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Lab. Ex. No.1 Inspection of the Testing Laboratory
Discussion:
‘The purpose of this laboratory exercise Isto let the student become acqualnted with the mate
testing laboratory, the equipment available, the requirements ofthe course.
Preparatory reading
Appendix A,B, and C, ASTM E 380
Procedure:
1, Under the guidance of the staff member, visit the laboratory and observe where general
equipment is located.
2. Inquire on the operation of the compression testing machine.
3. Make a list of the major types of equipment available, Note the units of calibration and the dial
divisions.
Report: Write an Informal report that Includes:
41. A guide to the laboratory, with the major features Indicated on a sketch.
2. Abrief description of each major testing machine and equipments. This should include, where
appropriate, the factor necessary to convert the calibration units to the correct SI units.
3. An assessment of the role of the course In your education
‘Sketch: Draw the floor plan of the testing laboratory on the space below.sill cl vet) a) cae
toed dtdododao deed oe oe
Lab. &x. No. Reducing Fleld Samples of Aggregates to Testing Size
Discussion:
‘The correct method of obtaining a sample of aggregates for mechanical analysis is an important aspect
‘of Material Testing, The purpose of these exercises Is to obtain a representative sample for testing
Standard No, ASTM Designation 702
AASHTO Designation T 2-74
Essential Equipment and Materials:
Representative sample of aggregates
Spade
Container
‘Standard sleve, 1”
‘Sample splitter (optional)
Testing Procedure:
1. Take a representative sand and gravel. Place It in a container.
2. Wash it thoroughly with water so that it willbe free from silt and clay.
3. Dry the sample.
4, Passitto 1” Inch and disregard the sample which Is more than 1” inch in diameter.
5. Make a mound and divide it into four parts. Take the opposite division for mechanical analysis
aggregates,
6. Incase a sample divider is avalable pour the sample of combined coarse and fine aggregates.
‘The sample will be used for the sieve analysis of combined coarse and fine aggregates.
SIZE OF SAMPLES
mm Inches Minimum Weight of field Samples
b ig
9s 3/8 10 5
25 % 20 10
39 % 30 35
Fry 1 50 25
375 142 70 30
50 2 90 40
63 24 100 45
8 3 125 60
90 342 150 65|
chee de!
a
—|-.— J
da!
i it
Lab. Ex. No. Ith Determination of Surface Molsture of Coarse Aggregate
Discussion:
‘This method of test covers a procedure for determining, n the field, the amount of surface
‘moisture in fine aggregate by displacement In water, The accuracy of the method depends upon
accurate Information on the bulk specific gravity of materfal ina saturated surface-dried condition. The
same procedure, with container, may be applied to coarse aggregate.
Standard No. ASTMC70-73,
ARSHTO
Essential Equipment and Materials:
1. Sample of aggregates
2. Balance
3, Flask
Testing Procedure:
1. The surface water content may be determined elther by welght or volume. In each case the test
shall be made at a temperature range of 18 to 29 C (65 to 85 F).
2. Determination by weight ~Fillthe container to the mark with water and determine the weight
Ingrams. Empty the contalner and place enough water in itto cover the sample. Introduced the
‘weighed sample of coarse aggregates Into the container and removed the entrained al. Fillthe
container to the original mark, and determine the weight in grams. Calculate the amount of
‘water displaced by the sample, as follows:
Vee We+ Ws-W.
Where;
Vs = weight of displaces by the sample, g.
‘We = weight of container filled to the mark with water .
Ws = weight of sample, g.
W= weight of container and sample, filed to mark with water, g.
41. Determination by Volume Measure a volume of water, milimeters, sufficient to cover the
sample and place in the container. Introduced the weighed sample of coarse aggregate into the
ccontalner and removed the entrained air. Determined the combined volume of the sample and
the water by direct reading when a graduated flask is used. When a pycnometer or volumetricdeel deel
t
vr
bos! ch!
-
“lal al el
Wah GL LA CL LL ed bed ded |
flask of known volume is used, determined the combined volume of the sample and the water,
‘by fing to the mark with a measured volume of water, Calculate the amount of water displaces,
by the sample ass follows;
Venva-vt
Where:
\s= volume ofthe water displaced bythe sample, ml.
V1= combined volume of sample and water, ml
Vi= volume of water required to cover the sample, mi
Calculation:
41. Calculate the percentage of surface moisture in terms of the saturated surface-dry fine aggregate as
follows:
P= [(Vs—Val] /[(Ws=Vs)} x 100
Where:
= surface moisture in terms saturated surface dry fine aggregate percent.
\Vd = mass of sample (Ws) divide by the bulk specific gravity ofthe fine aggregate in 2
saturated surface dried condition.
‘Vs = mass of water displaced, g.
Ws = mass of sample, ¢
2. Caleulate the percentage of surface moisture in terms of dry
‘aggregate is known as follows:
/egate ifthe absorption of the
Pd = P(1+ (Pa/100}}
Where:
= surface moisture in terms of dry fine aggregate, in percent,
Pa = absorption of fine aggregate, in percent.
The total moisture content, on dry aggregate basis, fs the sum of the surface, Pd and the absorption, PaLab. &x. No. IV Sleve Analysis of Coarse Aggregates
Discussto
Sleve analysis Is used to determine the particle size distribution or graduation of an aggregate. A suitable
graduation of an aggregate In a concrete mix s desirable In order to secure workability of the mixture
and economy In the use of cement. For asphalt concrete, suitable graduation only affect the work ability
nd economy in the use of the other Important properties,
of the mixtur
Standard No.ASTM —C 136-76
AASHTO T 27-74
Essential Equipment:
1. Set of Sleves
2. Containers
Testing Procedure:
41. Obtalin proper weight of dry aggregate.
8. Coarse aggregate: 10,000 grams use method of quartering
2. Assemble sieves in the following ord
2. for coarse aggregated: 1°, X", ", 3/8", #4, #8, pan
3, Place the weighted aggregates in the top of the sieve stack and cover with the lid. Properly secure the
‘sleves in the mechanical shaker and turn on the shaker for five minutes. In case of the absence of
mechanical shaker, shake the stack of sleves with your hands continuously for the same time.
