEt eth er G C !E C N Por P

2525 n !BU TYL MER CAPTAN 0.01 - 0.05 1-4 a cet G C !FPD Chrom 104

2526 N I TR O E T H AN E 0.01 - 0.05 1.5 - 3 Et Ac G C !FID 2 X A D !2

2527 N I TR O M E T H A N E 0.01 - 0.05 1.2 - 3 Et Ac G C !FPD Chrom 106

2528 2 !N I TR O P R O P A N E 0.01 - 0.05 0.1 - 2 Et Ac G C !FID Chrom 106

2529 FU R FU R AL 0.01 - 0.05 1 - 12 t ol G C !FID X A D !2 /H M P

2530 DIPHENYL 0.01 - 0.5 15 - 30 C C l4 G C !FID Te na x G C

2532 G L U TA R A LD E H Y D E 0.01 - 0.08 4 - 39 C H 3C N HPLC !U V SG/DNPH

2533 TETR AETHYL LEAD (as Pb ) 0.01 - 1.0 30 - 200 pentane G C !PID X A D !2

2534 TETR AMETHYL LEAD (as P b ) 0.01 - 0.2 15 - 100 pentane G C !PID X A D !2

2535 T O L UE N E !2,4 !DIISO CY ANA TE 0.2 - 1.0 2 - 170 MeOH HPLC !U V GW coated

2536 V A L ER A L D EH Y D E 0.01 - 0.04 0.5 - 10 toluene G C -FID X AD -2 /H M P

2537 ME THYL a nd ETH YL M ETHA CR YLATE 0.01 - 0.05 1-8 C S2 G C !FID X A D !2

2538 A C E T AL D E HY D E 0.01 - 0.05 1 - 12 t ol G C !F ID X A D !2 /H M P

2539 A L D EH Y D E S, SC R E E N IN G 0.01 - 0.05 5-5 t ol G C !F ID /M S X A D !2

2540 ETHY LENE DIAM INE, 0.01 - 0.1 1 - 20 DMF HPLC !U V X A D !2

DIETHY LENE TRIAM INE, & w/10 % N ITC
T R IE T HY L EN E TE T RA M I N E

2541 F O R M A L D E HY D E 0.01 - 0.1 1 - 36 t ol G C !FID X A D !2 /H M P

2542 M E R C A P TA N S 0.1 - 0.2 10 - 150 H C l/D C E G C !FPD GFF/HgAc

2543 H E X A C H LO R O B U T A D IE N E 0.05 - 0.2 1 - 100 hexane G C !E C D X A D !2

2544 N I C O TI N E 1.0 60 - 400 Et Ac G C !NPD X A D !2

2545 ALLYL GLYCIDYL ETHER 0.01 - 0.2 1.5 - 8 d ieth y l et h er G C !FID Tenax

2549 V O L A TI LE O R G A N IC C P D S 0.01 - 0.05 1-6 t h erma l TD /G C !M S TD

(Screen in g)

2550 B EN ZO TH IA ZO LE IN AS PH A LT F UM E 1.0 - 2.0 480 - 960 hexane G C - SC D PTFE + X D-2

2551 N I C O TI N E 0.1 - 1.0 0.5 - 600 ethy l ace tate GC-NPD XA D-4

2552 ME THYL A CR YLATE 0.01 - 0.2 1-5 C S2 G C -FID A -C M S

2553 KE TO NE S II 0.01 - 0.2 1 - 25 IP A -C S 2 G C -FID A -C M S

2554 GLYCOL ETHER S 0.1 - 0.2 3 - 25 M e C l2/Me th G C -FID A-747

2555 KETONES I 0.01 - 0.2 0.5 - 3.0 C S2 G C -FID A -C M S

1 - 10

2556 I SO P H O R O N E 0.01 - 1 2 - 25 DEE G C -FID XAD

2557 DIACETYL 0.01 - 0.2 1 - 10 Ac et-M eth G C -FID A -C M S

2558 AC ETO IN 0.01 - 0.2 1 - 10 Ac et-M eth G C -FID A -C M S

2559 D E C A B R O M O D I PH E N Y L O X I D E 2.0 48 - 960 DMSO HP LC /UV QFF

2560 1-NITROPYRENE in DIESEL 1.0 - 2.0 480 - 960 T ol G C - NC D GFF

PARTICULATES

2561 2 -(D IM E TH YL AM IN O )E TH A NO L 0.02 - 1 10 - 24 MeOH G C -FID XAD

1 -D IM E TH YL AM IN O -2 -P RO P AN O L

2562 1 , 1, 2 ,2 - TE T RA C H L O R O E TH A N E 0.01 - 0.2 3 - 30 C S2 G C -FID A -C M S

3500 F O R M A L D E HY D E 0.2 - 1.0 1 - 100 NaHSO 3 VIS P TF E & 2 IM P

3503 H Y D R A ZI N E 0.2 - 1.0 7 - 100 rea ge nts VIS BuB

3505 TETRAMETHYL THIOUREA 0.2 - 1.0 50 - 250 rea ge nts VIS IMP /H 2O

3506 A C E T IC A N H Y D R ID E 0.2 - 1.0 25 - 100 reagent VIS BuB

3/15/2003 MF!28 NIOSH Manual of Analytical Methods

 M eth Flow Ra te Vol. (L) E x tr a c ti o n A n a ly t ic a l
Chemical No. M e th od Na m e ( L /m i n ) T e c h n iq u e Sampler
min max

3507 A C E T AL D E HY D E 0.1 - 0.5 6 - 60 reagent HPLC !U V BuB

3508 M E T H YL E TH Y L K E TO N E P E R O X ID E 0.5 - 0.2 52 - 520 reagent VIS IM P

3509 AM INO ETH AN O L C O M PO UN DS II 0.5 - 1.0 5 - 300 HSA IC IM P

3510 M O N O M E T HY L H YD R A Z IN E 0.5 - 1.5 3 - 20 P M A /H C l VIS B u B/H C l

3511 M O N O M E T HY L AN I LI N E 0.2 - 1.0 11 - 100 N a OH G C !FID BuB /H 2SO 4

3512 M A L E IC A N H Y D R ID E 0.2 - 1.5 40 - 500 -- HPLC !U V BuB /H 2O

3513 T E TR A N IT R O M E TH A N E 0.5 - 1.0 20 - 250 !- G C !FID I M P /E t A c

3514 E T HY L EN I M IN E 0.2 1 - 48 C H C l3 HPLC !U V BuB

3515 1,1 !D I M E TH Y L HY D R A Z IN E 0.2 - 1.0 2 - 100 reagent VIS Bu B (. 1 M HC l)