4, Weigh the materials that are retained on each of the sleves, Including the weight retained on the pan,
‘and record In the data sheet. If the sum of these weights are not within 1 percent of the original sample
weight, the procedure should be repeated. Otherwise, use the sum of the weight retained to calculate
the percentage on each sieve.
5. Compute the cumulative percent retained and the percent passing each sieve
6. Plot the gradation curves for the coarse and fine aggregates from the experiment on the graph
provided. Plot the specified gradation curves for the coarse and fine aggregates (to be specified by the
laboratory instructor). Plot the combined grading curve using 40% coarse and 60% fine aggregate.SIEVE sizes
US. Standard
Sleve Size Clear Opening In Inches
ait 1s
fe
MIN. MASS OF SAMPLE FOR SIEVE ANALYSIS OF COARSE AGGREGATES
Size of Particle Min. Mass of Sample in Kg,
ce 20SIEVE ANALYSIS DATA SHEET
Name bate
Group No. Section
‘COARSE AGGREGATE
Initial Weight:
Sieve No, Weight Retained cum.soRetained | % Passing
FINE AGGREGATE
Initial Weight:
Sleve No, WelghtRetained | MWA | cum seRetained | — %Passing
RetainedSIEVE ANALYSIS
Name Date,
Group No, Section.
GRADUATION CURVES
P 100 _
— 90
R80
© 7
N60
T 30
40
P30
A 2
Ss 10
fs) 20 «20 «100=C«Ssti tC 4 ae"
1
N
6
SIEVE SIZELab. Ex. No. Determination of Unit Weight of Coarse Aggregates
Discussion:
‘The unit welght of aggregate Is usually expressed In pounds per cuble foot. Unit weight of
‘egregate is significant in that It gives a measure of the voids In aunit volume of aggregate, The voids of
‘8Eregate depends upon many on factors, among them are size, shape and surface texture of aggregate,
[Sradation, moisture content and compaction. For general information and for comparison of diferent
‘aggregates, the standard conditions used in determining the unit weight are dry and compact.
StandardNo.ASTM —¢ 29-78
AASHTO 1 19-74
Essentlal Equipmer
1. Tamping rod
2. Volume measure
3.Seale
Testing Procedu
1 Select approximately 60 Ib. of air-dry thoroughly mixed coarse aggregate.
2. Fill the measure one-third full, level the surface and tamp with 25 strokes, evenly distributed over the
surface,
3. Fill the measure two thirds full level and tamp 25 times over the surface. Only enough force should
bbe used to cause the tamping rod to just penetrate the last layer of aggregate placed In the measure.
4. Fill the measure to overflowing, tamp as before and strike off the surplus by rolling the tamping rod
lover the surface, Do not compress the aggregate.
5. Determine the weight of the aggregate In the measure and compute the unit weight. Make at least
‘two determinations. Results should agree within one pereent.TaBLE!
DIMENSIONS OF MEASURE, U.S. CUSTOMARY SYSTEM.
Capacity insides Wlgth Win, Thckneses of Tominal see
th’) Diameter (in) (in) Metal (in) of Aggregates
(ina)
bottom wall
vio so01 6a Z0a 020 010 %
3 8.0+0.1 115 40.1 0.20 0.10 1
% toto, 120404 020 0 1%
a motor 11240 020 on 4
Taste?
Dimensions of measures, Metric System
Capacty inside Inside Min. Thickness of Max. Nominal
Uiters) Diameter ‘Height: ‘Metal (mm) ‘Size of
(mm) tend Aaaregates
(mm. b)
bottom val
3 mh 10 50 25 25
10 205 +2 205 +2 5.0 25 25.0
1s 254229542 so 30 375
2» 354230542 50 30 100
2) The indicated size of container may be used to test aggregates of a maximum nominal size
equal to or smaller than that listed.
'b) Based on sieves with square openings.TABLES
‘Unit Welght of Water
une a ee
Temperature Thi kale
°F °C
6 156 2366-99901
6 183 62366 998.53,
70 aa 62301 997.97
(734) (23.0) (62,274) (597.53)
78 239 62261 997.32
80 26.7 62216 996.60
5 298 62166 995.80
UNIT WEIGHT OF AGGREGATE
ara SHEET
Name: ate:
Group No, Seaton:
Aggregate:
Max. Se
Nom. Grad;
Source:
um TOTAL
7~2][3] 4
Total Weught (bs)
Measure Welght (bs)
Wr of Age. (ibs)
Measure Vol (cu. Ft)
‘Unit we. (Ib.feu.t)
‘Sadifference from ave.
“Average Unit Weight, petLab fx, No. WI Determination of Specific Gravity and absorption of Coarse Ageregates
Discussion
‘Basically, specific gravity bs the ration of the weight of a given volume of material tothe weight of an
‘equal volume of water, However, there are several varlatlons ofthis definition depending upon the
‘material and purposes for which the value of specific gravity Is to be used. In concrete work, the term
specific customarily refers to the density of the individual particle, not to the aggregated mass as a
whole, The most common definition of specific gravity In concrete aggregate Is based upon the bulk
volume of the individual aggregate in a saturated surface dry-condition ($80). The bulk (oven-dry)
‘specific gravity and apparent specific gravity are used to a lesser degree. Solid unit welght In pound per
‘cubic foot (pef] of an aggregate Is customarily defined as the specific gravity times 62.4 pet.
‘The absorption capacity Is determined by finding the weight of an aggregate under SSD condition and an
‘oven-dry condition. The dference in weight expressed as a percentage of the oven-dry sample weight Is
the absorption capacity. Coarse aggregates are considered to be saturated surface-dry when they have
been wiped free of visible moisture films witha cloth after the aggregates have been soaked in water for
‘along petiod of time (over 24 hours). The saturated surface-dry condition of fine aggregate is usually
taken as that at which a previously wet sample just became free-flowing.
Standard No. ASTM. 127-77
ARSHTOT 8!
Essential Equipment (for Coarse Aggregate)
1. Seale sensitive to 0.01 in, oF 1 gm,
2. Wire mesh basket
3. Balance sensitive to. gm
4. Drying oven
5.3/8" sieve
Testing Procedure
1, Soak coarse aggregate under water for 24 hours (done for you by laboratory instructor)
2, Obtain approximately kg of saturate coarse aggregate (retained on 3/8" sieve).
3. Trowel the aggregate to the saturated surface-dry condition ($0)
14, Measure SSO welght. (8) of aggregate in arto the nearest 1 gram. Do this quickly to prevent
‘evaporation.5. Place @ sample in @ wire mesh basket, and determine its weight in water (). Be sure to subtract the
submerged weight ofthe basket of the basket from the total.
6, Place wet aggregate In oven and dry to constant weight (A). Leave the aggregate in oven over night.
7.From the above data (Le A, 8, and C) calculate three types of specific gravity and absorption as
Sefined below:
4. Apparent pectic Gravity
2. Buk Specte Gravity (SSD)
3, Bulk Specific Gravity (ORY)
4. Absorption Percentbee
bse nk
at
SPECIFIC GRAVITY AND ABSORPTION OF AGGREGATE
Name:
Group No.
DATASHEET
FINE AGGREGATE
ITEM
SSD Wt. Air (0)
Wt. of Pye. + Water (8)
Wt of Pye. + Water + Sample
(8)
‘Oven Dry Weight (A)
‘COURSE AGGREGATE
ITEM
‘SSD Wt. In Ar (8)
Wt. in Water (C)
‘Oven Dry Wr. (A)
RESULT
Coarse
Fine
Apparent Specific Gravity
Bulk Specific Gravity (Dry)
Bulk Specific Gravity (SSD)
Absorption
Date:
Section:
Nom. Size:
Nom Size:
Source:Lab. Ex. No. Vil: Fineness of Cement
The rate of hydration and hydrolysis and the consequent development of strength In a cement
‘mortar depends upon the fineness of the grinding the cement. To have the same rate of hardening in
ifferent brands of cement, the fineness has been standardized as follows:
The finer cement have quicker action with water and galn strength, though the ultimate
Strength is not affected, Fineness also gives it more cohesiveness and reduces the separation of water at
the top of concrete, However, the shrinkage and cracking of cement concrete which Increases In the
rate of strength development are higher with finer cement,
‘The objective of this experiment is to determine the fineness of cement by sieve analysis,
Essential Material and Apparatus:
‘Sample of Portland Cement
Balance, sensitive to 0.1 gm
Standard Sleve #200
Essential Procedure:
(1) Accurate weigh 100 gm of cement and place It on #200 sleve.
@)
skdown any alr-set lumps in the sample with fingers, but do not rob It on the sieve,
(3) Steving Is done by:
jentle motion of the wrist for 15 minutes continuously.
(4) The residue shall be the weighed and should not exceed 10 percent by weight of the cement sample.ab. Ex. No. Vil: Consistency of Standard Cement Paste
Consistency one property of the fresh concrete, Is an Important consideration In securing of a
Workable concrete that can be properly compacted In the forms, The term consistency relates fluidity
from the driest to the wettest mixtures. The common tests to determine consistency are the “slump”
test and the “ball penetration” test. These tests glve only rough measures of consistency, but they do
{ve satisfactory measures of this property for most practical work.
For convenience, varlous degrees of wetness of a mix may be roughly classified as dry, tif,
‘medium, wet, or sloppy. A concrete Is sald to have medium or plastic consistency when it is Just wet
‘enough to flow sluggishly ~ not so dry that it crumbles or so that water or paste rums from the mass,
The principal factors affecting consistency are (1) the relative proportions of cement to
‘aggregate (2) the water is content of aggregate (3) the size aggregate (4) the shape and surface
characteristics of the aggregate particles and (5) the fineness and type of cement and the kind and
‘amount of a mixture,
‘The aim of this experiment isto find out for a given cement the quality of water to be mixed to
‘ive a paste of normal consistency.
Essential Materials and Apparatus:
Sample of Portland Cement
Balance, sensitive to 0. em.
Vicat’s Apparatus
Spatula
Essential Procedur
(2) Weigh accurately about 300 gm of neat cement sample to be tested.
(2} Mix about 25% of a clean water to the cement by means of spatula.
(3) After about @ minute, mixed it thoroughly with hands for at least one minute.
{4) The kneaded paste is formed into a ball and tossed about sbx times from one hand to another.
{5} The balls then pressed into a rubber mold and the excess paste ls removed.
(6) The larger end of the rod is brought in contact with the surface of the paste and reading on the scale
Is taken(7) The rod is then quickly released without any jerk and penetration noted. If the rod penetrates by 33,
1035 mm the paste is sald to be of “normal consistency”.
(8) The time taken between adding of water to cement and the filling of the mold should be between 3
t05 minutes,
(8) Trial pastes should be made with varying percentage of water to determine the percentage for which
the desired penetration is obtained. The amount of the water Is expressed as percentage by weight of
dry cement usually 30%,
‘Appropriate range Is slump of concrete for varus degrees of consistency.