3516 C R O T O N A L D EH Y D E 0.1 - 0.2 1 - 49 b u ffer DPP BuB

3518 P H E N YL H Y DR A Z IN E 0.2 - 1.0 25 - 120 PMA VIS B u B/H C l

3600 MANEB NA NA Cy s/EDTA HP LC - U V Patch

3601 MANEB NA NA NA HP LC - U V Hand wa sh

3700 B EN ZE NE by po rta ble G C > 0.02 80% vol NA GC air bag

3701 TR IC H LO R O ETH YL EN E b y p ort G C > 0.02 80% vol NA GC -port air bag

3702 E TH YL EN E O X ID E b y p orta ble G C > 0.02 80% vol NA G C !PID air bag

3704 P ER C H LO R O E TH Y LE N E (p o rta b le G C ) 0.1 - 1 8 0% V O L NA Po rt G C -PID air bag

in e xh ale d b rea th a nd air

3800 ORG ANIC and INORGANIC G ASES 0.1 - 20 Inst r. d ep . NA FTIR Di r. R e a d

by EX TR ACTIV E FTIR SPE C T R O MET R Y

4000 TOLU ENE (Diffusive sam pler) NA 15 min-8h C S2 G C !FID Diffusive

5000 C A R BO N B LA C K 1-2 30 - 570 NA Grav P VC

5001 2,4 !D an d 2,4,5 !T 1-3 15 - 200 MeOH HPLC !U V GFF

5002 W AR FA RIN 1-4 200 - 1000 MeOH HPLC !U V PTFE

5003 PARAQUAT 1-4 40 - 1000 H 2O HPLC !U V PTFE

5004 H Y D R O Q U IN O N E 1-4 30 - 180 ac etic ac id HPLC !U V MC EF

5005 THIRAM 1-4 10 - 400 C H 3C N HPLC !U V PTFE

5006 CARBARYL 1-3 20 - 400 reagent VIS GFF

5007 ROTENONE 1-4 8 - 400 C H 3C N HPLC !U V PTFE

5008 PYRETHUM 1-4 20 - 400 C H 3C N HPLC !U V GFF

5009 B E N Z O Y L P E R O X ID E 1-3 40 - 400 d ieth y l et h er HPLC !U V MC EF

5010 BRO MO XYN IL and B 'OC TANO ATE 1-3 2 - 400 C H 3C N HPLC !U V PTFE

5011 ETHYLENE THIOUREA 1-3 200 - 800 H 2O VIS PVC or MCEF

5012 EPN 1-2 15 - 700 isooctane G C !FPD GFF

5013 DYES 1-3 150 - 500 H 2O HPLC !U V PTFE

5014 CH LORINA TED TERPH ENYL 1-3 100 - 1500 isooctane G C !E C D GFF

5016 S T RY C H N IN E 1-3 70 - 1000 rea ge nts HPLC !U V GFF

5017 DIBUTY L PHO SPH ATE 1-3 50 - 250 C H 3C N G C !FPD PTFE

5018 2,4,7 !TRINITR O !FLUOREN !9 !O N E 1-3 100 - 500 toluene HP LC - U V PTFE

5019 AZ ELA IC A C ID 1-3 200 - 1000 Et h a nol G C !FID P VC

5020 D I BU T YL P HT H A LA T E & 1-3 6 - 200 C S2 G C !FID MC EF

DI(2 !ETHY LHEX YL) PHTH ALATE

5021 o !TERPHENYL 1-3 2 - 30 C S2 G C !FID PTFE

5022 ARSENIC, organo! 1-3 50 - 1000 b u ffer IC !HYAAS PTFE

3/15/2003 MF!29 NIOSH Manual of Analytical Methods

 M eth Flow Ra te Vol. (L) E x tr a c ti o n A n a ly t ic a l
Chemical No. M e th od Na m e ( L /m i n ) T e c h n iq u e Sampler
min max