Consistency Slump, mm Remarks
Oy (0-25 Crumbles and falis apart under ordinary handling; can be
‘compacted into rigid mass under vigorous ramming, heavy
pressure and vibration, but unless care Is used exhibits
voids or honeycomb.
stift 15-65 Tends tostand asa plle; holds together fatly well but
‘crumbles ifchuted; with care and effort can be tamped
Into solid dense mass; satisfactory for vibratory
‘compaction.
Medium 50-140 Alternate terms; plastic, mushy quaking. Easly molded
although some care required to secure complete
‘compaction.
Wet 125-200 Pile flattens readily when dumped; can be poured into
place.
Sloppy 175-250 Group of mortar tends to run out of pile, leaving coarser
material behind,kf ey df di de
Bie ae
i oo
Wee edd
ab, fx, No. Fale Set in Cement
To.ensure sufficlent times to place concrete while It remains plastic, # minimum lint is inganed
(on the time of “initial” set, which may be taken as the condition of the mass when it begins to shiffen
appreciably. ASTM specification require that Initial set should nat take place within one hur. Depending
‘on the test used to determine it, initial set usually takes place within two or four hours. To ensure that
the cement wil harden for use, a minimum fimit is Imposed on the time of “finat” set. ASTIA
specifications requires that final set occurs within five to eight hours. The condition of initial and final set
1s determined by penetration of standard needles or rods Into a “neat” (straight) paste of specified
consistency.
Essential Materials and Apparatus:
Sample of Portland Cement
Balance, sensitive to 0.1 gm
Vieat’s Apparatus
Spatula
Mixing container
Essential Procedure:
(1) Take a cement sample about 500 gm in weight.
(2) Make a conical pile and mix with water.
{3) Place the mixture in a rubber mould and level the top.
(4) Place it in the Vicat's Apparatus. The larger and should be placed in contact of the surface of the
mixture and the reading should be set at zero mark.
(5) Release the plunger and after 30 seconds, read the reading on the scale, The reading should not read
lessthan 352mm.
(6) Level the mixture in the mould and wait for about 5 minutes for another testing. Repeat steps 4 and
5.
(7) The ditference of the first and final testing in the Vieat’s needle reading should not exceed 17 mm.Lab, b4.No. x: Determination of Time Setting of Hydraulle Cement by Vicat Needle (intial Set
‘of Cement)
Discussion:
‘The Initia set fsa stage in the process of hardening after which any cracks that may appear wil
‘not reunite. The concrete Is sald to be finally set when it has attained sufficient strength and hardness,
Standard No. ASTM 191-71
AASHTOT 131-74
Essential Equipment and Materials:
4. Portland cement sample
2. Balance sensitive to0.1 gm.
3. Vieat Apparatus
4, #200 sieve
5, Mixing container
6. Spatula
Testing Procedure:
4. Test for fineness of cement (350 gm).
2. Weigh about 300 gm. of cement accurately and make a paste with 0,085 times the water required to
make a paste of normal consistency.
3. The paste Is then placed inthe rubber mold.
4. The small end of the rod Is brought in contact with the surface ofthe paste and quickly released.
5. The penetration of the needle can be read on the goals. The intial set is sald to have occurred when
the needle ceases to pass a point 5 mm above the bottom of the mold.
6, The time taken from the instant of adding water to the cement up to the moment when the needle
ceases to penetrate 2 point 5 mm above the bottom of the mold Is known as the itil setting of the
cement.
For ordinary Portland cement, the Initial setting time should not be less than 30 minutes.Lad. Ex. No, xt Laboratory Concrete this Proportioning
Discusston:
The purposes of the experiment are: (1) to use the teal mia method described hereina
Setermine optimum proportions of aggregates, cement, and water for concrete to meet specified
strength requirements, (2) to learn concreting practice In laboratory environment, and (3) to observe
the characteristic properties of fresh concrete,
Standard No. ASTM 192469
e143
AASHTO. 7126-70
7119-74
Essential Equipment:
1.6" X6" X18“ horizontal molds
2. Five 6" X 12" cylinder molds with cover plates
3. Two large containers for stocking aggregates
2) Large mixing pans, two trowels, slump cone, tamping rod 12” rule
5. Scale sensitive to0.01 Ib,
Trial Mix Design Procedure
‘This procedure is for calculating the approximate quantities of coarse aggregate, fine aggregate,
cement and water needed to make up one cubic yard of non air-entrained concrete of specified
Compressive strength. This calculation should be done before the beginning of the laboratory period.
Results of the design shall be submitted to the laboratory instructor for his approval.
1. The following information shal be provided to each party by laboratory instructor:
1a). 28-day compressive strength required forthe concrete.
'b) Properties of the coarse and fine aggregate Including maximum aggregate ste, fineness
‘modulus of the fine aggregate, effective absorption ofthe fine and coarse aggregates.
Assume normal Type 2 portland cement isto be used In the laboratory and slump of the
concrete mix will be ranged between 3 and 4 in,
2. Based on the 28-day compressive strength, obtain the water cement ratio required from table for alt=
entrained concrete using Type 1 portland cement.Lab. Ex.No.X Determination of Time Setting of Hydraulle Cement by Vicat Needle (Initial Set of
Cement)
Discussion:
the Initial set is a stage In the process of hardening after which any cracks that may appear will not
reunite. The concrete Is sald to be finally set when It has attained sufficient
strength and hardness.