5025 C H L O R IN A T ED D IP H E N YL O X ID E 0.5 - 1.5 8 - 200 isooctane G C !E C N MC EF

5026 OIL MIST, MINER AL 1-3 20 - 500 C C l4 IR PVC or MCE

5027 RIB AV IRIN 1-4 5 - 1000 H 2SO 4 HPLC !U V GFF

5029 4,4'!M E T H YL E N ED I AN I LI N E 1-2 10 - 1000 K O H/M e O H HPLC !U V GF F/H 2SO 4

5030 C YA NU RIC AC ID 1-3 10 - 1000 rea ge nts HPLC !U V P VC

5031 A SP AR TA M E 1-3 70 - 1200 eluent HPLC !U V PTFE

5032 PEN TAM IDINE ISETH ION ATE 1-2 50 - 1500 rea ge nts HPLC/FL P VC / o p a q u e

5033 p !N I TR O A N IL IN E 1-3 20 IPA HPLC !U V MC EF

5034 TRIBUTY L PHO SPH ATE 1-3 2 - 100 d ieth y l et h er G C !FPD MC EF

5035 SUPER ABSORBENT POLYMER 1-3 50 - 1500 C u (Ac)2 IC P or AAS P VC

5036 T R IM E L LI TI C A N HY D R ID E 1.5 - 2 400 - 1000 MeOH G C -FID P VC

5037 TRIOR THO CR ESYL P HO SPH ATE 1-3 2 - 100 d ieth y l et h er GC-FPD MC EF

5038 TRIPHE NYL P HO SPH ATE 1-3 10 - 400 d ieth y l et h er GC-FPD MC EF

5039 C H L O R IN A T ED C A M P H E N E 0.2 - 1 2 - 30 p et eth er G C !E C D MC EF

5040 ELEMENTAL CARBON (DIESEL 2-4 142 -19000 t h erma l E G A/TO A QFF
PARTICULATE)

5041 C AP SA ICIN an d D IHY DR O C AP SA ICIN 1-3 5 - 1000 C H 3C N HPLC !FL GFF

5042 B E N Z EN E S O LU B LE F R AC T IO N A N D 1 -4 28 - 400 benzene Grav tared PTFE

TOTAL PARTICULATE (ASPHALT FUME)

5043 p -TO LUE NE SU LFO NIC AC ID 1-3 10 - 1000 1PA /H 20 HP LC - U V GFF

5044 E S TR O G E N I C C O M P O U N D S 1 150 - 1000 M eth HP LC - U V PTFE

5046 TETRAKIS (HYD RO XYM ETHYL) 1 - 1.7 1 - 400 ACN HP LC - U V GFF

P H O S P H O N IU M C H L O R ID E

5502 A L D R IN & L IN D A N E 0.2 - 1.0 18 - 240 isooct G C !E C N GFF & BuB

5503 POLY CH LORO BIPHENY LS 0.05 - 0.2 1 - 50 hexane G C !E C D G FF & F lor isil

5504 O R G A N O T IN C O M P O U N D S 1 - 1.5 50 - 500 a c etic a /C H 3C N HP LC - G FAAS GF F & X AD -2

5506 PO LYN UC LEA R A RO M ATIC 2.0 200 - 1000 ac eto nitr ile HPLC !FL/U V P T F E & X A D !2
HYDROC ARBONS

5508 KEPONE 0.5 - 1.0 50 - 600 b z/M e O H G C !E C D M C E F & IM P

5509 BENZIDINE and 0.2 20 - 100 triethyl amine HPLC !U V GFF

3,3'!DICHLORO !B E N Z ID I NE /M e O H

5510 CHLORDANE 0.5 - 1.0 10 - 200 t ol G C !E C D M C E F & Ch ro m

102

5512 P EN TA C HL OR O PH EN O L 0.5 - 1.0 48 - 480 MeOH HPLC !U V MCEF & BuB

5514 D EM E TO N 0.2 - 1.0 30 - 500 t ol G C !FPD M C E F & X A D !2

5515 PO LYN UC LEA R A RO M ATIC 2.0 200 - 1000 va r ies G C !FID P T F E & X A D !2
HYDROC ARBONS

5516 2,4 ! & 2,6 !T O L UE N E D IA M I N E 1.0 30 - 500 a ce ty la te /M e O H HPLC !U V IM P

5517 POLYCHLORO BENZENES 0.01 - 0.2 3 - 12 hexane G C !E C D P T F E & X A D !2

5518 NAPHTHYLAMINES 0.2 - 0.8 30 - 100 acetic a /IPA G C !FID GFF & SG

5519 EN DR IN 0.5 - 1.0 12 - 400 t ol G C !E C D M C E F & Ch ro m

102

5521 ISO C YA NA TES , M O NO M ER IC 1.0 5 - 500 rea ge nts HPLC !EC HD IM P

5522 ISOCYANATES 1-2 15 - 360 tryptamine/DMSO HPLC !FL/EC HD IM P

5523 GLYC OLS 0.5 - 2 5 - 60 MeOH G C !FID O VS !7

3/15/2003 MF!30 NIOSH Manual of Analytical Methods

 M eth Flow Ra te Vol. (L) E x tr a c ti o n A n a ly t ic a l
Chemical No. M e th od Na m e ( L /m i n ) T e c h n iq u e Sampler
min max