Standard No. ASTM ¢ 191-71
ARSHTOT 131-74
Essential Equipment and Materials:
4. Portland cement sample
2. Balance sensitive 0.1 gm
3. Vieat apparatus
4.11200 seve
5. Mixing container
6. Spatula
Testing Procedure;
1. Test for fitness of cement (350 gm).
2, Weigh about 300 gm. of cement accurately and make a paste with 0.085 times the water required to
make a paste of normal consistency.
3. The paste s then placed In the rubber mold.
4, The small end ofthe rod is brought in contact with the surface of the paste and quickly released,
5, The penetration of the needle can be read on the goals. The intial set is sald to have occurred when
the needle ceases to pass a polnt 5 mm above the bottom of the mold.
6, The time taken from the Instant of adding water to the cement up to the moment when the needle
‘ceases to penetrate a point 5 mm above the bottom of the mold is known as the initial setting of the
cement.
Forerdinary portland cement, the intial setting time should not be less than 30 minutes.Lab. Ox. No. Xt Laboratory Concrete-thlx Proportioning
Discussion:
The purposes of the experiment are: (1) to use the trial mix method described hereinafter to
determine optimum proportion of aggregates, cement, and water for concrete to meet specified
strength requirements. (2) to learn concreting practice in laboratory environment, and (3) to observe
the characteristies properties of fresh concrete.
Standard No, ASTM. €192469
cuan
AASHTO T 12670
Tu974
ESSENTIAL EQUPMENT:
1.66" 18" horizontal molds
2. Five 6" x 12" cylinder molds with over plates
3. Two lage containers for stocking aggregates
4. Large mining pan, two trowel, sump cone, tamping od 12° rule
5. Seale sensitive to 0.01 Ib.
‘rial Mix design Procedure
This procedure is for calculating the approximate quantities of coarse aggregate, fine aggregate,
cement, and water needed to make up one cubic yard of non air-entrained concrete of a specified
‘compressive strength. This calculation should be done before the beginning of the laboratory period.
Results of the design shall be submitted tothe laboratory instructor for his approval.
4. The following information shal be provided to each party by laboratory instructor:
{2} 28-day compressive strength required forthe concrete.
(b) Properties ofthe coarse and fie aggregate including maximum aggregate sie, fineness modulus
ofthe fine aggregate, effective absorption ofthe fine and coarse aggregate.
(c) Assume normal Type 1 portland cement ito be used in the laboratory an slump ofthe concrete
‘mix will be ranged between 3 and 4 in.2. Based on the 28-day compressive strength, obtain the water cement ratlo required from table for
entrained concrete using Type 1 portland cement,
3. Based on the W/C the maximum aggregate size and FM of the fine aggregate, and using the table,
‘compute the quantities ofthe coarse aggregate (ac), fine aggregate (af), cement (c), water (wc) for
hydration, and water (wao) and (waf) needed to bring the coarse aggregate and fine aggregate in the
‘SSD conditions for one cubic yard of concrete by ACI method. Record these results in the data sheet.
4. divide all the quantities determined in step 3 by 27 to obtain the estimated quantities of the materials,
(ac, af, C, We, Wac, Waf) for one cuble ft. may be needed. Consult the laboratory Instructor for the
amount of concrete needed.
Laboratory Batching Method:
5. Weigh the amount of coarse aggregate (ac), determined in Step 4, store in a container.
{Add the amount of water of for effective absorption (Wac) tothe aggregate and mix them thoroughly
Weigh the amount of fine aggregate (af) (Waf) mix them thoroughly. Record all the weights in the data
sheet.
6. Welgh the quantity of cement {c) and put ina larger mixing pan. Welgh the amount of water
for absorption (Waf) mix them thoroughly. Record all the weights in the data sheet.
7. Coarse and fine aggregates contalned In Step $ are added Into the miking pan to produce a
concrete mix with the desired slump of 3 to 4 In, and with good workability. This can be done by first
‘using only 2/3 of the coarse and fine aggregates and thoroughly mixing the aggregates with the paste,
Then test the slump (see step 8 for sump test). At this pot, the slump ofthe mixture should be greater
than 4”. Gradually add small quantities of fine or coarse aggregate (or both) and thoroughly remix the
concrete and test the slump. Repeat this process until the mix reaches the desired slump. As the limiting
slump is approaching, the batch should be carefully examined in order to judge which aggregate to add.
‘The correct amount of sand isthe minimum which will produce enough mortar to fil the space between
pieces of coarse aggregate. In general understanding creates harshness (lack of toweling ability) and
show lack of cohesiveness whereas oversanding decreases “yleld” and may result In greater potential
volume change. When the batch is judged to b satisfactory, the remaining supplies of aggregates are
weighed and recorded inthe data sheet.
8. In testing the slump, the mold shall be dampened and placed in the mixing pan. The mold
shall be firmly held down against the pan. Fill the slump cone with concrete in three layer, each
approximately one-third of the volume of the mold. Each layer shall be rodded with 25 strokes,
distributed uniformly over the cross-section of the cone. The rod shall lightly penetrate the previouslayer, After the top layer has been rosdded. The surface of concrete shall shall be struck of with a trowel
So that the cone is exactly filed, The cone shall be Immediately removed from the concrete by ralsing It
carefully in a vertical direction, The slump shall be measured immediately by determining the difference
‘between the height of the mold and the height of the subsided concrete, After the slump measurement
{s completed, the side of the concrete frustum should be tapped gently with the tamping rod. The
‘behavior of the concrete under these treatment Is a valuable Indication of the cohesiveness. A well
roportioned mix will gradually slump to lower elevation and retain its original form while a poor mix
willerumple, Segregate and fall apa
9. Before iting the concrete nto a cylinder molds, determine the weight of exch cylinder mold
{and record the weight in the data sheet. The cylindrical concrete specimen shall be formed by placing
the concrete in the cylinder mold In three layers of approximately equal volume. Each layer should be
‘rodded with 25 strokes using 8 tamping rod. The strokes should be alstibuted uniformly over the cross
section of the mold, Also the cylinder mold filed with conerete should be tapped gently with the
tamping rod. This treatment will help to consolidate the concrete and to drive out the air bubbles
trapped in the concrete After the top layer has been rodded, the surface ofthe concrete shal be struck
‘out with a trowel. Three cylinder concrete specimen shall be made. Measure the weight of each cylinder
mold filed with concrete and record the welghts In the data sheet. Cover each with a greased glass
plate.
20. The beam specimen shall be formed by placing the concrete In a steel beam mold in two
layers of approximately equal volume. Each layer shall be rodded with n strokes (one strokes per 2
‘square inches) cover the top surface of the beam with a greased steel plate.
11. After 24 hrs, test specimen shall be removed from the molds and stored in the curing room.
12. Compute the unit weight of concrete, the weight of materials for making one cuble yard of
concrete and the “cement factor” for the concrete mix. Record these results In the data sheet.
Table for Compressive Strength of Concrete for Varlous Water-Cement Ratlo,
Probable Average for Compressive Strength at 28 days,
Water-Cement Ratio pl (Type I Cement)
Chas Non-Air-Entrained
femece Alr-Entrained Concrete
036 ‘6000 4800
04s 5000 3800
056 4000 3300
61 3500 2700
0.67 3000 2300
078 2500 2000‘Table for Bulk Volume of Coarse Aggregate (cu. ft.) Per Cuble Yard of Concrete
Maximum site of Mictalaet tac
Aggregate (in)
24 26 28 30
v8 135 130 124 110
% 159 154 148 143
x v7 167 162
1 192 186 184 176
np 202 197 192
2 aa 205 200 194
3 na 216 216 205
‘Table for Appropriate Mixing Water Requirements for Different Slumps and Maximum Sizes of
‘Aggregates
‘Alrntralned Concrete Non-AirEntained Concrete
Maximum | Recommended Approximate
Sueot | Total —- mount AP. inane
Water, b/eu. yd. of Water, Ib/eu. yi of
Concrete Concrete
36 73 310 340 3603
350 385 419
% 75 300 25 340 25
335 365 385
% 6 25 300 as 2
310 340 360
1 6 260 238 300 15
300 25 340
1A 5 240 265 2s 4
25 300 315
2 5 2s 250 265 0s
260 235 300
3 4 210 2s 03
240 268 -
6 3 185 200 02
210 235(CONCRETE TRIAL MIX DATA
sane ue croup Wo,__ Seton
seatwe dn Aegean
Esso Conon Tie ewerter
sows ws Absorption
e__freshater__ Seawater Fe reste x
Design Strength ps Coarse Aggregate, %
wc fr stent voiture
wc tor expovre tine Awerte x
wicterus conse never “
van PROER] MRGER Tat | wee | wea
| aut | a | een | nemoning | Und
Mere stump Weraity
‘wr. Container + Conerete
Wt. Container =
wr. Concrete =
Vol. of Container
Unit Wt. of Conerete=
Fine Aggregate Percentage of Total Aggregate.
Wt. for 1 yd3 of Concrete,
Cement Factor
Coarse Age.
Fine Age.
Total Water.Lab, Bx. No. Xt: Slump Test of a Concrete
Aslump tests mate by measuting the settlement of a 12 ~In, (300 mm) high, formed In mold
that hasa shape of afrustum of a cone
Essential Material and Apparatus:
Slump one Device
Portland Cement
Sand and Gravel
Spade
‘Standard Sieve, 1”
Container
Mixing box
Essential Procedure:
(1) Take a sample of cement, sand and gravel
(2) Wash the sand and gravel thoroughly with a waters that wil be free from itt and cay.
(3) Weigh equal amount of sand and gravel fora total of about 15 kg. and place them In a mixing box.
‘Add 2 kg. of cement, add water, using a water-cement ratlo of 0.45, 0.55, or 0.65. Keep precise records
of the amounts. Its convenient to measure the water ina beaker (1L = 1 kg.). Mix them thoroughly. Use
a misture of 1:2:4.
{8) Put the concrete mixture to the slump cone device up to depth of 4 In. then tamp with a rod evenly
distributed over a cross section. Tamp it 25 times.
(5) Again add to the device another portion of the concrete mixture another 4 In. deep and tamp with
rod another 25 times.
(6) Add a concrete mixture to the device until its full. Rod It again for 25 times of a depth of 4 in. and
then level the top ofthe cone,
(7) Gently lft the slump cone device by lifting It from the handle.
(8) Measure the distance of setting and compare the result to the allowable slump shown on the
previous table,Lab. Ex. No. Xt Test For Weight Per Cublc Foot, Vield, and Alr Content (Gravimetric) of
Concrete
Discussion:
‘This tests covers the determination of the weight per cubic foot of freshly mixed concrete and
‘ives formulas for calculating the yield, cement content, and the air content of the concrete. Yield Is
defined as the volume of the concrete produced from the mixture of known quantities of the competent
materials,
Standard No.ASTM 138-77
AASHTO T 121,
Essential Equipment:
1. Balance
2. Tamping Rod
3. Measure
4, Strke-Off Plate
5. Calibration Equipment
Testing Procedure:
1. Compact measures smaller than 0.04 ft3 (10 dm3) by rodding because of the danger of excessive lors
of entrained alr. For measures 0.4 ft3 (10 dm3) or larger, base the selection of the method of
consolidation on the slump unless the method is stated in the specification under which the work Is.