5524 META LWO RKING FLUIDS (MW F) ALL 1.6 - 2.0 1000 - ND D C M/MeO H/T ol Grav PTFE/CYC
CATEGO RIES MeOH

5525 ISOCYANATES, TOTAL (MAP) 1-2 1 - 500 MAP HP LC - U V G F F, IM P

5526 METHYLTIN CHLORIDES 0.25 - 1 15 - 75 AAA GC-FPD O VS

5527 T R IP H E N YL TI N C H L O R ID E 1-4 100 - 2000 TW M H P LC - IC P P VC

5600 ORG ANOPHO SPHORUS PESTICIDES 0.2 - 1 12 - 240 t ol/a cet G C !FPD O VS !2

5601 ORG ANONITROGEN PESTICIDES 0.1 - 1 var - 480 reagent HP LC - U V OV S-2

5602 CHLORINATED ORG ANONITROGEN 0.2 - 1 12 - 480 reagent G C /E C D OV S-2

H ER BIC ID ES (A IR SA M PL IN G )

5603 ALA C HLO R in AIR 1 70 - 1750 MeOH ELISA SPE disk

5606 THIO PH EN ATE -M ETH YL in AIR 0.1 - 1.0 20 - 480 IP A /A C N HP LC - U V QFF/SST

5700 FORM ALDEHYDE on dust 2 240 - 1050 H 2O /D N PH /C H 3C N HPLC !U V I O M / P VC

5701 R ES O RC IN O L 0.2 - 1 5 - 160 MeOH G C -FID OV S-7

5800 P O L Y AR O M A T IC C O M P O U N D S 1-2 5 - 1000 hexane FI-FL PTFE +

(PACs) XA D-2

6001 A R S IN E 0.01 - 0.2 0.1 - 10 HNO3 G FAAS CCT

6002 P H O S P H IN E 0.01 - 0.2 1 - 16 reagent VIS S G / H g( C N )2

- 2-
6004 S U LF U R D IO X I D E 0.5 - 1.5 4 - 200 H C O 3 /C O 3 IC M CE F & p a d
w / N a2C O 3

6005 I O D IN E 0.5 - 1.0 15 - 225 N a 2C O 3 IC C C T w /alk ali

6006 D I BO R A N E 0.5 - 1.0 60 - 260 H 2O 2 PES P TF E & C C T

w / o xi d iz e r

6007 NICKEL CARBONYL 0.05 - 0.2 7 - 80 HNO3 G FAAS C C T (lo w N i)

6008 S T IB IN E 0.01 - 0.2 4 - 50 HCl VIS S G w /H g C l2

6009 MER CURY 0.15 - 0.25 2 - 100 H N O 3/H C l AAS !cold va p Ho pc alite

6010 H Y D R O G E N C Y A N ID E 0.05 - 0.2 2 - 90 H 2O VIS s od a lim e

6011 C H L O R IN E a n d B R O M I N E 0.3 - 1.0 2 - 90 N a 2S 2O 3 IC Ag F

6012 S U LF U R Y L F L UO R I D E 0.05 - 0.1 1.3 - 10 N a OH IC C CT ( lg )

6013 H Y D R O G E N S UL F ID E 0.1 - 1.5 1.2 - 40 N H 4OH /H 2O 2 IC P T FE &

(withdrawn) C CT ( lg )