‘being performed. The methods of consolidation are rodding and internal vibration. Rod concretes with a
slump greater than 3 inch (75 mm). Rod or vibrate concrete od 1 to 3 in. (25 to 75 mm). Consolidate
concrete witha slump less than 1 in. (25 mm.) by vibration.
2, Rodding ~ Place the concrete in the measures in the three layers of approximately equal volume. Rod
‘each layer with 25 strokes of the tamping rod when the O.S ft3 (14 dm2) or smaller measures are used
and SO strokes when the one cubic feet measure is used. Rod the bottom layer throughout its depth but
the rod shall not forcibly strike the bottom of the measure. Distribute the strokes uniformly over the
cross section of the measure and for the two layers penetrate about 1 in. / (25 mm) into the underlying
layer. After each layer is rodded, the sides of the measure smartly ten or more times until no large
‘bubbles of air appear on the surface and voids left by the tamping rod are closed. Add the final ayer so
as to avoidd overfiling3. On completion of consolidation the measure must not contain a substantial excess or deficiency of
concrete, An excess of concrete protruding approximately 1/5 in, ( 3mm.) above the top of the mold is
ptimum. A small quantity of concrete may be added to correct a deficiency. Ifthe measure contains a
‘reat excess of concrete at completion of the excess concrete with a trowel or scoop immediately
following completion of consolidation and before the measure is struck-off
4, Struck-off ~ After consolidation strke-off the top surface ofthe concrete and finish it smoothly with
the first strike-off plate using great care to leave the measure just level full. The strike-off is best
‘accomplished by pressing the strike-off plate on the top surface of the measure to cover about two thirds
of the surface and with-drawing the plate with vertical pressure and a sewing motion to cover the whole
surface of the measure. Several final strokes with the inclined edge of the plate will produce a smooth
finished surface.
5. Cleaning and Weighing ~ after strike-off, clean all excess concrete from the exterior ofthe measure and
determine the net mass ofthe concrete in the measure to an accuracy consistent with the requirements
Caleulation:
1, Unit weight (Density) ~ calculate the net density of the concrete in pounds (or kilograms) by
subtracting the mass of the measure from the gross mass, Calculate the mass per cubic foot (or cubic
‘meter) by multiplying the net mass by the calibration factor forthe measure used.
2. Vields ~ calulate the yield, V. (volume of conerete produced per batch) by avoiding the total mass of
all materials batched, W. by the density, W. determined in procedure 6.1. The total mass ofall materials
batched is the sum of the cement, the fine aggregate in the condition used, the mixing water added tothe
batch and any other solid or liquid materials used.
3. Relative Yields relative yiels isthe tio ofthe actual volume of concrete obtained tothe volume as
designed forthe batch calelated as follows:
Y
Rvs
Where:
Ry = relative yield
Y = volume of the conerete which the batch was designed to produces.yd(m).
4, Cenvent Content — calculate tha actual cement content as follows:
NeXt
Y
Where:
N = actual cement content. b/d (kg/m)
Nz= mass of cement in batch. (ka).
5. Ait Content calculate the air content as follows:
OrWhere:
‘A = air content (percentage of voids) inthe concrete
T= theoretical mass ofthe concrete computed on an airfre basis. b/A? (or ke/m')
W = density (unit weight) of concrete, Ib/ft’ (or kg/m’), and
\V = total absolute volume of the computed ingredients inthe batch, 0(m’)Lab. Ex, No, NIV Determination of Ale Content of Freshly Mix
Concrete
Ry the Volumetric \
thod
Discussion:
type of aggregate, Whether it be dense, cellular, or lightweight, This testis one of the essent
‘This metho covers the determination of the air content of freshly mixed concrete containing any
test in the
Preparation of a concrete test specimen.
Standard No. ASTM C 173-78
AASHTO T 196-74
Essential Equipment:
Airmeter
Bow!
Top Section
Funnel
‘Tamping Rod
Strike-off Bar
Measuring Cup
Syringe
Pouring Vessel
10. Trowel
1. Scoop
Calibration of Apparatus
‘The volume of the bowl of the airmeter, in cubic feet or cubic meters shall be determined by
accurately weighing the amount of water at 21, JC namely 62.3 bof. A glass plate shall be used to cover,
the bowl to remove excess water and to ensure that the container is full.
Testing Procedure:
1
Rodding and Tepping ~ Using the second, sided by the trowel if necessary, fill the bow! with
freshly mixed concrete in three layers of equal depth. Fod each layer 25 times with the tamping
rod and tap the sides ofthe bow! 10 to 15 times after ench rodding
Striking Off — after placement ofthe third layer of the concrete strike off the excess coneretewith
the strike-off bar until the surface is flsh withthe top ofthe bowl. Wipe the flange of the bowl
clean.
‘Adding Water ~ Clamp the top section into position on the bowl, insert the funnel, and add the
‘water until it appears in the neck. Remove the water and adjust the water level, sing the rubber
syringe, until the bottom of the meniscus is level with zero mar Attach and tighten the serew cap.
Agitating ang Folling - Invert and agitate the unit until the concrete settles free from the base, and
then, with the neck elevated, roll and rock the unit until the air appears to have been removed
from the concrete. Set the apparatus upright, jar it lightly, and allow it to stand until the air rises
to the top. Repeat the operation until no further drop inthe water column is observed.5. Dispelling Bubbles - when all the air has been removed from the concrete and allowed to rise to
the top of the apparatus, removed the screw cap. Add, in I-cup increments using the syringe,
suficient isopropyl alcool to dispel the foamy mass on the surface ofthe water.