6014 N I TR IC O X I D E & N IT R O G E N D IO X I D E 0.025 1.5 - 6 reagent VIS M S w / T EA &

o x id i ze r

6015 AM M O NIA by VIS 0.1 - 0.2 0.1 - 90 H 2O VIS !Au to S G + H 2SO 4

6016 AM M O NIA by IC 0.1 - 0.5 0.1 - 96 H 2O IC S G + H 2SO 4

6017 H Y D R O G E N C Y A N ID E 0.05 - 2 2 - 90 H 2O IC -D C Am p SL

6402 P H O S P H O R U S T R IC H L O R ID E 0.05 - 0.2 11 - 100 rea ge nts VIS BuB /H 2O

6600 N I TR O U S O X ID E NA 80% vol NA IR air bag

6601 OXYG EN NA 1 - NA NA Sens or po rta ble

6602 S U LF U R H EX A F LU O R ID E 0.01 - 0.05 80% vol NA G C !E C D air bag

6603 C A R B O N D IO X I D E 0.02 - 0.1 80% vol NA G C !T C D air bag

6604 CARBON MONOXIDE NA NA NA Sens or Port In str

6700 NITR OGEN DIOX IDE (Di ffu sive) NA NA reagent VIS Diffusive

7013 ALUMINUM & CPDS, as Al 1-3 10 - 400 HNO3 FAAS MC EF

7020 C A LC IU M a nd c pd s a s C a 1-3 20 - 400 H N O 3/HC lO 4 FAAS MC EF

7024 C H R O M IU M a nd c pd s, as C r 1-3 10 - 1000 H C l /H N O 3 FAAS MC EF

3/15/2003 MF!31 NIOSH Manual of Analytical Methods

 M eth Flow Ra te Vol. (L) E x tr a c ti o n A n a ly t ic a l
Chemical No. M e th od Na m e ( L /m i n ) T e c h n iq u e Sampler
min max

7027 C O B A LT an d c p ds , a s C o 1-3 30 - 1500 a q re g /H N O 3 FAAS MC EF

7029 CO PPER (dust & fumes) 1-3 50 - 1500 H N O 3/H C l FAAS MC EF

7030 ZINC and compounds, as Zn 1-3 2 - 400 HNO3 FAAS MC EF

7048 C A D M IU M a nd c pd s, as C d 1-3 25 - 1500 H N O 3/H C l FAAS MC EF

7056 B A R IU M , S O LU B LE C O M P O U N D S 1-4 50 - 2000 H 2O FAAS MC EF

7074 TU NGSTEN (sol ubl e/i nso lu b le) 1-4 200 - 1000 H F /H N O 3 FAAS MC EF

7082 LEAD by FAAS 1-4 200 - 1500 H N O 3/H 2O 2 FAAS MC EF

7102 BERYLLIUM and cpds, as Be 1-4 25 - 2000 H N O 3/H 2SO 4 G FAAS MC EF

7105 LEAD by GFAAS 1-4 1 - 1500 H N O 3/H 2O 2 G FAAS MC EF

7300 E LE M E NT S b y IC P 1-4 V a r ies H N O 3/HC lO 4 IC P !AES MC EF

7301 E LE M E NT S b y IC P 1-4 V a r ies Aq R eg ICP-AES MC EF

(A Q UA RE G IA AS HIN G ) PVCF

7301 E LE M E NT S b y IC P 1-4 V a r ies H C l /H N O 3 ICP-AES MC EF

(A Q UA RE G IA AS HIN G )

7303 EL EM EN TS b y IC P (H ot B loc k/H C l/ 1-4 Se e Ta ble H C l /H N O 3 ICP-AES MC EF

H N O 3 Digestion)

7400 A S BE ST O S F IB ER S b y PC M 0.5 - 16 400 - va r NA PCM MCEF open

7401 ALKA LINE DU STS 1-4 70 - 1000 HCl T it ra t ion PTFE

7402 ASBESTOS FIBERS by TEM 0.5 - 16 400 - va r NA TEM MCEF open

7404 C E LL UL OS E IN SU LA TIO N 1 NA NA SEM ACF

7500 S IL IC A , C R Y ST A LL IN E , b y X R D. 1.7, 2.2 ,2.5 400 - 1000 a s h or T HF XR D C Y C + P VC

7501 SILICA, AMOR PHOUS 1.7, 2.2 ,2.5 50 - 400 ash XR D PVC (total)
PVC&C YC

7502 Z IN C O X I D E 1-3 10 - 400 NA XR D P VC

7504 VANADIUM OX IDES 1.7, 2.2 ,2.5 200 - 1000 T HF XR D C Y C & P VC

7505 L E AD S U LF ID E 1.7, 2.2 ,2.5 600 - 1000 T HF XR D C Y C & P VC

7506 B O R O N C A R B ID E 1.7, 2.2 ,2.5 100 - 1000 ash XR D C Y C & P VC

7600 C H R O M I U M , HE X A V A LE N T 1-4 8 - 400 reagent VIS P VC

7601 S IL IC A , C R Y ST A LL IN E 1.7, 2.2 ,2.5 400 - 800 H 3PO 4/HF VIS CYC & MC E or
P VC

7602 SILICA, CRYSTALLINE (IR ) 1.7, 2.2 ,2.5 400 - 800 ash IR CYC & MC E or
P VC

7603 SILICA in coal mine dust 1.7, 2.2 ,2.5 300 - 1000 ash IR C Y C & P VC

7604 C H R O M I U M , HE X A V A LE N T 1-4 100 - 1000 N a O H / N a2 C O 3 IC P VC

7605 CHROM IUM, HEXAV ALEN T b y 0.1 - 4 1 - 400 N a O H - N a2C O 3 IC P VC

IONCHROMATOG RAPHY

7700 LEAD in Air by Che mical Spot Test 2 10 - 240 NA Sp ot MC EF

7701 LEAD BY ULTRASOUND /ASV 1-4 20 - 1500 HNO3 Port ASV MC EF

7702 LEAD by Fi eld Portabl e XR F 1-4 570 - 1900 NA XR F (po rt) MC EF

7703 CHROM IUM, HEXAV ALEN T b y Field - 1-4 10 - 1200 ( N H4) 2SO 4/ VIS PVC, MCE, PTFE
Portab le Spe ctroph otom etry N H 4O H

7900 AR SENIC & compoun ds , a s As 1-3 30 - 1000 H N O 3/H 2SO 4/HC lO 4 HYAAS MC EF

7901 AR SENIC TR IOX IDE, as A s 1-3 30 - 1000 H N O 3/H 2O 2 G FAAS MC EF

7902 FLUORIDES, aerosol & ga s 1-2 12 - 800 N a OH ISE MCEF & pad w/
N a 2C O 3

7903 AC IDS , INO RG AN IC 0.2 - 0.5 3.0 - 100 H C O 3-/C O 32- IC SG(washed)

3/15/2003 MF!32 NIOSH Manual of Analytical Methods

 M eth Flow Ra te Vol. (L) E x tr a c ti o n A n a ly t ic a l
Chemical No. M e th od Na m e ( L /m i n ) T e c h n iq u e Sampler
min max

7904 CYANIDES, aerosol an d g a s 0.5 - 1.0 10 - 180 KOH ISE MCEF & BuB

7905 PHOSPHOR U S 0.01 - 0.2 5 - 100 xylene G C !FPD Te na x G C

7906 FLU O RID ES by IC 1-2 s 1 - 800 N a OH IC MCEF & pad w/

i 120 - 800 N a 2C O 3

8301 HIP PU RIC an d M ETH YL H IPP UR IC NA NA Et a c HP LC - U V NA

A C I D in U R IN E

8315 TR IAZ INE HE RB IC IDE S a nd the ir NA NA NA SC-MSD Urine

METABOLITES

8316 B U TO X Y A C E TI C A C ID in U R IN E NA NA NA G C - EC D NA

8317 ANALINE and o-TOLUIDINE in urine NA NA ALK H P LC - EC D NA

9000 ASBESTOS, CHRYSOTILE b y XR D NA NA NA XR D bu lk

9002 ASBES TOS (bulk) by PLM NA NA NA PLM bu lk

9100 LEAD in Surface Wipe Sa mp les NA NA H N O 3/H 2O 2 A A S; IC P Wipes

9101 CHROM IUM, HEXAV ALENT in s ett led NA NA NA Sp ot Te st s trip

dust

9102 ELEMENTS on WIPES NA NA NA ICP-AES Wipe

9105 LEAD in DUST WIPES by C h emica l NA NA NA Sp ot Wipe

Spot Test

9200 CHLORINATED ORG ANONITROGEN NA NA NA G C - EC D polyethylene

HER BICIDES (HAND WAS H) bag

9201 CHLORINATED ORG ANONITROGEN NA NA IPA/diazomethane G C - EC D PUF pad

HE RBIC IDES (DER M AL P ATC H))