6. Reading - make a direct reading ofthe liquid on the neck, reading othe botom ofthe meniscus,
and estimating tothe nearest 0.1%,
Cateulation:
Calculate the air content of the content in percent by adding to the reading from 6 the amount of
alcohol used in accordance with $,Lab. EX.No.NV Determination of
Discussion:
‘observe the behaviour of concrete under compressive londing and study the fractu
inressive Strength of Concrete
‘The objective ofthis experiment isto determine the compressive strength of the concrete, 10
ifthe concrete under
‘compressive loading. This tet isthe standard test used to determine the compressive strength of concrete
Standard No. ASTM 39-72
AASHTO 722-74
Essential Equipment:
Testing machine with 200,000 Ibs. capacity or compression machine.
Concrete cylinder
Capping apparatus
Compressometer
‘Testing Procedure:
‘Remove the concrete cylinder from the curing room and surface dry the cylinder.
Cap the conerete cylinder.
‘Artach the compressometer tothe cylinder. Make sure the compressometer is properly positioned
and dial gage attached tothe compressometer will respond properly
Place the cylinder in the loading machine, Zero the load needle. Adjust the loading head ntl a
small load (about 50 Ibs) is applied to the cylinder, Zero the dal gage reading. For high strength
concrete (above 4,000 psi compressive strength) it is advisable to place a protecting shield
‘between the cylinder and the observers
‘Apply compressive load slowly and continuously until the maximum load (failure) is reached.
During the testing take simultaneous load readings from the load dial and deflection readings
from deflection gages at intervals indicated by laboratory instructor. Record the loads and the
corresponding deflection readings on the data sheet. Failure of the cylinder is imminent during
the test when the 32 load indicator is slowing down and finally stops while the deformations
indicated in the deflection gage continues in an increasing rte, When the load indicator stats to
drop from the maximum load in the datasheet.
Remove the cylinder from the testing machine, detach the compressometer from the cylinder, put
the cylinder back in the machine, and reapply the compressive load until the eylinder is toally
crushed, Release the load and raised the loading head. Examine closely the type of failure of the
cylinder.jummary of Hardened Concrete Properties
we
Curing Conditions
CompressiveLab, Ex. No.XVI_ Determination of Tensile Strength of Cylinder Concrete Specimens
Discussion:
‘This method of test covers the determination of the splitting tensile strength of cylindrical
concrete specimens such as molded cylinders and drilled cases. This test Is not as Important as the
compressive test of cylindrical concrete samples since it will determine the split tensile strength of
concrete,
Standard No. ASTM = 496-71
ARSHTO T 198-74
Essentlal Equipment:
1. Testing machine
2. Bearing bar
3. Plywood strips
Testing Procedure:
1, Measure the dimensions of the cylinder. Draw diameter lines on each and of the specimen in the
same axial plone.
2. Center one plywood strip along the center ofthe lower bearing block ofthe testing machine, Place
the eyinder onthe plywood strip and align zo that the lines marked onthe ends of he specimen are
vertical and centered over the plywood strips. Place @ second plywood strip lengthwise on the
evlinder and place 92° x 2" x12" steel bar over the plywood stip, Lower the upper loading head
until the assembly is secured in the machine.
3. Apply the compressive load slowly and continuously unt falure. Record the maximum applied load.
Examine the type of allure.
Compunstion:
4. Compute the spit ten strength Sp = 2%
Where:
Sy =Splting tensile strength
F = Maximumload aplied
L eLength of concrete
D = Diameter of concrete sample
Ultimate toad:Lab. Bx. No. XVI ‘Test For Flexural Strength of Concrete
Discussion:
This method covers the determination of the flexural strength of small size concrete
specimens by the use of a simple beam with center point loading.
Standard No, ASTM 496-71
AASHTO. T 198-74
Essential Equipment:
1. Testing machine
2, Flexure testing attachment
Testing Procedure:
41, Measure the dimensions of the beam and record them in the data sheet.
2. Place the concrete beam in the flexural attachment and position the assembly in the compression
‘machine. Adjust the loading head untilit sin contact with the top of the assembly.
3. Apply load slowly until beam breaks. Examine the type of failure. Record the maximum load,
Computation:
1, Compute the modulus of rapture (maximum flexure stress at fallure) My
oF
R= en
jodulus of rapture
P= maximum load applied
pan length
average width of specimen
H_ = average depth of specimen
Unimateload=___Mp
Sketch of Falled Section
ab. Ex. No. XVII Determination of Compressive Strength of Concrete Hollow BlocksDiscussion:
This task seeks to determine the ultimate compressive strength of concrete hollow blocks. The
Procedure ofthe test Is similar to the test for compressive strength of concrete,
Essential Equipment:
1. Compressive machine
Testing Procedure:
11, Place the bottom of a concrete hollow block on a compression block made of 1 inch plywood. Place
‘another 1 Inch plywood on top of the conerete hollow block,
2. Apply the compression load slowly on the plywood unt fallure is attained.
3. Test a total of three hollow blocks for each batch.
Computation:
1. Compute the ultimate compressive stress of concrete hollow blocks.
Maximum compressive Load
Ultimate compressive Stress = Mesimum ounptensset
‘Compute the average value forthe three samples tested,
Lab. Ex.No.XIX Test For Compression of Wood Parallel To The Grain
Discussion:
‘The purpose of this experiment Is to determine the strength of wood under compressive
loading.
Standard No, ASTM D 143-83
D 198-84
Essential Apparatus:
1, Testing machine
2. Load Indicator
3, Bearing blocks
4. Compressometer
Procedure:
4, Measure the cross section and length of the specimen to the nearest 0.01 In, Record the dimensions.
of the specimen of the specimen,
2. Place the specimenin the machine.3. Apply the load continuously until the specimen falls, Record the maximum load.
4. Drawa sketch in perspective, indiating the grain of wood and manner of failure.
Computation:
1. Compute the compressive strength
Total Load
‘rea of Bearing