9202 C AP TA N a nd TH IO PH EN AT EM ETH YL in NA NA NA HP LC - U V Hand wa sh

Handrinse

9205 CAPTAN and THIOPHENATEMETHYL NA NA IP A -A C N HP LC - U V Patch

on Dermal Patch

3/15/2003 MF!33 NIOSH Manual of Analytical Methods

METHOD FINDER KEY TO ABBREVIATIONS

Sampling Media/Devices Analytical Techniques

A-747 Anasorb 747 AAS Atomic absorption spectrophotometry
A-CMS Anasorb CMS AMP Amperometric detector
Ag F Silver membrane filter ASV Anodic stripping voltammetry
BuB Bubbler CD Conductivity detector
CCT Coconut shell charcoal tube DPP Differential Pulse Polargraphy
Chrom Chromosorb ECD Electron capture detector
CYC Cyclone ECHD Electrochemical detector
DNPH Dinitrophenylhydrazine Hcl ECN Electrolytic conductivity detector
Dry Drying tube EG Evolved gas analysis
GFF Glass fiber filter FAAS Flame AAS
GW Glass wool FI Flow injection
HMP 2! (Hydroxymethyl)piperidine FID Flame ionization detector
IMP Impinger FL Fluorescence detector
IOM Inspirable dust sampler FPD Flame photometric detector
MCEF Mixed cellulose ester filter GC Gas chromatography
MS Molecular sieve Grav Gravimetric (filter weight)
NITC 1! naphthylisothiocyanate GFAAS Graphite furnace AAS
OVS! 2 OSHA versatile sampler (quartz filter/XAD! 2) HPLC High performance liquid chromatography
OVS! 7 OSHA versatile sampler ( glass fiber filter/XAD! 7) HYAAS Hydride generation AAS
Pad Cellulose backup pad IC Ion chromatography
PCT Petroleum charcoal tube ICP! AES Inductively coupled plasma! atomic emission
Por Poropak spectroscopy
PTFE Polytetrafluoroethylene (Teflon) filter IR Infrared spoectrophotometry
PUF Polyurethane foam ISE Ion specific electrode
PVC Polyvinyl chloride filter MS Mass spectrometry
QFF Quartz fiber filter NPD Nitrogen phosphorus detector
SG Silica gel PCM Phase contrast microscopy
SL Soda lime PES Plasma emission spectrometry
TD Thermalalal desorption tube PID Photoionization detector
TEA Triethanolamine PLM Polarized light microscopy
XAD Polymeric resin SCD Sulfur chemiluminescence detector
SEM Scanning electron microscopy
Extraction Media Spot Spot test
aaa acetic acid/acetonitrile TCD Thermalalal conductivity detector
a acid TEM Transmission electron microscopy
ac acetate TOA Thermal optical analyzer
ACN acetonitrile UV Ultraviolet
acet acetone VIS Visible absorption spectrophotometry
al alcohol XRD X! ray diffraction
alk alkali XRF X! ray fluorescence
aq aqueous / water
aq reg aqua regia Other
bz benzene cap capacity
cychex cyclohexane i insoluble
DCE dichloroethane NA not applicable
DMF dimethylformamide port portable
DMSO dimethylsulfoxide s soluble
DNPH dinitrophenyl hydrazine var varies / variable
Et ethyl
Etac ethyl acetate
hex hexane
HSA hexanesulfonic acid
IPA isopropanol
isooct isooctane
MeCl2 /Meth methylene chloride/methanol
Me methyl
Meth methanol
MTBE methyl-tert-butyl ether
pet petroleum
PMA phosphomolybdic acid
pyr pyridine
reag reagent
THF tetrahydrofuran
tol toluene
TWM tropolone-water-methanol

3/15/2003 MF!34 NIOSH Manual of Analytical Methods